scholarly journals Effects of C and N additions on primary MAX phase particles in intermetallic Ti-Al-Nb-Mo matrix in-situ composites prepared by vacuum induction melting

2020 ◽  
Vol 57 (03) ◽  
pp. 151-157 ◽  
Author(s):  
A. Klimová ◽  
J. Lapin
2007 ◽  
Vol 334-335 ◽  
pp. 297-300
Author(s):  
Si Young Sung ◽  
Bong Jae Choi ◽  
Young Jig Kim

The aim of this study is to evaluated the possibility of the in-situ synthesized (TiC+TiB) reinforced titanium matrix composites (TMCs) for the application of structural materials. In-situ synthesis and casting of TMCs were carried out in a vacuum induction melting furnace with Ti and B4C. The synthesized TMCs were characterized using scanning electron microscopy, an electron probe micro-analyzer and transmission electron microscopy, and evaluated through thermodynamic calculations. The spherical TiC plus needle-like and large, many-angled facet TiB reinforced TMCs can be synthesized with Ti and B4C by a melting route.


2006 ◽  
Vol 15-17 ◽  
pp. 231-235
Author(s):  
Bong Jae Choi ◽  
Si Young Sung ◽  
Young Jig Kim

The aim of this study is to fabricate an α-case free (TiB+TiC) hybrid titanium matrix composites (TMCs) shot sleeve for aluminum alloy diecasting by in-situ synthesis and investment casting. Granular 1.88 wt% B4C was added to a titanium matrix in a vacuum induction melting furnace. The synthesized (TiB+TiC) TMCs were examined using electron probe micro-analysis and transmission electron microscopy. The results of the in-situ synthesis and investment casting of the TMCs show that our casting route constitutes an effective approach to the economic net-shape forming of TMC sleeves.


Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1223 ◽  
Author(s):  
Frederic Brinkmann ◽  
Carolin Mazurek ◽  
Bernd Friedrich

Due to its enhancing properties in high-tech material applications, the rare earth element Scandium (Sc) is continuously gaining interest from researchers and material developers. The aim of this research is to establish an energy and resource efficient process scheme for an in situ extraction of Al-Sc master alloys, which offers usable products for the metallurgical industry. An AlSc20 alloy is targeted with an oxyfluoridic slag as a usable by-product. The thermochemical baseline is presented by modelling using the software tool FactSage; the experimental metal extraction is conducted in a vacuum induction furnace with various parameters, whereas kinetic aspects are investigated by thermogravimetric analysis. The Sc-containing products are analyzed by ICP-OES/IC concerning their chemical composition. Optimum parameters are derived from a statistical evaluation of the Sc content in the obtained slag phase. The material obtained was high in Ta due to the crucible material and remarkably low in Al and F; a comparison between the modelled and the obtained phases indicates kinetic effects inhibiting the accomplishment of equilibrium conditions. The formation of a Sc-rich Al-Sc phase (32.5 wt.-% Sc) is detected by SEM-EDS analysis of the metal phase. An in situ extraction of Al from Ca with subsequent metallothermic reduction of ScF 3 as a process controlling mechanism is presumed.


2021 ◽  
Vol 1016 ◽  
pp. 792-797
Author(s):  
Juraj Lapin ◽  
Kateryna Kamyshnykova

Samples of TiAl-based matrix in-situ composite with the chemical composition Ti-46.4Al-5.1Nb-1C-0.2B (at.%) reinforced with a low volume fraction of primary Ti2AlC particles were prepared by vacuum induction melting in graphite crucibles and centrifugal casting into graphite moulds. The hot isostatic pressing (HIP) of the as-cast samples and subsequent heat treatments leads to the formation of equiaxed grains with fully lamellar α2(Ti3Al) + γ (TiAl) microstructure and uniformly distributed Ti2AlC and TiB particles. The minimum creep rates of the in-situ composite are significantly lower compared to those measured for the counterpart low carbon benchmark alloy with the chemical composition Ti-47Al-5.2Nb-0.2C-0.2B (at.%) at temperatures ranging from 800 to 900 °C and applied stress of 200 MPa. The studied in-situ composite shows also significantly improved creep resistance compared to that of some TiAl-based alloys with fully lamellar, convoluted and pseudo-duplex microstructures at a temperature of 800 °C and applied stress of 200 MPa.


Author(s):  
June D. Kim

Iron-base alloys containing 8-11 wt.% Si, 4-8 wt.% Al, known as “Sendust” alloys, show excellent soft magnetic properties. These magnetic properties are strongly dependent on heat treatment conditions, especially on the quenching temperature following annealing. But little has been known about the microstructure and the Fe-Si-Al ternary phase diagram has not been established. In the present investigation, transmission electron microscopy (TEM) has been used to study the microstructure in a Sendust alloy as a function of temperature.An Fe-9.34 wt.% Si-5.34 wt.% Al (approximately Fe3Si0.6Al0.4) alloy was prepared by vacuum induction melting, and homogenized at 1,200°C for 5 hrs. Specimens were heat-treated in a vertical tube furnace in air, and the temperature was controlled to an accuracy of ±2°C. Thin foils for TEM observation were prepared by jet polishing using a mixture of perchloric acid 15% and acetic acid 85% at 10V and ∼13°C. Electron microscopy was performed using a Philips EM 301 microscope.


Alloy Digest ◽  
1987 ◽  
Vol 36 (1) ◽  

Abstract UDIMET 700 is a wrought nickel-base alloy produced by vacuum-induction melting and further refined by vacuum-arc remelting. It has excellent mechanical properties at high temperatures. Among its applications are blades for aircraft, marine and land-based gas turbines and rotor discs. This datasheet provides information on composition, physical properties, elasticity, and tensile properties as well as creep. It also includes information on high temperature performance and corrosion resistance as well as forming, heat treating, machining, joining, and surface treatment. Filing Code: Ni-51. Producer or source: Special Metals Corporation. Originally published March 1959, revised January 1987.


Alloy Digest ◽  
1991 ◽  
Vol 40 (7) ◽  

Abstract Allvac 718 is produced by vacuum induction melting followed by vacuum arc or electroslag consumable remelting. Th alloy has excellent strength and good ductility up to 1300 F (704 C). It also has excellent cryogenic properties. It has unique welding characteristics. This datasheet provides information on composition, physical properties, elasticity, and tensile properties. It also includes information on corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Ni-394. Producer or source: Allvac Inc..


Alloy Digest ◽  
1990 ◽  
Vol 39 (12) ◽  

Abstract NICKEL VAC N was originally developed as a container material for molten fluoride salts. It is a moderate strength, solid solution strengthened alloy with good oxidation resistance to 1800 F. It has excellent resistance to fluoride salts in the range 1300-1600 F. It is produced by vacuum induction melting followed electroslag remelting. This datasheet provides information on composition, physical properties, elasticity, and tensile properties as well as creep. It also includes information on high temperature performance and corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Ni-388. Producer or source: Teledyne Allvac.


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