Method for determination of bromine number of petroleum distillates and commercial aliphatic olefins by the electrometric method

1980 ◽  
Keyword(s):  
Electrometric Method ◽  
Petroleum Distillates ◽  
Bromine Number

scholarly journals STUDIES ON RDX AND RELATED COMPOUNDS: IX. DETERMINATION OF NITRIC ACID AND ACETIC ANHYDRIDE IN BACHMANN LIQUORS

1953 ◽  
Vol 31 (3) ◽  
pp. 201-203
Author(s):  
R. H. Betts ◽  
R. S. Stuart ◽  
C. A. Winkler
Keyword(s):  
Nitric Acid ◽  
Acetic Anhydride ◽  
Ammonium Nitrate ◽  
Routine Analysis ◽  
Calcium Hypochlorite ◽  
Electrometric Method ◽  
Direct Titration ◽  
Related Compounds ◽  
External Indicator

An electrometric method for determination of nitric acid in RDX(B) liquors has been developed. The method is not largely affected by ammonium nitrate and acetic anhydride. A precision of ± 0.5% may be readily obtained. Acetic anhydride in RDX(B) liquors may be determined by direct titration with standard aniline–toluene solution at 0 °C., using calcium hypochlorite as an external indicator. In routine analysis, a precision of ± 2% may be obtained.

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