The accumulation model of organic matters for the Niutitang Formation shale and its control on the pore structure: a case study from Northern Guizhou

Shale gas reservoir is a fine-grained sedimentary rock with component of clastic particles and organic matters, and the accumulation of the organic matters would determine the effective development of shale gas. The paleoclimate, detrital influx, redox of the water and paleoproductivity are effective geochemical indicators that could help to find the favorable shale gas reservoir stratum. In this study, the shale samples collected from Niutitang Formation (Northern Guizhou, China) were launched the measurements of the content of major elements and trace elements, and the characteristics of geochemical indicators were analyzed, which can be used to discuss the accumulation model of organic matters. Besides, the pore structure of shale sample controlled by the enrichment of organic matters is also discussed. The paleoclimate is dominant cold and dry, and it changes to warm and humid at the later Niutitang period, and the detrital influx also increased at the later Niutitang period; the water environment of Niutitang Formation shale presents as reductive, and the paleoproductivity of the Niutitang Formation shale is commonly high. The enrichment of organic matters in the Niutitang Formation is dominantly controlled by the redox of the water, while the hydrothermal activity and the paleoproductivity lead to the difference enrichment of organic matters in the Niutitang Formation shale. The accumulation model of organic matters also influences the characteristics of pore structure from the Niutitang Formation shale, and the pore structure could be divided into two types. The shale with high content of organic matters also features high content of quartz and pyrite, and these minerals contribute to the preservation of pore space in the shale, while that of the clay minerals is contrary. The high content of organic matters and preferable pore characteristics indicate the Niutitang Formation favors the development of shale gas, especially that for the lower Niutitang Formation.

Experimental and Numerical Simulation of Interlayer Propagation Path of Vertical Fractures in Shale

The complex fracture network formed by volume fracturing of shale gas reservoir is very important to the effect of reservoir reconstruction. The existence of bedding interface will change the propagation path of the hydraulic fracture in the vertical direction and affect the reservoir reconstruction range in the height direction. The three-point bending test is used to test and study the mechanical parameters and fracture propagation path of natural outcrop shale core. On this basis, a two-dimensional numerical model of hydraulic fracture interlayer propagation is established based on the cohesive element. Considering the fluid-solid coupling in the process of hydraulic fracturing, the vertical propagation path of hydraulic fracture under different reservoir properties and construction parameters is simulated. According to the results, the strength of the bedding interface is the weakest, the crack propagation resistance along the bedding interface is the smallest, and the crack propagation path is straight. When the crack does not propagate along the bedding interface, the fracture propagation resistance is large, and the fracture appears as an arc propagation path or deflection. The difference between vertical stress and minimum horizontal stress difference, interlayer stress difference and interface stiffness will have a significant impact on the propagation path of vertical fractures. Large injection rate and high viscosity fluid injection are helpful for vertical fractures to pass through the bedding interface, and low viscosity fracturing fluid is helpful to open the bedding interface. This research work is helpful to better understand the characteristics of bedding shale and the interlayer propagation law of vertical fractures, and to form the stimulation strategy of shale gas reservoir.

Numerical Simulation of Gas-Water Two-Phase Flow in Deep Shale Gas Reservoir Development Based on Mixed Fracture Modeling

In this paper, the development of a three-dimensional, two-phase fluid flow model (Modified Embedded Discrete Fracture Model) to study flow performances of a fractured horizontal well in deep-marine shale gas is presented. Deep-marine shale gas resources account for nearly 80% in China, which is the decisive resource basis for large-scale shale gas production. The dynamic characteristics of deep shale gas reservoirs are quite different and more complex. This paper uses the embedded discrete fracture model to simulate artificial fractures (main fractures and secondary fractures) and the dual-media model to simulate the mixed fractured media of natural fractures and considers the flow characteristics of partitions (artificial fractures, natural fractures, and matrix). Gas desorption is considered in the matrix. Different degrees of stress sensitivity are considered for natural and artificial fractures. Aiming at accurately simulating the whole production history of horizontal well fracturing, especially the dynamic changes of postfracturing flowback, a postfracturing fluid initialization method based on fracturing construction parameters (fracturing fluid volume and pump stop pressure) is established. The flow of gas and water in the early stage after fracturing is simulated, and the regional phase permeability and capillary force curves are introduced to simulate the process of flowback and production of horizontal wells after fracturing. The influence of early fracture closure on the gas-water flow is characterized by stress sensitivity. A deep shale gas reservoir of Sinopec was selected for the case study. The simulation results show it necessary to consider the effects of fractures and stress sensitivity in the matrix when considering the dynamic change of production during the flowback and production stages. The findings of this study can help for better understanding of the fracture distribution characteristics of shale gas, shale gas production principle, and well EUR prediction, which provide a theoretical basis for the effective development of shale gas horizontal well groups.

Baseline surface- and groundwater monitoring prior to an onshore shale gas operation in the Vale of Pickering, UK

A comprehensive programme of baseline groundwater hydrochemical monitoring has been carried out in connection with the proposed hydraulic fracturing of a 2 to 3 km deep Bowland Shale gas reservoir in borehole KM8 at Kirby Misperton, North Yorkshire, UK. The monitoring infrastructure encompassed: five on-site boreholes with hydraulically open intervals ranging from shallow weathered cover to a c. 200 m deep Corallian limestone aquifer, six off-site wells (hydraulically open in superficial materials and/or Kimmeridge Clay) and four surface water monitoring stations. Groundwater chemistry was high stratified with depth, ranging from slightly acidic, fresh, very hard Ca-HCO3-SO4 waters in shallow weathered cover, to brackish, calcium-depleted, highly alkaline waters in the Corallian aquifer. Dissolved methane was detected in most boreholes, with 10 µg/L being typical of shallow boreholes and around 50 mg/L in the Corallian. Low ethane concentrations and isotopic evidence suggest that the methane was predominantly microbial in origin (carboxylate fermentation at shallow depth, natural methanogenic CO2 reduction at greater depth). Elevated dissolved ethane (20-30 µg/L) was found in one well of intermediate depth, suggesting admixture of a possible thermogenic component, although this could be derived directly from the Kimmeridge Clay penetrated by the well.

Development of Production-Forecasting Model Based on the Characteristics of Production Decline Analysis Using the Reservoir and Hydraulic Fracture Parameters in Montney Shale Gas Reservoir, Canada

This study developed a production-forecasting model to replace the numerical simulation and the decline curve analysis using reservoir and hydraulic fracture data in Montney shale gas reservoir, Canada. A shale-gas production curve can be generated if some of the decline parameters such as a peak rate, a decline rate, and a decline exponent are properly estimated based on reservoir and hydraulic fracturing parameters. The production-forecasting model was developed to estimate five decline parameters of a modified hyperbolic decline by using significant reservoir and hydraulic fracture parameters which are derived through the simulation experiments designed by design of experiments and statistical analysis: (1) initial peak rate ( P hyp ), (2) hyperbolic decline rate ( D hyp ), (3) hyperbolic decline exponent ( b hyp ), (4) transition time ( T transition ), and (5) exponential decline rate ( D exp ). Total eight reservoir and hydraulic fracture parameters were selected as significant parameters on five decline parameters from the results of multivariate analysis of variance among 11 reservoir and hydraulic fracture parameters. The models based on the significant parameters had high predicted R 2 values on the cumulative production. The validation results on the 1-, 5-, 10-, and 30-year cumulative production data obtained by the simulation showed a good agreement: R 2 > 0.89 . The developed production-forecasting model can be also applied for the history matching. The mean absolute percentage error on history matching was 5.28% and 6.23% for the forecasting model and numerical simulator, respectively. Therefore, the results from this study can be applied to substitute numerical simulations for the shale reservoirs which have similar properties with the Montney shale gas reservoir.

Application of Heat Treatment to Prevent Fracturing Fluid-Induced Formation Damage and Enhance Matrix Permeability in Shale Gas Reservoirs

The low flowback efficiency of fracturing fluid would severely increase water saturation in a near-fracture formation and limit gas transport capacity in the matrix of a shale gas reservoir. Formation heat treatment (FHT) is a state-of-the-art technology to prevent water blocking induced by fracturing fluid retention and accelerate gas desorption and diffusion in the matrix. A comprehensive understanding of its formation damage removal mechanisms and determination of production improvement is conducive to enhancing shale gas recovery. In this research, the FHT simulation experiment was launched to investigate the effect of FHT on gas transport capacity, the multi-field coupling model was established to determine the effective depth of FHT, and the numerical simulation model of the shale reservoir was established to analyze the feasibility of FHT. Experimental results show that the shale permeability and porosity were rising overall during the FHT, the L-1 permeability increased by 30- 40 times, the L-2 permeability increased by more than 100 times. The Langmuir pressure increased by 1.68 times and the Langmuir volume decreased by 26%, which means the methane desorption efficiency increased. Results of the simulation demonstrate that the FHT process can practically improve the effect of hydraulic fracturing and significantly increase the well production capacity. The stimulation mechanisms of the FHT include thermal stress cracking, organic matter structure changing, and aqueous phase removal. Furthermore, the special characteristics of the supercritical water such as the strong oxidation, can not be ignored, due to the FHT can assist the retained hydraulic fracturing fluid to reach the critical temperature and pressure of water and transform to the supercritical state. The FHT can not only alleviate the formation damage induced by the fracturing fluid, but also make good use of the retained fracturing fluid to enhance the permeability of a shale gas reservoir, which is an innovative method to dramatically enhance gas transport capacity in shale matrix.