Study of Nb Solubility in Hot Charging Process

The aim of this work is to investigate the dissolution behavior of Nb in hot charging hot rolling configurations. To do so, an indirect experimental procedure is used to quantify the amount of Nb present in solution before rolling. The method is based on the effect of dissolved Nb on static recrystallization kinetics due to its solute drag effect. After different thermal cycles, simulating cold and hot charging conditions, double hit torsion tests have been performed with a 0.23%C steel microalloyed with 0.03% Nb. By means of these tests, the static softening behavior has been determined. Comparison of the recrystallization times allows indirect evaluation of the amount of Nb in solid solution after each treatment. The results have been correlated with the precipitation state of the samples.

Study of static recrystallization behavior of austenite in a Ti–V microalloyed steel

The static recrystallization (SRX) behavior in Ti–V microalloyed steel was studied through two-pass compression tests using a Gleeble-3500 thermo-mechanical simulator. Under the experimental conditions with the deformation temperatures of 950–1050 °C, strain rates of 0.01–1 s–1, pass strains of 0.1–0.2 and inter-pass time of 1–100 s, respectively. The influence of various processing parameters on the static softening were discussed seriously and the results showed that the softening fractions raise quickly with the deformation temperature, the strain rate, the pass strain and the inter-pass time; Oppositely, it is reduced as the initial austenite grain size raises. In addition, the kinetic equations have been adopted and the required parameters have been determined based on the experiments, the calculated results are consistent with the experimental results, indicating the SRX behavior and microstructural evolutions of Ti–V microalloyed steel could be estimated by the determined kinetics parameters.

Static Softening Behavior and Modified Kinetics of Al 2219 Alloy Based on a Double-Pass Hot Compression Test

In this paper, the static softening mechanism of a 2219 aluminum alloy was studied based on a double-pass isothermal compression test. For the experiment, different temperatures (623 K, 723 K, and 773 K), strain rates (0.1/s, 1/s, and 10/s), deformation ratios (20%, 30%, and 40%), and insulation periods (5 s, 30 s, and 60 s) were used. Based on the double-pass flow stress curves obtained from the experiment, the step rate expressed by the equivalent dynamic recrystallization fraction is dependent on the deformation parameters, which increases with the increase in strain rate and insulation time, while it decreases with the increase in temperature and strain. Based on the microstructure observed using electron backscattered diffraction (EBSD), the static softening mechanism of the Al 2219 alloy is mainly static recovery and incomplete static recrystallization. A new expression for the static recrystallization fraction is proposed using the reduction rate of the sub-grain boundary. The dependent rule on the deformation parameters is consistent with the step rate, but it is of physical significance. In addition, the modified static recrystallization kinetics established by the new SRX fraction method was proven to have a good modeling and prediction performance under given deformation conditions.

Static Softening Behavior of Low Carbon High Niobium Microalloyed Steel

The MMS-200 thermal simulation testing machine was used to study the static softening behavior of low carbon high niobium microalloyed steel. The effect of niobium to the static recrystallization softening behavior of the microalloy steel had been analyzed by establishing the kinetics model of static recrystallization and the micro-morphology of precipitates. The results indicated that: the static softening behavior of the tested steel significantly influenced by the deformation temperature and the interval pass time of the rolling processing. At relatively high deformation temperature and long interval pass time, the ratio of static softening was increased. Then the deformation temperature was lower to 950°C, and the static softening behavior of the test steel was ceased. But when the deformation temperature was higher than 1000°C, the static softening behavior of the test steel completely occurred. The activation energy of the test steel was 325·mol-1 by the established model calculated.

Static Recrystallization Behavior of Non-Quenched and Tempered Steel 38MnSiVS

Refinement and uniform austenite grains are essential to obtain excellent and homogenous properties for non-quenched and tempered steel, which is mainly affected by static recrystallization of the rolling process. Using the Gleeble-3500 thermal simulation test machine, 20% compression test was carried out for two passes at 850~1050 °C (interval of 50 °C) and different pass interval time conditions to study the static softening and recrystallization behavior of 38MnSiVS non-quenched and tempered steel during deformation process. The effects of strain rate, deformation temperature and interval time on static softening rate and austenite recrystallization fraction were analyzed. The results showed that the increase of deformation temperature and the increase of pass interval time had more significant impact on the static recrystallization volume fraction of 38MnSiVS steel, while the influence of strain rate was relatively smaller. When the deformation temperature was 950 °C or higher, the non-conditioning steel 38MnSiVS could undergo complete recrystallization, and partial recrystallization occurred in the temperature range of 850-950 °C. A static recrystallization volume fraction model of non-regulatory steel 38MnSiVS was established. The static recrystallization activation energy was 296.7 kJ·mol-1, and the static recrystallization volume fraction model had a relative error of 2%.