scholarly journals Accelerated solvent extraction of metabolites from marine fungi

2013 ◽  
Vol 7 (24) ◽  
pp. 3125-3134
Author(s):  
Liu Fen ◽  
Wang Qian ◽  
Xia Jinmei ◽  
Wang Hongtao ◽  
Xu Chen ◽  
...  
2013 ◽  
Vol 60 (1) ◽  
Author(s):  
Mohd Azizi Che Yunus ◽  
Manzurudin Hasan ◽  
Norasikin Othman ◽  
Siti Hamidah Mohd-Setapar ◽  
Liza Md.-Salleh ◽  
...  

Kajian ini bertujuan untuk mengkaji kesan saiz zarah ke atas pengekstrakan sebatian catechin daripada biji Areca catechu L. dengan menggunakan Pengekstrakan Pelarut Terpecut (PPT). Saiz zarah biji Areca catechu dipelbagaikan dari 75 μm sehingga 500 μm. Pengekstrakan telah dijalankan padaparameter tetap iaitu suhu (140oC), tekanan (1500 psi), masa (10 minit), isipadu semburan (60%) dan satu kitaran pengekstrakan, masing-masing. Hasil minyak peratusan yang lebih tinggi adalah 300 mg minyak / gram sampel (30.00% pati minyak) ditemui pada 125 μm. Walaubagaimanapun, kandungan catechin dalam pati minyak hanya 0.0375 mg catechin / gram sampel. Saiz zarah yang terbaik dalam julat uji kaji ini telah dikenal pasti pada 500 μm yang memberikan kandungan catechin yang tinggi iaitu 0.0515 mg catechin / gram sampel dari 247.5 mg minyak / gram sampel (24.75% pati minyak). Kata kunci: Saiz zarah; catechin; LC-MS-TOF; pengekstrakan pelarut terpecut The purpose of this work is to investigate the effects of particle size on the extraction of catechincompound from Areca catechu L. seeds by using Accelerated Solvent Extraction (ASE). The particle sizes of Areca catechu L. seeds are varied from 75 µm until 500 µm. The extraction is conducted at fixed parameters which are temperature (140oC), pressure (1500 psi), extraction time (10 minutes), flush volume (60%) and the static cycle is done for 1 extraction cycle respectively. Higher percentage oil yield of 300mg oil/gram of sample (30.00% oil yield) is found at 125 µm. However, the amount of catechin in oil yields is only 0.0375 mg of catechin/gram of sample. The best of particle size within the experimental range has been identified at 500 µm which gives a high content of catechin with 0.0515 mg Catechin/gram of sample from 247.5 mg oil/gram of sample (24.75% oil yield). Keywords: Particle size; catechin; LC-MS-TOF; accelerated solvent extraction


2002 ◽  
Vol 37 (2) ◽  
pp. 141-150 ◽  
Author(s):  
S. Tao ◽  
Y. H. Cui ◽  
J. Cao ◽  
F. L. Xu ◽  
R. Dawson ◽  
...  

2021 ◽  
pp. 101471
Author(s):  
Amanda Rajakaruna ◽  
Charles F. Manful ◽  
Ibrahim M. Abu-Reidah ◽  
Amber L. Critch ◽  
Natalia P. Vidal ◽  
...  

1998 ◽  
Vol 21 (4) ◽  
pp. 535-549 ◽  
Author(s):  
E. Björklund ◽  
M. Järemo ◽  
L. Mathiasson ◽  
L. Karlsson ◽  
J. T. Strode ◽  
...  

Author(s):  
Devanand Luthria ◽  
Dutt Vinjamoori ◽  
Kirk Noel ◽  
John Ezzell

2016 ◽  
Vol 12 (9) ◽  
pp. 4023-4044
Author(s):  
Karim Allaf ◽  
Khaoula Elaydi ◽  
Ibtisam Kamal ◽  
Ahmed Bedoui

The current work discusses the use of Instant Controlled Pressure Drop (DIC) as a pretreatment texturing stage intensifying phenolic compound extraction from South Tunisian Punicagranatum L. peels in both cases of conventional and Accelerated Solvent Extraction (ASE). Response Surface Methodology (RSM) allowed identifying the effects of DIC processing parameters on the yields of Total Phenol Compounds (TPC), Total Flavonoid (TF), Condensed Tannins (CT), and Hydrolysable Tannins (HT), and antioxidant capacities via 2, 2-diphenyl-1-picrylhydrazyl (DPPH) radical-scavenging capacity and ß-carotene-linoleic acid as responses. Comparative methods were used to evaluate DIC-textured and Raw samples. The results obtained confirmed that appropriate DIC-texturing improved both kinetic and yield of bioactive compound extraction using ASE from Punicagranatum L. peels. Extraction kinetics was studied through Coupled Washing-Diffusion CWD model. The effective diffusivity was identified and quantified ranged from 0.27 to 8.22 against 0.4710-10 m2s-1 for DIC textured and raw material (RM), respectively. DIC swelling enabled solid vegetal material matrix to expand and be more adapted to mass transfer thus increasing extractability of the phenol compounds. Scanning Electron Microscope SEM showed that DIC generated pores with an average diameter of 50 µm.


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