scanning droplet cell
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2020 ◽  
Vol 117 (12) ◽  
pp. 6316-6322 ◽  
Author(s):  
Yonggang Yao ◽  
Zhennan Huang ◽  
Tangyuan Li ◽  
Hang Wang ◽  
Yifan Liu ◽  
...  

Multimetallic nanoclusters (MMNCs) offer unique and tailorable surface chemistries that hold great potential for numerous catalytic applications. The efficient exploration of this vast chemical space necessitates an accelerated discovery pipeline that supersedes traditional “trial-and-error” experimentation while guaranteeing uniform microstructures despite compositional complexity. Herein, we report the high-throughput synthesis of an extensive series of ultrafine and homogeneous alloy MMNCs, achieved by 1) a flexible compositional design by formulation in the precursor solution phase and 2) the ultrafast synthesis of alloy MMNCs using thermal shock heating (i.e., ∼1,650 K, ∼500 ms). This approach is remarkably facile and easily accessible compared to conventional vapor-phase deposition, and the particle size and structural uniformity enable comparative studies across compositionally different MMNCs. Rapid electrochemical screening is demonstrated by using a scanning droplet cell, enabling us to discover two promising electrocatalysts, which we subsequently validated using a rotating disk setup. This demonstrated high-throughput material discovery pipeline presents a paradigm for facile and accelerated exploration of MMNCs for a broad range of applications.


RSC Advances ◽  
2017 ◽  
Vol 7 (10) ◽  
pp. 6031-6039 ◽  
Author(s):  
Isabella Pötzelberger ◽  
Cezarina Cela Mardare ◽  
Lisa Maria Uiberlacker ◽  
Sabine Hild ◽  
Andrei Ionut Mardare ◽  
...  

A co-evaporated Cu–Pd thin film combinatorial library was screened for electrocatalytic oxidation of formaldehyde by scanning droplet cell microscopy. The best activity was found for 7.5 at% Pd and an amperometric sensor was fabricated and tested.


2015 ◽  
Vol 179 ◽  
pp. 32-37 ◽  
Author(s):  
Jan Philipp Kollender ◽  
Andrei Ionut Mardare ◽  
Achim Walter Hassel

2015 ◽  
Vol 740 ◽  
pp. 53-60 ◽  
Author(s):  
Jan Philipp Kollender ◽  
Michael Voith ◽  
Simon Schneiderbauer ◽  
Andrei Ionut Mardare ◽  
Achim Walter Hassel

2014 ◽  
Vol 118 (30) ◽  
pp. 16919-16926 ◽  
Author(s):  
Jan Philipp Kollender ◽  
Jacek Gasiorowski ◽  
Niyazi S. Sariciftci ◽  
Andrei I. Mardare ◽  
Achim Walter Hassel

2014 ◽  
Vol 1 (5) ◽  
pp. 903-908 ◽  
Author(s):  
Mu Fan ◽  
Kirill Sliozberg ◽  
Fabio La Mantia ◽  
Naoko Miyashita ◽  
Marcel Hagymási ◽  
...  

2014 ◽  
Vol 16 (8) ◽  
pp. 3739 ◽  
Author(s):  
Jacek Gasiorowski ◽  
Jan Philipp Kollender ◽  
Kurt Hingerl ◽  
Niyazi Serdar Sariciftci ◽  
Andrei Ionut Mardare ◽  
...  

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