DETERMINATION OF THE SEX-PHEROMONE COMPONENTS OF CHEIMOPHILA SALICELLA (LEPIDOPTERA: OECOPHORIDAE), A PEST OF BLUEBERRY IN BRITISH COLUMBIA

1984 ◽  
Vol 116 (10) ◽  
pp. 1397-1402 ◽  
Author(s):  
David R. Gillespie ◽  
G. G. S. King ◽  
Victor A. Salas-Reyes ◽  
Keith N. Slessor
Keyword(s):  
Liquid Chromatography ◽  
Sex Pheromone ◽  
Field Trapping ◽  
Gas Liquid Chromatography ◽  
Chemical Analyses ◽  
Individual Female ◽  
Tetradecyl Acetate ◽  
Pheromone Components ◽  
Tetradecenyl Acetate

AbstractThe female-produced sex pheromone Cheimophila salicella (Hbn.) was found to be a mixture of E-11-tetradecenyl acetate, E-11-tetradecen-1-ol, tetradecyl acetate and E-11-tetradecenal, as determined by chemical analyses and field-trapping results. Capillary gas-liquid chromatography of individual female tip washes indicated relative ratios of 100:15:10:2. Field-trapping experiments showed the E-11 acetate to be essential and the E-11 aldehyde to be a powerful synergist for trapping of male moths.

Sex Pheromone Components in the New Zealand Greenheaded Leafroller. Planotortrix excessana (Lepidoptera: Tortricidae)

1985 ◽  
Vol 40 (3-4) ◽  
pp. 266-271 ◽  
Author(s):  
R. A. Galbreath ◽  
M. H. Benn ◽  
H. Young ◽  
V. A. Holt
Keyword(s):  
New Zealand ◽  
Sex Pheromone ◽  
The Other ◽  
Tetradecyl Acetate ◽  
Sex Pheromone Components ◽  
Pheromone Components ◽  
Tetradecenyl Acetate ◽  
Planotortrix Excessana

Abstract Planotortrix excessana was found to include moths of two distinct pheromone-types which were not mutually attractive. Tetradecyl acetate and (Z)-8-tetradecenyl acetate were identified as pheromone components in one, and two other tetradecenyl acetates, probably (Z)-5-and (Z)-7-tetradecenyl acetate, in the other. By contrast with other pheromones reported from the tribe Archipini,⊿11-tetradecenyl compounds were not found in either pheromone-type.

GASCHROMATOGRAPHIC DETERMINATION OF STEROIDS IN THE URINE OF PATIENTS WITH CUSHING'S SYNDROME

1971 ◽  
Vol 67 (2) ◽  
pp. 303-315 ◽  
Author(s):  
A. J. Moolenaar ◽  
A. P. van Seters
Keyword(s):  
Liquid Chromatography ◽  
Cushing’S Syndrome ◽  
Normal Subjects ◽  
Diagnostic Value ◽  
Cushing's Syndrome ◽  
Gas Liquid Chromatography ◽  
Obese Subjects

ABSTRACT The 17-oxosteroids were estimated in the urine of 27 patients with Cushing's syndrome by gas-liquid chromatography (G. L. C.). The values of the various steroid fractions are compared with those of normal subjects, patients with thyrotoxicosis and obese subjects. The effect of the age of the patients on the diagnostic value of the invidual 17-oxosteroids and their ratios is discussed.

Simultaneous Determination of Lactulose and Mannitol in Urine of Burn Patients by Gas-Liquid Chromatography

1992 ◽  
Author(s):  
Ronald L. Shippee ◽  
Avery A. Johnson ◽  
William G. Cioffi ◽  
James Lasko ◽  
Thomas E. LeVoyer
Keyword(s):  
Liquid Chromatography ◽  
Simultaneous Determination ◽  
Gas Liquid Chromatography ◽  
Burn Patients

scholarly journals Gas Chromatographic Determination of Traces of Accelerants in Physical Evidence

1972 ◽  
Vol 55 (4) ◽  
pp. 840-845 ◽  
Author(s):  
Charles R Midkiff ◽  
Willard D Washington
Keyword(s):  
Liquid Chromatography ◽  
Solvent Extraction ◽  
Vapor Phase ◽  
Selection Criteria ◽  
Chromatographic Determination ◽  
Operating Parameters ◽  
Gas Liquid Chromatography ◽  
Internal Standards ◽  
Physical Evidence

Techniques developed for use with gas-liquid chromatography for the examination of evidence collected at the scene of suspected arson fires and firebombings are discussed. Both solvent extraction and vapor phase examinations are employed. Internal standards are used for the identification of specific components in actual samples to allow confirmation of hydrocarbon type, e.g., gasoline and kerosene. Operating parameters and solvent selection criteria are included. Results obtained from known materials and residual hydrocarbons in actual samples are compared.

Micro-Determination of p-Hydroxybenzoic Esters in Pharmaceuticals and Cosmetics

1977 ◽  
Vol 60 (1) ◽  
pp. 56-59 ◽  
Author(s):  
Emil Weisenberg ◽  
Baruch Gershon ◽  
Judith Schoenberg
Keyword(s):  
Liquid Chromatography ◽  
Phosphate Ester ◽  
Specific Method ◽  
Gas Liquid Chromatography ◽  
Direct Extraction ◽  
Flame Photometric Detector ◽  
Phenol Derivatives ◽  
Margin Of Error ◽  
Diethyl Phosphate

Abstract A rapid and specific method is described for the determination of microamounts of methyl, propyl, and butyl p-hydroxybenzoic esters (parabens) in pharmaceuticals and cosmetics. The method involves the direct extraction of parabens into benzene or chloroform followed by derivatization with phosphorochloridate. The diethyl phosphate ester derivatives are cleaned up on a Florisil minicolumn and finally measured by gas-liquid chromatography on 5% OV-210 on Gas-Chrom Q. A flame photometric detector or a KCl thermionic detector may be used. The concentration response was linear up to 40 ng parabens. The reproducibility and margin of error were tested with fortified samples. This method may be applied to the estimation of other phenol derivatives.

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