Technical Microscopy in the Rubber Industry

1943 ◽  
Vol 16 (1) ◽  
pp. 219-243 ◽  
Author(s):  
R. P. Allen

Abstract For supplying information not obtainable by the usual methods, the microscope is useful and often essential; not only will it disclose details which would otherwise be unseen, but by its unique methods of examination measurements of certain properties of materials can be readily secured which are not otherwise obtainable. When one considers the value of the microscope to the rubber industry specifically, the study of the size of particles is usually the first and frequently the only application which comes to mind, although other uses have been suggested and described. The present paper not only describes the importance of the microscope in determining particle size and shape, but also covers its applications in the solution of other problems which ordinarily are not considered to lie in the field of microscopy. [Chamot describes many interesting applications in different industries which indicate the unusual capabilities of microscopic methods.] In a well-organized industrial laboratory, the microscope is used to supplement and aid other methods for examination of raw materials, control of factory processing, correlation of physical properties with service performance, and solution of factory difficulties. The specific examples cited in this paper represent uses which have originated in connection with the manufacture of rubber goods, but they serve also to illustrate methods applicable to problems of the same type originating in other industries.

2014 ◽  
Vol 71 (2) ◽  
Author(s):  
Hussain, S. ◽  
M.K Abdul Hamid ◽  
A.R Mat Lazim ◽  
A.R. Abu Bakar

Brake wear particles resulting from friction between the brake pad and disc are common in brake system. In this work brake wear particles were analyzed based on the size and shape to investigate the effects of speed and load applied to the generation of brake wear particles. Scanning electron microscopy (SEM) with energy-dispersive X-ray spectroscopy (EDX) was used to identify the size, shape and element compositions of these particles. Two types of brake pads were studied which are non-asbestos organic and semi metallic brake pads. Results showed that the size and shape of the particles generatedvary significantly depending on the applied brake load, and less significantly on brake disc speed. The wear particle becomes bigger with increasing applied brake pressure. The wear particle size varies from 300 nm to 600 µm, and contained elements such as carbon, oxygen, magnesium, aluminum, sulfur and iron.


2017 ◽  
Vol 2017 ◽  
pp. 1-9 ◽  
Author(s):  
Zhaolin Lu ◽  
Xiaojuan Hu ◽  
Yao Lu

Particle morphology, including size and shape, is an important factor that significantly influences the physical and chemical properties of biomass material. Based on image processing technology, a method was developed to process sample images, measure particle dimensions, and analyse the particle size and shape distributions of knife-milled wheat straw, which had been preclassified into five nominal size groups using mechanical sieving approach. Considering the great variation of particle size from micrometer to millimeter, the powders greater than 250 μm were photographed by a flatbed scanner without zoom function, and the others were photographed using a scanning electron microscopy (SEM) with high-image resolution. Actual imaging tests confirmed the excellent effect of backscattered electron (BSE) imaging mode of SEM. Particle aggregation is an important factor that affects the recognition accuracy of the image processing method. In sample preparation, the singulated arrangement and ultrasonic dispersion methods were used to separate powders into particles that were larger and smaller than the nominal size of 250 μm. In addition, an image segmentation algorithm based on particle geometrical information was proposed to recognise the finer clustered powders. Experimental results demonstrated that the improved image processing method was suitable to analyse the particle size and shape distributions of ground biomass materials and solve the size inconsistencies in sieving analysis.


Author(s):  
A. Hizal ◽  
B. Sadasivam ◽  
D. Arola

A preliminary study was conducted to evaluate the parametric dependence of the residual stress distributions in bone that result from an abrasive air-jet surface treatment. Specifically, the influence of particle size and shape used in the treatment on the residual stress, propensity of embedding particles and material removal were studied. Rectangular beams of cortical bone were prepared from bovine femurs and treated with aluminum oxide and glass particles with different treatment angles. Residual stresses within the bone were quantified in terms of the radius of curvature of the bone specimens measured before and after the treatments, as well as a function of time to quantify decay in the stress. The sub-surface distribution was also examined using the layer removal technique. Results showed that the particle size and shape could be used to control the amount of material removal and the magnitude of residual stress within the treated surfaces. An increase in size of the glass particles resulted in an increase in the residual stress and a decrease in material removed during the treatment. The magnitude of residual stress ranged from 22 MPa to nearly 44 MPa through modulation of the particle qualities (size and shape). A microscopic examination of the treated surfaces suggests that the residual stresses resulted primarily from near-surface deformation.


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