Effect of Deformation Structure of AISI 316L in Low-Temperature Vacuum Carburizing

The effect of plastic deformation applied to AISI 316L in low-temperature vacuum carburizing without surface activation was investigated. To create a difference in the deformation states of each specimen, solution and stress-relieving heat treatment were performed using plastically deformed AISI 316L, and the deformation structure and the carburized layer were observed with EBSD and OM. The change in lattice parameter was confirmed with XRD, and the natural oxide layers were analyzed through TEM and XPS. In this study, the carburized layer on the deformed AISI 316L was the thinnest and the dissolved carbon content of the layer was the lowest. The thickness and composition of the natural oxide layer on the surface were changed due to the deformed structure. The natural oxide layer on the deformed AISI 316L was the thickest, and the layer was formed with a bi-layer structure consisting of an upper Cr-rich layer and a lower Fe-rich layer. The thick and Cr-rich oxide layer was difficult to decompose due to the requirement for lower oxygen partial pressure. In conclusion, the oxide layer is the most influential factor, and its thickness and composition may determine carburizing efficiency in low-temperature vacuum carburizing without surface activation.

Temperature Dependence of Deformation Behaviors in High Manganese Austenitic Steel for Cryogenic Applications

The deformation structure and its contribution to strain hardening of a high manganese austenitic steel were investigated after tensile deformation at 298 K, 77 K and 4 K by means of electron backscatter diffraction and transmission electron microscopy, exhibiting a strong dependence of strain hardening and deformation structure on deformation temperature. It was demonstrated that sufficient twinning indeed provides a high and stable strain hardening capacity, leading to a simultaneous increase in strength and ductility at 77 K compared with the tensile deformation at 298 K. Moreover, although the SFE of the steel is ~34.4 mJ/m2 at 4 K, sufficient twinning was not observed, indicating that the mechanical twinning is hard to activate at 4 K. However, numerous planar dislocation arrays and microbands can be observed, and these substructures may be a reason for multi-peak strain hardening behaviors at 4 K. They can also provide certain strain hardening capacity, and a relatively high total elongation of ~48% can be obtained at 4 K. In addition, it was found that the yield strength (YS) and ultimate tensile strength (UTS) linearly increases with the lowering of the deformation temperature from 298 K to 4 K, and the increment in YS and UTS was estimated to be 2.13 and 2.43 MPa per 1 K reduction, respectively.

Formation of Heterogeneous Microstructure in AA1050/AA5052/AA6061/AA1050 Layered Sheet Processed by Cold Roll-Bonding and Subsequent Annealing

A cold roll-bonding process was applied to fabricate an AA1050/AA6061/AA5052/AA1050 four-layer clad sheet and subsequently annealed. Three types of aluminum alloy sheets such as AA1050, AA6061 and AA5052 with 2 mm thickness, 40 mm width and 300 mm length were stacked up each other after such surface treatment as degreasing and wire brushing, then reduced to a thickness of 2 mm by multi-pass cold rolling. The rolling was performed at ambient temperature without lubricant using a 2-high mill with a roll diameter of 400 mm at rolling speed of 6.0 m/sec. The roll bonded AA1050/AA6061/AA5052/AA1050 clad sheet was then annealed for 0.5 h at 200~400 °C. Microstructures of the as-roll bonded and subsequently annealed aluminum sheets are investigated by electron back scatter diffraction (EBSD) measurement. After rolling, the roll-bonded AA1050/AA5052/AA6061/AA1050 sheet showed a typical deformation structure that the grains are largely elongated to the rolling direction. However, after annealing, it exhibits a very heterogeneous structure consisting of both deformation structure and recrystallization structure containing nanometer order grains. The formation of this heterogeneous structure and texture with annealing is investigated in detail through EBSD analysis.

Self-toughened high entropy alloy with a body-centred cubic structure

Multi-scale deformation structure & evolution analysis of strong-yet-ductile interstitially hardened alloy, exhibiting a two-step phase transformation and concentration wave strengthening.

Are corestones due to weathering and/or tectonism? Problems and suggestions

Many of the so-called corestones have been developed from rocky blocks that have been apparently affected by subsurface physicochemical weathering that results in lamination, granulation, and eventually a puggy or stiff clay. The truth is that weathering takes advantage of a previous deformation structure and does not create it by weathering.

Experimental Study of Mesostructure Deformation Characteristics of Unsaturated Tailings with Different Moisture Content

A portion of the accumulated tailings in a tailings pond exhibits an unsaturated state. The mechanical properties of unsaturated tailings affect the safety and stability of tailings dams. To investigate the effect of moisture content on the deformation characteristics of unsaturated tailings in the mesoscale, a special testing apparatus is applied to experimentally study the settlement deformation and mesostructure evolution of unsaturated tailings under continuous load. The results show that the mesostructure deformation of unsaturated tailings with different moisture contents under load is the same and can be divided into four stages: pore compression, elastic deformation, structure change, and further compaction. However, the critical pressures of the four stages are significantly different; there is an optimal moisture content corresponding to the maximum deformation resistance. Moreover, the influence of the liquid bridge regime on the mesostructure deformation of unsaturated tailings is discussed in this paper.

A new type of slumping-induced soft-sediment deformation structure: the envelope structure

The sediments of the Cretaceous Gyeokpori Formation in south-western South Korea accumulated in a lake in which mainly siliciclastic rocks were deposited, with some interbedded volcaniclastics. The nearby volcanic activity resulted in unstable lake margins inducing a dominance of gravity-flow deposits. The high sedimentation rate facilitated soft-sediment deformation on the sloping margin. The deposition of numerous gravity-flow deposits resulted in a vertically heterolithic stratification. The slumps are composed of different lithologies, which is expressed in different types of deformation due to the difference in cohesion between sandy and mussy layers within the slumps. Coarser-grained (cohesionless) slumps tend to show more chaotic deformation of their lamination or layering. The difference in slumping behaviour of the cohesive and non-cohesive examples is explained and modelled. A unique soft-sediment deformation structure is recognized. This structure has not been described before, and we call it ‘envelope structure’. It consists of a conglomerate mass that has become entirely embedded in fine-grained sediment because slope failure took place and the fine-grained material slumped down with the conglomerate ‘at its back’. The cohesive laminated mudstone formed locally slump folds that embedded the non-cohesive overlying conglomerate unit, possibly partly due to the bulldozing effect of the latter. This structure presumably can develop when the density contrast with the underlying and overlying deposits is exceptionally high. The envelope structure should be regarded as a special – and rare – type of a slumping-induced deformation structure.