scholarly journals Study on Microstructure and Mechanical Properties of Al7068 Reinforced with Silicon Carbide and Fly Ash by Powder Metallurgy

Author(s):  
Md Mehtab Alam and B.S Motgi

The paper deals with detailed study on microstructure and mechanical properties of aluminum 7068 reinforced with fly ash and silicon carbide by powder metallurgy, aluminum 7068, silicon carbide and fly ash were taken in powder form of required size and mixed together in varying proportion according to specification and compacted with pressure of 400MPa using hydraulic press to make samples and then samples were sintered at 600°c for 2 hours, the samples were tested for density, compressive strength, hardness and microstructure was analyzed using scanning electron microscope, energy dispersive x-ray study was carried out in order to confirm presence of silicon carbide and fly ash in aluminum matrix.

2017 ◽  
Vol 12 (1) ◽  
pp. 63-77 ◽  
Author(s):  
Siriporn Sirikingkaew ◽  
Nuta Supakata

This study presents the development of geopolymer bricks synthetized from industrial waste, including fly ash mixed with concrete residue containing aluminosilicate compound. The above two ingredients are mixed according to five ratios: 100:0, 95:5, 90:10, 85:15, and 80:20. The mixture's physico-mechanical properties, in terms of water absorption and the compressive strength of the geopolymer bricks, are investigated according to the TIS 168-2546 standard. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) analyses are used to investigate the microstructure and the elemental and phase composition of the brick specimens. The results indicate that the combination of fly ash and concrete residue represents a suitable approach to brick production, as required by the TIS 168–2546 standard.


2017 ◽  
Vol 79 (5-2) ◽  
Author(s):  
Mohd Shukor Salleh ◽  
Mohd Azizul Hikmi Safian ◽  
Mohamad Ridzuan Mohamad Kamal ◽  
Zolkarnain Marjom ◽  
Saifudin Hafiz Yahaya ◽  
...  

Thixoforming is a type of semisolid metal (SSM) processing for forming alloys in the semisolid state to near net-shaped products. In the present study, the effect of a thixoforming process on the microstructure and mechanical properties of Al-6Si-3Cu aluminium alloy was investigated. Melt was poured on a cooling slope at 630oC and the samples were obtained through permanent mold casting. They were thixoformed using a hydraulic press after holding at 571oC for 5min to yield a microstructure predominantly composed of α-Al globules and inter-globular Si particles. As-cast and thixoformed samples were characterized using optical microscopy, scanning electron microscopy (SEM), energy dispersive X-ray (EDX) and X-ray diffraction (XRD) as well as hardness measurements and tensile tests. The results indicate that the mechanical properties of thixoformed alloy have improved as compared to permanent mold cast alloy. The ultimate tensile strength of as-cast sample was 210 ± 3.5 MPa and increased to 241 ±3.1 MPa in the thixoformed sample while the yield strength of as-cast alloy was 140 ±4.5 MPa and increased to 176±3.3 MPa in the thixoformed sample. The thixoformed alloy also showed an improvement in elongation to fracture as it increased from 2% in as-cast sample to 3.2% in thixoformed alloy. The fracture of as-cast sample showed a cleavage fracture, whereas in the thixoformed alloy, a combination of dimple and cleavage was observed.


2012 ◽  
Vol 05 ◽  
pp. 551-558 ◽  
Author(s):  
A. RAHIMNEZHAD YAZDI ◽  
H.R. BAHARVANDI ◽  
H. ABDIZADEH ◽  
N. EHSANI

In this study Al 2 O 3- SiC nanocomposites have been fabricated by mixing of alumina and silicon carbide nano powders, followed by hot pressing at 1700°C. The mechanical properties and fracture mode of Al 2 O 3- SiC nanocomposites containing different volume fractions (5, 10 and 15%) of nano scale SiC particles were investigated and compared with those of alumina. Al 2 O 3- SiC powders were prepared by planetary milling in isopropanol. Fracture mode of specimens was investigated by means of scanning electron microscopy. Nanocomposites were tougher than alumina when they were hot pressed at the same temperature, and the values of nanocomposite's flexural strength and hardness were higher than those of alumina. Flexural strength, hardness and fracture toughness of the nanocomposites increase by increasing the volume percent of SiC up to 10% and then decrease slightly. The Scanning electron microscopy observations showed that fracture mode changes from intergranular for alumina to transgranular for nanocomposites. Finally X-ray diffraction analysis couldn't detect any chemical reactions between Al 2 O 3 and SiC particles.


2013 ◽  
Vol 281 ◽  
pp. 426-429
Author(s):  
Tao Chen ◽  
Hua Wu ◽  
Qing Hui Wang

PVD method is used to deposit (Ti,Al)N coatings on the surface of W6Mo5Cr4V2 steels. The value of bias voltage changes from -100V to -400V. X-ray diffraction (XRD), Scanning electron microscope(SEM) and UNMT-1 were employed to analysis the microstructure and mechanical properties of (Ti,Al)N coatings. The research results showed that the microstructure and mechanical properties of coatings became better when the value of bias voltage was -400V. The size and quantity of particles on coatings both decreased obviously. The adhesion between coatings and substrates increase to 54.6N. The hardness of (Ti,Al)N coatings rise to 39.7N.


2014 ◽  
Vol 988 ◽  
pp. 156-160
Author(s):  
Hong Wei Liu ◽  
Feng Wang ◽  
Bai Qing Xiong ◽  
Yong An Zhang ◽  
Zhi Hui Li ◽  
...  

The microstructure and mechanical properties of the Al-2.24Cu-1.42Mg-0.9Fe-0.9Ni alloy were studied using optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and tensile tests. The results indicate that the microstructures of the as cast alloy involve α-Al matrix, Al/Al2CuMg eutectic structure, Al7Cu2Fe, Al7Cu4Ni and Al9FeNi compounds. The tensile test results indicate that the alloy at elevated temperature (200°C) displays superior tensile strength due to the presence of the thermally stable Al7Cu2Fe, Al7Cu4Ni and Al9FeNi compounds.


2005 ◽  
Vol 494 ◽  
pp. 211-216 ◽  
Author(s):  
B. Dimčić ◽  
M. Vilotijević ◽  
D. Božić ◽  
D. Rajnović ◽  
M.T. Jovanović

The structural and compression mechanical properties of Ti3Al-based intermetallics produced by powder metallurgy techniques have been studied. The as-milled powders were compacted by hot pressing to non-porous homogenous compacts. Prior to compression tests, all compacts were homogenized by a solution treatment at 1050°C (a+β region) for 1h, followed by water quenching. The compression tests were performed from room temperature to 500°C in vacuum at a strain rate of 1 3 10 4 . 2 − − × s . Detailed microstructural characterization was evaluated by scanning electron microscopy (SEM), followed by energy dispersive spectroscopy (EDS) and X-ray diffraction analysis.


2016 ◽  
Vol 716 ◽  
pp. 464-471 ◽  
Author(s):  
Wojciech Skuza ◽  
Henryk Paul ◽  
Katarzyna Berent ◽  
Mariusz Prazmowski ◽  
Piotr Bobrowski

In this study, unalloyed titanium (Gr.1) and deoxidized high phosphorus copper plates were joined through explosive welding process. Different stand-off distances were used to investigate their influence on the microstructure and mechanical properties of the clad fabricated at the same amount of explosive charge. Microstructures near-the-interface were examined with the use of scanning electron microscope equipped with energy dispersive X-ray spectrometer and then microhardness measurements were carried out on the clad. Microstructure examinations showed that with increasing stand-off distance the length and amplitude of the waviness and the quantity of melted zones in areas near-the-interface increase. The inclusions of the melted zones are formed behind the wave crests on titanium side or within the wave vortex. Microhardness measurements indicate a significant increase of both plates microhardness, especially near-the-interface.


Author(s):  
Hansong Xue ◽  
Gang Yang ◽  
Di Li ◽  
Zhihui Xing ◽  
Fusheng Pan

AbstractThe effects of Y on microstructure and mechanical properties of as-cast AZ80–2Sn magnesium alloys were investigated by optical microscopy, scanning electron microscopy and X-ray diffraction. Y addition not only changes the as-cast microstructure but also influences the mechanical properties of AZ80–2Sn alloy. Unmodified AZ80–2Sn alloys under casting state show that Mg


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