Measuring the residual stress and stress-corrosion cracking susceptibility of additively manufactured 316L by ASTM G36-94

CORROSION ◽  
10.5006/3894 ◽  
2021 ◽  
Author(s):  
Erin Karasz ◽  
Jason Taylor ◽  
David Autenrieth ◽  
Phillip Reu ◽  
Kyle Johnson ◽  
...  
Keyword(s):  
Residual Stress ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Corrosion Cracking ◽  
Powder Bed ◽  
Heat Treated ◽  
Sample Height ◽  
Density Analysis ◽  
Saturated Boiling ◽  
The Relationship

Residual stress is a contributor to stress-corrosion cracking (SCC) and a common byproduct of additive manufacturing (AM). Here the relationship between residual stress and SCC susceptibility in laser powder bed fusion AM 316L stainless steel was studied through immersion in saturated boiling magnesium chloride per ASTM G36-94. The residual stress was varied by changing the sample height for the as-built condition and additionally by heat treatments at 600, 800, and 1200 °C to control, and in some cases reduce, residual stress. In general, all samples in the as-built condition showed susceptibility to SCC with the thinner, lower residual stress samples showing shallower cracks and crack propagation occurring perpendicular to melt tracks due to local residual stress fields. The heat-treated samples showed a reduction in residual stress for the 800 and 1200 °C samples. Both were free of cracks after >300 hours of immersion in MgCl2, while the 600 °C sample showed similar cracking to their as-built counterpart. Geometrically necessary dislocation (GND) density analysis indicates that the dislocation density may play a major role in the SCC susceptibility.

Stress corrosion cracking assessment of API X65 steel non-conventionally heat treated

2015 ◽  
Vol 67 (4) ◽  
pp. 352-360 ◽  
Author(s):  
C. Natividad ◽  
R. García ◽  
V. H. López ◽  
R. Galván-Martínez ◽  
M. Salazar ◽  
...  
Keyword(s):  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Corrosion Cracking ◽  
Heat Treated ◽  
Api X65 Steel ◽  
X65 Steel

NRC/EPRI Residual Stress Validation Program Phase I: Experimental Specimen Modeling and Measurement

2011 ◽  
Author(s):  
J. Broussard ◽  
P. Crooker
Keyword(s):  
Residual Stress ◽  
Residual Stresses ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Phase 1 ◽  
Measurement Techniques ◽  
Corrosion Cracking ◽  
Welding Residual Stress ◽  
Hole Drilling ◽  
Pressurized Water

The US Nuclear Regulatory Commission (NRC) and the Electric Power Research Institute (EPRI) are working cooperatively under a memorandum of understanding to validate welding residual stress predictions in pressurized water reactor primary cooling loop components containing dissimilar metal welds. These stresses are of interest as DM welds in pressurized water reactors are susceptible to primary water stress corrosion cracking (PWSCC) and tensile weld residual stresses are one of the primary drivers of this stress corrosion cracking mechanism. The NRC/EPRI weld residual stress (WRS) program currently consists of four phases, with each phase increasing in complexity from lab size specimens to component mock-ups and ex-plant material. This paper describes the Phase 1 program, which comprised an initial period of learning and research for both FEA methods and measurement techniques using simple welded specimens. The Phase 1 specimens include a number of plate and cylinder geometries, each designed to provide a controlled configuration for maximum repeatability of measurements and modeling. A spectrum of surface and through-wall residual stress measurement techniques have been explored using the Phase 1 specimens, including incremental hole drilling, ring-core, and x-ray diffraction for surface stresses and neutron diffraction, deep-hole drilling, and contour method for through-wall stresses. The measured residual stresses are compared to the predicted stress results from a number of researchers employing a variety of modeling techniques. Comparisons between the various measurement techniques and among the modeling results have allowed for greater insight into the impact of various parameters on predicted versus measured residual stress. This paper will also discuss the technical challenges and lessons learned as part of the DM weld materials residual stress measurements.

Effects of Cold Working and Heat Treatment on Caustic Stress Corrosion Cracking of Alloy 800M

2005 ◽  
Vol 297-300 ◽  
pp. 993-998 ◽  
Author(s):  
Chun Bo Huang ◽  
Guang Fu Li ◽  
Zhan Peng Lu ◽  
Jian Min Zeng ◽  
Wu Yang
Keyword(s):  
Heat Treatment ◽  
Residual Stress ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Cold Working ◽  
Corrosion Cracking ◽  
Caustic Solution ◽  
Surface Films ◽  
Microstructure Examination ◽  
Increasing Temperature

The effects of cold working and heat treatment on caustic stress corrosion cracking (SCC) of mill annealed (MA) alloy 800M in boiling solution of 50%NaOH+0.3%SiO2+0.3%Na2S2O3 were investigated by means of microstructure examination, tensile test, X-ray stress analysis, SCC testing of C-rings, Auger electron spectroscopy (AES), scanning electron microscopy (SEM) and metallography. The microstructure of alloy 800M under tested conditions was austenite. With a train of 25% by cold working, the grains of alloy 800M became longer, yield strength (YS) and ultimate tensile strength (UTS) increased, elongation (δ ) decreased, residual stress and the susceptibility to SCC increased. With increasing temperature of heat treatment of alloy 800M with cold working, the grains became bigger , residual stress, YS and UTS decreased and δ increased, the susceptibility to SCC of alloy 800M decreased. In boiling caustic solution, SCC cracks on the surfaces of C-ring specimens polarized potentiostatically at –20mV/SCE initiated from pitting and propagated along grain boundaries. AES analysis indicated that the surface films on MA alloy 800M were enriched in nickel and depleted in iron and chromium.

Effect of Ultrasonic Impact Treatment on the Stress Corrosion Cracking of 304 Stainless Steel Welded Joints

2008 ◽  
Author(s):  
Gang Ma ◽  
Xiang Ling
Keyword(s):  
Residual Stress ◽  
Finite Element ◽  
Stainless Steel ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Welded Joints ◽  
Corrosion Cracking ◽  
Coarse Grained ◽  
304 Stainless Steel ◽  
Ultrasonic Impact Treatment

High tensile weld residual stress is an important factor contributing to stress corrosion cracking (SCC). Ultrasonic impact treatment (UIT) can produce compressive stresses on the surface of welded joints that negate the tensile stresses to enhance the SCC resistance of welded joints. In the present work, X-ray diffraction method was used to obtain the distribution of residual stress induced by UIT. The results showed that UIT could cause a large compressive residual stress up to 325.9MPa on the surface of the material. A 3D finite element model was established to simulate the UIT process by using a finite element software ABAQUS. The residual stress distribution of the AISI 304 stainless steel induced by UIT was predicted by finite element analysis. In order to demonstrate the improvement of the SCC resistance of the welded joints, the specimens were immersed in boiling 42% magnesium chloride solution during SCC testing, and untreated specimen cracked after immersion for 23 hours. In contrast, treated specimens with different coverage were tested for 1000 hours without visible stress corrosion cracks. The microstructure observation results revealed that a hardened layer was formed on the surface and the initial coarse-grained structure in the surface was refined into ultrafine grains. The above results indicate that UIT is an effective approach for protecting weldments against SCC.

Relationship Between Acid Intergranular Corrosion and Caustic Stress Corrosion Cracking of Alloy 600

CORROSION ◽  
1977 ◽  
Vol 33 (1) ◽  
pp. 20-26 ◽  
Author(s):  
G. J. THEUS
Keyword(s):  
Heat Treatment ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Corrosion Cracking ◽  
Alloy 600 ◽  
Intergranular Attack ◽  
Electrochemical Tests ◽  
Stress Relieving ◽  
Service Conditions ◽  
The Relationship

Abstract Modified Streicher and 288 C (550 F) electrochemical caustic stress corrosion tests were performed on Alloy 600 to determine the relationship between acid intergranular attack susceptibility and caustic stress corrosion cracking (SCC) susceptibility. Mill annealed and solution annealed materials with and without a subsequent 621 C (1150 F) heat treatment (simulated stress relief) were evaluated. Susceptibility to attack in the Streicher test was greatest for material that had received a 621 C (1150 F) heat treatment, whereas this heat treatment caused the same material to be least susceptible to cracking in the electrochemical tests. The conclusions drawn from these results are: (1) stress relieving Alloy 600 does improve its resistance to caustic SCC, and (2) resistance of Alloy 600 to acid intergranular attack does not imply resistance of Alloy 600 to caustic SCC. Therefore, the results demonstrate the need for selecting corrosion qualification tests which are relevant to service conditions.

X-Ray Fractography of Stress Corrosion Cracking in Aisi 4340 Steel Under Controlled Electrode potential

1987 ◽  
Vol 31 ◽  
pp. 269-276 ◽  
Author(s):  
Masaaki Tsuda ◽  
Yukio Hirose ◽  
Zenjiro Yajima ◽  
Keisuke Tanaka
Keyword(s):  
Residual Stress ◽  
Fracture Surface ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Electrode Potential ◽  
Diffraction Method ◽  
Corrosion Cracking ◽  
Fracture Mechanisms ◽  
X Ray ◽  
Electrode Potentials

The residual stress left on the fracture surface is one of the important parameters in X-ray fractography and has been used to analyze fracture mechanisms in fracture toughness and fatigue tests especially of high strength steels.In the present paper, the distribution of residual stress beneath the fracture surface made by stress corrosion cracking was measured by the X-ray diffraction method. Stress corrosion cracking tests were conducted by using compact tension specimens of 200°C tempered AISI steel in 3.5% NaCl solution environment under various electrode potentials. The effect of electrode potential on the growth kinetics of stress corrosion cracking is discussed on the basis of residual stress distribution.

A Development of the Technical Basis for the New Code Case “Mitigation of PWSCC and CISCC in ASME Section III Components by the Advanced Surface Stress Improvement Technology”

2019 ◽  
Author(s):  
S. W. Cho ◽  
W. G. Yi ◽  
N. Mohr ◽  
A. Amanov ◽  
C. Stover ◽  
...  
Keyword(s):  
Residual Stress ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Surface Stress ◽  
Compressive Residual Stress ◽  
Corrosion Cracking ◽  
Chloride Salt ◽  
Spent Fuel ◽  
Term Operation ◽  
Technical Basis

Abstract It is necessary for nuclear power plant operation and spent fuel canisters to provide a sound technical basis for the safety and security of long-term operation and storage respectively. A new code case for mitigation of Primary Water Stress Corrosion Cracking (PWSCC) and Chloride Induced Stress Corrosion Cracking (CISCC) in Section III components by using an advanced surface stress improvement technology (ASSIT) is being developed by Task Group ASSIT which is one of the task groups under the ASME (The American Society of Mechanical Engineers). The necessary technical reports supporting this code case are being developed as part of joint research projects conducted by Doosan Heavy Industries and Construction (DOOSAN), Electric Power Research Institute (EPRI) and Sun Moon University (SMU). A well-known approach to prevent PWSCC and CISCC are to be performed using materials resistant to PWSCC and CISCC. The objective is to eliminate residual tensile stresses, or to induce compressive residual stress using ASSIT methods such as laser peening, water jet/cavitation peening, ultrasonic peening and ultrasonic nanocrystal surface modification (UNSM). Performance and measurement criteria for mitigation of PWSCC by ASSIT will be established based on the magnitude of surface stress and depth of compressive residual stress, sustainability, inspectability and lack of adverse effects. Additionally, for mitigation of CISCC by ASSIT, the evaluation of chloride induced corrosion pitting, the depth and density of corrosion pits and stress corrosion crack initiation and growth under chloride salt chemistry conditions are also being examined. This paper explains the approach, and progress of testing and analysis. The results and details from testing and analysis will be presented in a future PVP paper upon completion.

Failure Analysis of a Cracked Outlet Elbow in Coal Gasification Unit

2015 ◽  
Author(s):  
Wen Liu ◽  
Shanshan Shao ◽  
QiuPing Chen ◽  
Jin Shi ◽  
ZhiRong Yang ◽  
...  
Keyword(s):  
Residual Stress ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Coal Gasification ◽  
Stress Measurement ◽  
Corrosion Cracking ◽  
Chemical Components ◽  
Intergranular Stress Corrosion ◽  
Secondary Cracks ◽  
Strain Induced Martensite

A crack was observed on an outlet elbow of the pre-converter in coal gasification unit during operation. This paper details the investigation into the failure and highlights the most probable cause of failure based on available documents and experimental analysis. Visual examination, chemical components analysis, energy spectrum analysis, fracture analysis, metallurgical analysis, mechanical properties test and residual stress measurement were performed. The experimental results show that the primary crack initiated from inside and propagated to outer surface of the elbow. The content of titanium element was lower than the requirement in GB/T 14976-2002. Corrosion products were rich in O and S elements. Amounts of secondary cracks and strain induced martensite were observed. Furthermore, the residual stress on the inner surface near the crack tip was extremely high. According to the experiment results and the analysis of operating condition and history, the failure mechanism of the elbow is stress corrosion cracking. Sensitization of the stainless steel due to low Ti content and the faulty heat treatment contributed to the intergranular stress corrosion cracking.

Sign in / Sign up

Export Citation Format

Share Document