Evolution with Exposure Time of Copper Corrosion in a Concentrated Lithium Bromide Solution. Characterization of Corrosion Products by Energy-Dispersive X-Ray Analysis and X-Ray Diffraction

CORROSION ◽  
2006 ◽  
Vol 62 (1) ◽  
pp. 64-73 ◽  
Author(s):  
M. T. Montañés ◽  
V. Pérez-Herranz ◽  
J. García-Antón ◽  
J. L. Guiñón
Keyword(s):  
Exposure Time ◽  
Lithium Bromide ◽  
Corrosion Products ◽  
Energy Dispersive ◽  
Copper Corrosion ◽  
X Ray Diffraction ◽  
X Ray ◽  
Bromide Solution ◽  
Lithium Bromide Solution

Effect of Fluid Velocity and Exposure Time on Copper Corrosion in a Concentrated Lithium Bromide Solution

CORROSION ◽  
2001 ◽  
Vol 57 (10) ◽  
pp. 835-842 ◽  
Author(s):  
V. Pérez-Herranz ◽  
M. T. Montañés ◽  
J. García-Antón ◽  
J. L. Guiñón
Keyword(s):  
Exposure Time ◽  
Fluid Velocity ◽  
Lithium Bromide ◽  
Copper Corrosion ◽  
Bromide Solution ◽  
Lithium Bromide Solution

scholarly journals Karakterisasi Membran ZSM-5 yang Disintensis dengan Variasi Jenis dan Ukuran Kasa Penyangga

2020 ◽  
Vol 16 (1) ◽  
pp. 1
Author(s):  
Ana Hidayati Mukaromah ◽  
Tulus Ariyadi ◽  
Inas Hasna Azizah ◽  
Mifbakhuddin Mifbakhuddin
Keyword(s):  
Fourier Transform ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Energy Dispersive Spectroscopy ◽  
Energy Dispersive ◽  
X Ray Diffraction ◽  
X Ray ◽  
Aisi 316 ◽  
Scanning Electron

<p>Telah dilakukan sintesis dan karakterisasi membran ZSM-5 dengan penyangga kasa jenis 304 ukuran 200 dan 400 mesh dan jenis kasa AISI 316 ukuran 180 mesh. Tujuan penelitian ini adalah mensintesis membran ZSM-5 dengan penyangga kasa jenis 304 ukuran 200 dan 400 mesh dan jenis kasa AISI 316 ukuran 180 mesh dan mengkarakterisasi membran ZSM-5 hasil sintesis. Sintesis membran dilakukan dengan cara melapiskan prekursor ZSM-5 (<em>coating)</em> pada penyangga kasa yang telah diberi perlakuan dan dipanaskan pada suhu 90 °C selama 4 hari. Selanjutnya, membran yang dihasilkan dikarakterisasi engan metoda <em>X-ray diffraction</em> (XRD), <em>scanning electron microscope-energy dispersive spectroscopy</em> (SEM-EDS) dan <em>Fourier-transform infrared</em> (FTIR). Hasil citra SEM-EDS menunjukkan bahwa ukuran membran ZSM-5 yang semakin besar, menghasilkan jumlah lubang atau pori semakin banyak dengan luasan pori yang semakin kecil. Pola difraksi XRD menunjukkan bahwa membran yang dihasilkan mempunyai intensitas tertinggi pada 2 8º dan 23º yang merupakan karakteristik dari ZSM-5. Hasil spektra FTIR menunjukkan adanya serapan pada bilangan gelombang 450 cm<sup>-</sup><sup>1</sup>yang merupakan ciri khas membran ZSM-5.</p><p class="Text"><strong>Characterization of ZSM-5 Membranes Synthesized by Variation of Support Types and Sizes.</strong> Synthesis and characterization of ZSM-5 membrane were carried out with 304 type 200 and 400 mesh gauze supports and 180 mesh AISI 316 gauze types. The purpose of this study was to synthesize ZSM-5 membrane with 304 type 200 and 400 mesh gauze support and AISI 316 type 180 mesh size 180 mesh and characterize the synthesized ZSM-5 membrane. Membrane synthesis was carried out by coating the pre-treated gauze support with the ZSM-5 precursor and was heated at 90 °C for 4 days. Furthermore, the resulting membrane was characterized by X-ray diffraction (XRD), scanning electron microscope-energy dispersive spectroscopy (SEM-EDS) dan Fourier-transform infrared (FTIR). The SEM-EDX analysis shows that the increasing of ZSM-5 membrane size allowed pores number to increase with smaller pore surface area. The X-ray Diffraction pattern (XRD) shows that the resulting membrane has the highest intensity at 2  of 8º and 23º as the characteristics of ZSM-5. The FTIR spectra results show absorption at wavenumbers 450 cm<sup>-1</sup> which is a characteristic of ZSM-5 membranes.</p>

scholarly journals Synthesis and Characterization of a New Aluminum-Doped Bismuth Subcarbonate

Crystals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 466
Author(s):  
Loisangela Álvarez ◽  
Blanca Rojas de Gascue ◽  
Rolando J. Tremont ◽  
Edgar Márquez ◽  
Euclides J. Velazco
Keyword(s):  
Infrared Spectroscopy ◽  
Photoelectron Spectroscopy ◽  
Energy Dispersive ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
Characterization Methods ◽  
X Ray ◽  
Fourier Transformed Infrared Spectroscopy ◽  
Anionic Part

A new compound, Bi2O2CO3:Al, was synthesized by the coprecipitation method. The characterization was done by X-ray diffraction (XRD), Fourier transformed infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), electronic scanning microscopy (SEM), and energy dispersive X-ray spectroscopy (EDX). The characterization methods allowed to identify the Bi2O2CO3:Al compound, such as the Al-doped Bi2O2CO3 by XRD, the anionic part (CO32−) by FTIR, and the presence of aluminum in the compound by XPS and EDX. It was confirmed to have a nanostructure like a nanosheet and a microstructure that resembles a type sponge by SEM.

scholarly journals Identification of corrosion products on iron artefact from Bratislava castle

2021 ◽  
Vol 14 (1) ◽  
pp. 1-6
Author(s):  
Roman Košťúr ◽  
Matilda Zemanová
Keyword(s):  
Raman Spectroscopy ◽  
Corrosion Products ◽  
Energy Dispersive ◽  
X Ray Diffraction ◽  
X Ray ◽  
Atmospheric Exposure

Abstract Corrosion layers of an iron artefact were characterized to study long-term exposition of iron in Slovakia. The iron artefact from Bratislava castle has been coated with a strong layer of corrosion products and masonry residues. Corrosion products were characterized by different methods including energy-dispersive X-ray spectroscopy (EDX), X-Ray diffraction (XRD), and µ-Raman Spectroscopy. Magnetite and goethite on the surface are confirmed typical corrosion products from long-term atmospheric exposure in environment with corrosivity category C-2 (low).

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