phase transfer reaction
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2019 ◽  
Vol 15 ◽  
pp. 431-436 ◽  
Author(s):  
Arin Gucchait ◽  
Angana Ghosh ◽  
Anup Kumar Misra

A pentasaccharide repeating unit containing α-linked D-glucuronic acid, β-linked D-mannose, corresponding to the repeating unit of biofilms produced by Klebsiella pneumoniae, has been synthesized using a stereoselective [2 + 3] convergent glycosylation strategy. The β-D-mannosidic moiety has been synthesized using a D-mannose-derived thioglycoside by a two-step activation process. Late stage TEMPO-mediated oxidation of the pentasaccharide derivative using phase-transfer reaction conditions furnished the target compound in satisfactory yield.


Author(s):  
Geethy P. Gopalan ◽  
Ajith Nair Anil ◽  
Sushant Ghimire ◽  
Nidhin Joy ◽  
Ken-ichi Yuyama ◽  
...  

Synlett ◽  
2015 ◽  
Vol 26 (18) ◽  
pp. e6-e6 ◽  
Author(s):  
Kohji Seio ◽  
Mitsuo Sekine ◽  
Nobuhiro Tago ◽  
Yoshiaki Masaki ◽  
Hiroshi Nagasawa ◽  
...  

Synlett ◽  
2015 ◽  
Vol 26 (18) ◽  
pp. 2578-2582
Author(s):  
Kohji Seio ◽  
Mitsuo Sekine ◽  
Nobuhiro Tago ◽  
Yoshiaki Masaki ◽  
Hiroshi Nagasawa ◽  
...  

ChemInform ◽  
2015 ◽  
Vol 46 (33) ◽  
pp. no-no
Author(s):  
Sean P. Bew ◽  
G. Richard Stephenson ◽  
Jacques Rouden ◽  
Polly-Anna Ashford ◽  
Manuel Bourane ◽  
...  

2015 ◽  
Vol 357 (6) ◽  
pp. 1245-1257 ◽  
Author(s):  
Sean P. Bew ◽  
G. Richard Stephenson ◽  
Jacques Rouden ◽  
Polly-Anna Ashford ◽  
Manuel Bourane ◽  
...  

2014 ◽  
Vol 9 (6) ◽  
pp. 1586-1593 ◽  
Author(s):  
Seiji Shirakawa ◽  
Lijia Wang ◽  
Rongjun He ◽  
Satoru Arimitsu ◽  
Keiji Maruoka

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