Dentistry. Analysis of fluoride concentration in aqueous solutions by use of fluoride ion-selective electrode

2018 ◽  
Keyword(s):  
Aqueous Solutions ◽  
Fluoride Concentration ◽  
Ion Selective Electrode ◽  
Fluoride Ion ◽  
Selective Electrode ◽  
Fluoride Ion Selective Electrode

Determination of inorganic fluoride in blood with a fluoride ion-selective electrode.

1987 ◽  
Vol 33 (2) ◽  
pp. 253-255 ◽  
Author(s):  
E Kissa
Keyword(s):  
Whole Blood ◽  
Fluoride Concentration ◽  
Ion Selective Electrode ◽  
Fluoride Ion ◽  
Inorganic Fluoride ◽  
Selective Electrode ◽  
Cell Potential ◽  
Novel Method ◽  
Fluoride Ion Selective Electrode

Abstract Inorganic fluoride in whole blood, serum, or plasma has been determined with a fluoride ion-selective electrode by adding the 0.5- to 2.0-mL sample to 20 mL of water containing a buffer and fluoride, 25 micrograms/L. The fluoride concentration in the sample is calculated from the resulting cell potential difference recorded after equilibrating for 10 min. This novel method has the advantages of simplicity, accuracy, and high precision, standard deviations for 5 to 7 replicate determinations of fluoride ranging from +/- 1.7 to +/- 2.4 micrograms/L. For whole blood from donors living in an area with fluorinated drinking water, the F- concentration was 20 to 60 micrograms/L.

scholarly journals simplified protocol to determine total fluoride concentration in NaF/ silica-based toothpastes

2020 ◽  
Vol 19 ◽  
pp. e201689
Author(s):  
Jenniffer Quiroz-Torres ◽  
Cinthia Pereira Machado Tabchoury ◽  
Carlos Liñán-Durán ◽  
Antonio Pedro Ricomini-Filho ◽  
Ailin Cabrera-Matta ◽  
...  
Keyword(s):  
Fluoride Concentration ◽  
T Test ◽  
Ion Selective Electrode ◽  
Fluoride Ion ◽  
Selective Electrode ◽  
Direct Technique ◽  
The Mean ◽  
Fluoride Salts ◽  
Fluoride Ion Selective Electrode

Aim: To determine total fluoride (TF) concentration in Na2FPO3/Ca-based toothpastes, using fluoride ion selective electrode (F-ISE) by the direct technique, it is necessary to use acid (Ac+) to hydrolyze the FPO3 2- ion and to dissolve insoluble fluoride salts bound to the abrasive. For NaF/silicabased toothpastes, the use of acid is not necessary (Ac-) and a simplified protocol could be followed. Methods: Thus, we evaluated TF concentration in seven brands of NaF/silicabased toothpastes, following the validated conventional Cury’s protocol (Ac+) or a simplification of this protocol (Ac-). Fluoride was analyzed with ISE calibrated with fluoride standard solutions prepared in the same conditions as the samples (Ac+ or Ac-). Results: The mean (±SD; n=21) of TF concentrations (μg F/g) found by Ac+ (971.3±191.2) and Ac- (982.4±201.3) protocols were not statistically different (t test, p=0.22). The TF concentrations found agree with those declared by the manufacturers, except for one toothpaste imported from China. Conclusion: The findings suggest that the determination of fluoride in NaF/silica-based toothpastes can be accurately made using a simplified protocol of analysis.

Chemically Soluble Fluoride in Na2FPO3/CaCO3-Based Toothpaste as an Indicator of Fluoride Bioavailability in Saliva during and after Toothbrushing

2020 ◽  
Vol 54 (2) ◽  
pp. 185-193
Author(s):  
Camila Siqueira Silva Coelho ◽  
Jaime Aparecido Cury ◽  
Cínthia Pereira Machado Tabchoury
Keyword(s):  
Fluoride Concentration ◽  
Area Under The Curve ◽  
Fluoride Ion ◽  
Selective Electrode ◽  
Fresh Sample ◽  
Group V ◽  
Group I ◽  
Adult Participants ◽  
The Relationship ◽  
Fluoride Ion Selective Electrode

The relationship between the concentration of chemically soluble fluoride found in toothpaste and that present in saliva, during and after brushing, was evaluated as an indicator of potentially bioavailable fluoride in toothpaste. Ten adult participants brushed their teeth with the assigned toothpastes: group I: fresh sample of a fluoride toothpaste: Na2FPO3/CaCO3, 1,378 µg F/g of total soluble fluoride (TSF); groups II–IV: aged samples of toothpaste presenting TSF concentrations of 1,160, 900, and 597 µg F/g, respectively; group V: non-F placebo toothpaste. The volunteers brushed their teeth for 1 min with 0.7 g of the toothpaste, all toothbrushing residues (TR) produced were collected, the mouth was rinsed with water, and saliva samples were collected up to 120 min. Total fluoride (TF) and TSF concentrations were determined in TR and in saliva samples using a fluoride ion-selective electrode. TSF concentration (µg F/mL) in TR was determined as an indicator of fluoride bioavailability during toothbrushing and the areas under curves of saliva fluoride concentration versus time (area under the curve, AUC = µg F/mL × min) were calculated as an indicator of fluoride bioavailability after toothbrushing. A significant correlation was found between the TSF concentrations in the toothpastes and the variables TR (r = 0.850; p = 0.0001) and AUC (r = 0.445; p = 0.004). For TF no significant correlation was found for TR (r = –0.099; p = 0.542) and AUC (r = –0.018; p = 0.912). The findings suggest that TSF concentration chemically found in Na2FPO3/CaCO3-based toothpaste could estimate how much fluoride would be bioavailable in saliva when the teeth are brushed.

Fluoride determination in various matrices relevant to nuclear industry: A review

2007 ◽  
Vol 95 (10) ◽  
Author(s):  
R. M. Sawant ◽  
M. A. Mahajan ◽  
Poonam Verma ◽  
Dipti Shah ◽  
U. K. Thakur ◽  
...  
Keyword(s):  
Nuclear Industry ◽  
Ion Selective Electrode ◽  
Nuclear Technology ◽  
Fluoride Ion ◽  
Selective Electrode ◽  
Experimental Parameters ◽  
Fluoride Determination ◽  
Reactor Materials ◽  
Fluoride Ion Selective Electrode

The determination of fluoride from diverse matrices at front and back end of nuclear technology and some studies from this laboratory on optimizations of different experimental parameters differing with multiple fuels and reactor materials, have been reviewed. The most useful techniques such as fluoride ion selective electrode (F-ISE) and ion-chromatography (IC) widely adopted as routine methods for fluoride determination in nuclear industry have been discussed. The effect of various buffer strengths on the response of the fluoride ion selective electrode has been examined. The ion chromatographic studies on mobile phase concentration, medium of sample, sample injection volume

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