Effect of Plasticity on Creep Deformation in Type 316H Stainless Steel

The creep life and deformation behaviour of high-temperature steels can be significantly affected by the prior plastic loading. This effect is partly due to the generation of intergranular strains from the grain-scale elastic and plastic anisotropic deformation during plastic loading. This paper investigates the effect of these plasticity generated intergranular strains on the subsequent creep strain accumulation behavior in type 316H stainless steel. An in-situ synchrotron diffraction experiment was conducted at 550°C, where the sample was loaded incrementally to different magnitudes of plastic strain, followed by a displacement-controlled stress relaxation dwell at each of this stage. The lattice strains of 4 grain families were measured during these stages. It was found that the intergranular strains generated during the plastic deformation significantly affect the relative magnitude of creep strain accumulation in different grain families. A subtle but significant difference has been observed between the creep intergranular strain accumulation behavior and the plastic intergranular strain accumulation behavior in different grain families which can be used to interrogate the validity of any micromechanical models’ formulation for creep and plastic deformation. The macroscopic stress relaxations measured from the experiment were compared with the prediction from a novel crystal plasticity based micromechanical model developed in our group. A good overall match was found between the experiment and the model regarding the magnitude of stress relaxation after various level of plasticity. The experiments have demonstrated that the model requires further development to accurately predict the rate of stress relaxation and the micro scale lattice strain evolution during creep.

Intergranular Strains in Pre-Strained and Welded Pipes

Neutron diffraction has been used to investigate the weld residual stresses and the intergranular residual strains in butt-welded 316H pipes. Measurements have been made on pipes subjected to varying degrees of plastic pre-straining before welding, in order to assess the effects of plastic strain on the weld residual stresses and the intergranular strains in the material. The intergranular strains following plastic deformation will also be affected by the annealing effect of the welding. Pipes were initially prepared with plastic strain of 0, 10, 15, 20 and 25% plastic deformation. Thereafter, the pipes were cut in half and welded with a circumferential butt-weld. Bar specimens were extracted from the remote end of the 0, 10, 15, 20 and 25% pre-strained and welded pipes. Cross-weld bar specimens were also machined from the 0 and 20% pre-strained and welded pipes. Neutron diffraction measurements were made at ENGIN-X, ISIS and FRM-II, Munich. The aim of this paper is to evaluate the intergranular strains developed after pre-straining from measurements made in remote bar specimens from the remote-end of the pipes. The annealing effect of the welding cycle on the intergranular strains is also studied, with measurements done at several points on cross-weld bar specimens, obtaining the strain response of different hkl lattice planes. The results show that the {200} and {220} planes are at the extremes of response during loading. Furthermore, the welding thermal cycling relaxed the intergranular strains from the prior plastic deformation.