Design and use of a sapphire single-crystal gas-pressure cell for in situ neutron powder diffraction

A sapphire single-crystal gas-pressure cell without external support allowing unobstructed optical access by neutrons has been developed and optimized for elastic in situ neutron powder diffraction using hydrogen (deuterium) gas at the high-intensity two-axis diffractometer D20 at the Institut Laue-Langevin (Grenoble, France). Given a proper orientation of the single-crystal sample holder with respect to the detector, parasitic reflections from the sample holder can be avoided and the background can be kept low. Hydrogen (deuterium) gas pressures of up to 16.0 MPa at 298 K and 8.0 MPa at 655 K were tested successfully for a wall thickness of 3 mm. Heating was achieved by a two-sided laser heating system. The typical time resolution of in situ investigations of the reaction pathway of hydrogen (deuterium) uptake or release is on the order of 1 min. Detailed descriptions of all parts of the sapphire single-crystal gas-pressure cell are given, including materials information, technical drawings and instructions for use.

Study of nuclear properties with muonic atoms

Muons are a fascinating probe to study nuclear properties. Muonic atoms can easily be formed by stopping negative muons inside a material. The muon is subsequently captured by the nucleus and, due to its much higher mass compared to the electron, orbits the nucleus at very small distances. During this atomic capture process, the muon emits characteristic X-rays during its cascade down to the ground state. The energies of these X-rays reveal the muonic energy level scheme, from which properties like the nuclear charge radius or its quadrupole moment can be extracted. While almost all stable elements have been examined using muons, probing highly radioactive atoms has so far not been possible. The muX experiment has developed a technique based on transfer reaction inside a high-pressure hydrogen/deuterium gas cell to examine targets available only in microgram quantities.

Effect of the gas puff location on the divertor plasma properties in COMPASS tokamak

Langmuir probes are used to study the plasma parameters in the divertor during deuterium gas puff injection on the high- (HFS) or low-field sides (LFS). The probe data were processed to evaluate the plasma potential and the electron temperatures and densities. A difference was found in the plasma parameters depending on the gas puff location. In the case of a gas puff on the LFS, the plasma parameters changed vastly, mainly in the inner divertor – the plasma potential, the ion saturation-current density and the electron temperature dropped. After the gas puff, the electron temperature changed from 10-15 eV down to within the 5-9 eV range. As a result, the parallel heat-flux density decreased. At the same time, in the outer divertor the plasma parameters remained the same. We thus concluded that using a gas puff on the LFS will facilitate reaching a detachment regime by increasing the density of puffed neutrals. When the deuterium gas puff was on the HFS, the plasma parameters in the divertor region remained almost the same before and during the puff. The electron temperature decreased with just few eV as a result of the increased amount of gas in the vacuum chamber.