scholarly journals On Elastic Symmetry Identification for Polycrystalline Materials

Symmetry ◽  
2017 ◽  
Vol 9 (10) ◽  
pp. 240 ◽  
Author(s):  
Peter Trusov ◽  
Kirill Ostapovich
Keyword(s):  
Polycrystalline Materials ◽  
Elastic Symmetry

Observation of secondary slip systems in tungsten bicrystals

1984 ◽  
Vol 42 ◽  
pp. 478-479
Author(s):  
J. R. Fekete ◽  
R. Gibala
Keyword(s):  
Stress Field ◽  
Grain Boundaries ◽  
Deformation Behavior ◽  
Stress Axis ◽  
Polycrystalline Materials ◽  
Slip Systems ◽  
Metallic Materials ◽  
Twist Boundary ◽  
Secondary Slip ◽  
Plane Normal

The deformation behavior of metallic materials is modified by the presence of grain boundaries. When polycrystalline materials are deformed, additional stresses over and above those externally imposed on the material are induced. These stresses result from the constraint of the grain boundaries on the deformation of incompatible grains. This incompatibility can be elastic or plastic in nature. One of the mechanisms by which these stresses can be relieved is the activation of secondary slip systems. Secondary slip systems have been shown to relieve elastic and plastic compatibility stresses. The deformation of tungsten bicrystals is interesting, due to the elastic isotropy of the material, which implies that the entire compatibility stress field will exist due to plastic incompatibility. The work described here shows TEM observations of the activation of secondary slip in tungsten bicrystals with a [110] twist boundary oriented with the plane normal parallel to the stress axis.

The structure of amorphous and polycrystalline materials using energy-filtered RDF analysis

1992 ◽  
Vol 50 (2) ◽  
pp. 1190-1191
Author(s):  
David Cockayne ◽  
David McKenzie
Keyword(s):  
Electron Diffraction ◽  
Diffraction Pattern ◽  
Density Function ◽  
Electron Diffraction Pattern ◽  
Polycrystalline Materials ◽  
Nearest Neighbour ◽  
X Ray ◽  
Selected Area Electron Diffraction ◽  
Reduced Density ◽  
System F

The technique of Electron Reduced Density Function (RDF) analysis has ben developed into a rapid analytical tool for the analysis of small volumes of amorphous or polycrystalline materials. The energy filtered electron diffraction pattern is collected to high scattering angles (currendy to s = 2 sinθ/λ = 6.5 Å-1) by scanning the selected area electron diffraction pattern across the entrance aperture to a GATAN parallel energy loss spectrometer. The diffraction pattern is then converted to a reduced density function, G(r), using mathematical procedures equivalent to those used in X-ray and neutron diffraction studies.Nearest neighbour distances accurate to 0.01 Å are obtained routinely, and bond distortions of molecules can be determined from the ratio of first to second nearest neighbour distances. The accuracy of coordination number determinations from polycrystalline monatomic materials (eg Pt) is high (5%). In amorphous systems (eg carbon, silicon) it is reasonable (10%), but in multi-element systems there are a number of problems to be overcome; to reduce the diffraction pattern to G(r), the approximation must be made that for all elements i,j in the system, fj(s) = Kji fi,(s) where Kji is independent of s.

Morphology and atomic structure of segregated grain boundaries in Cu-Sb

1992 ◽  
Vol 50 (1) ◽  
pp. 254-255
Author(s):  
R. W. Fonda ◽  
D. E. Luzzi
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Intergranular Fracture ◽  
Atomic Structure ◽  
Copper Alloys ◽  
Polycrystalline Materials ◽  
Grain Boundary Embrittlement ◽  
Boundary Embrittlement

The properties of polycrystalline materials are strongly dependant upon the strength of internal boundaries. Segregation of solute to the grain boundaries can adversely affect this strength. In copper alloys, segregation of either bismuth or antimony to the grain boundary will embrittle the alloy by facilitating intergranular fracture. Very small quantities of bismuth in copper have long been known to cause severe grain boundary embrittlement of the alloy. The effect of antimony is much less pronounced and is observed primarily at lower temperatures. Even though moderate amounts of antimony are fully soluble in copper, concentrations down to 0.14% can cause grain boundary embrittlement.

Interface structures in polycrystalline ceramic materials

1986 ◽  
Vol 44 ◽  
pp. 468-471
Author(s):  
K. J. Morrissey
Keyword(s):  
Electron Microscopy ◽  
Analytical Electron Microscopy ◽  
Physical And Mechanical Properties ◽  
High Resolution Electron Microscopy ◽  
Ceramic Materials ◽  
Polycrystalline Materials ◽  
Transmission Electron ◽  
Resolution Electron ◽  
Interface Structures

Grain boundaries and interfaces play an important role in determining both physical and mechanical properties of polycrystalline materials. To understand how the structure of interfaces can be controlled to optimize properties, it is necessary to understand and be able to predict their crystal chemistry. Transmission electron microscopy (TEM), analytical electron microscopy (AEM,), and high resolution electron microscopy (HREM) are essential tools for the characterization of the different types of interfaces which exist in ceramic systems. The purpose of this paper is to illustrate some specific areas in which understanding interface structure is important. Interfaces in sintered bodies, materials produced through phase transformation and electronic packaging are discussed.

Electron diffraction studies of amorphous and polycrystalline thin films

1990 ◽  
Vol 48 (4) ◽  
pp. 118-119
Author(s):  
D J H Cockayne ◽  
D R McKenzie
Keyword(s):  
Thin Films ◽  
Electron Diffraction ◽  
Polycrystalline Materials ◽  
Good Resolution ◽  
Scattered Intensity ◽  
Radial Density ◽  
X Ray ◽  
Polycrystalline Thin Films ◽  
Nitrogen Ion ◽  
Diffraction Patterns

The study of amorphous and polycrystalline materials by obtaining radial density functions G(r) from X-ray or neutron diffraction patterns is a well-developed technique. We have developed a method for carrying out the same technique using electron diffraction in a standard TEM. It has the advantage that studies can be made of thin films, and on regions of specimen too small for X-ray and neutron studies. As well, it can be used to obtain nearest neighbour distances and coordination numbers from the same region of specimen from which HREM, EDS and EELS data is obtained.The reduction of the scattered intensity I(s) (s = 2sinθ/λ ) to the radial density function, G(r), assumes single and elastic scattering. For good resolution in r, data must be collected to high s. Previous work in this field includes pioneering experiments by Grigson and by Graczyk and Moss. In our work, the electron diffraction pattern from an amorphous or polycrystalline thin film is scanned across the entrance aperture to a PEELS fitted to a conventional TEM, using a ramp applied to the post specimen scan coils. The elastically scattered intensity I(s) is obtained by selecting the elastically scattered electrons with the PEELS, and collecting directly into the MCA. Figure 1 shows examples of I(s) collected from two thin ZrN films, one polycrystalline and one amorphous, prepared by evaporation while under nitrogen ion bombardment.

Ductility Limit Diagrams for Superplasticity and Forging of High Temperature Polycrystalline Materials

2020 ◽  
Author(s):  
Wei Zhang ◽  
Yanfei Gao ◽  
Zhili Feng ◽  
Xin Wang ◽  
Siyu Zhang ◽  
...  
Keyword(s):  
High Temperature ◽  
Polycrystalline Materials

Modeling the Role of the Buildup of Magnetic Charges in Low Anisotropy Polycrystalline Materials

2018 ◽  
Vol 54 (11) ◽  
pp. 1-5
Author(s):  
Hatem Elbidweihy ◽  
Anthony S. Arrott ◽  
Virgil Provenzano
Keyword(s):  
Polycrystalline Materials

scholarly journals Laser Floating Zone Growth: Overview, Singular Materials, Broad Applications, and Future Perspectives

Crystals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 38
Author(s):  
Francisco Rey-García ◽  
Rafael Ibáñez ◽  
Luis Alberto Angurel ◽  
Florinda M. Costa ◽  
Germán F. de la Fuente
Keyword(s):  
Equilibrium Phase ◽  
Polycrystalline Materials ◽  
Floating Zone ◽  
High Crystalline Quality ◽  
Experimental Parameters ◽  
Phase Selectivity ◽  
Oriented Polycrystalline ◽  
Laser Heated ◽  
Lfz Technique ◽  
Zone Growth

The Laser Floating Zone (LFZ) technique, also known as Laser-Heated Pedestal Growth (LHPG), has been developed throughout the last several decades as a simple, fast, and crucible-free method for growing high-crystalline-quality materials, particularly when compared to the more conventional Verneuil, Bridgman–Stockbarger, and Czochralski methods. Multiple worldwide efforts have, over the years, enabled the growth of highly oriented polycrystalline and single-crystal high-melting materials. This work attempted to critically review the most representative advancements in LFZ apparatus and experimental parameters that enable the growth of high-quality polycrystalline materials and single crystals, along with the most commonly produced materials and their relevant physical properties. Emphasis will be given to materials for photonics and optics, as well as for electrical applications, particularly superconducting and thermoelectric materials, and to the growth of metastable phases. Concomitantly, an analysis was carried out on how LFZ may contribute to further understanding equilibrium vs. non-equilibrium phase selectivity, as well as its potential to achieve or contribute to future developments in the growth of crystals for emerging applications.

scholarly journals Graph neural networks for an accurate and interpretable prediction of the properties of polycrystalline materials

2021 ◽  
Vol 7 (1) ◽  
Author(s):  
Minyi Dai ◽  
Mehmet F. Demirel ◽  
Yingyu Liang ◽  
Jia-Mian Hu
Keyword(s):  
Neural Network ◽  
Network Architecture ◽  
Polycrystalline Materials ◽  
Feed Forward Neural Network ◽  
Microscopic Interactions ◽  
Physical Interactions ◽  
Graph Neural Networks ◽  
Individual Grains ◽  
Physical Features ◽  
Machine Learning Models

AbstractVarious machine learning models have been used to predict the properties of polycrystalline materials, but none of them directly consider the physical interactions among neighboring grains despite such microscopic interactions critically determining macroscopic material properties. Here, we develop a graph neural network (GNN) model for obtaining an embedding of polycrystalline microstructure which incorporates not only the physical features of individual grains but also their interactions. The embedding is then linked to the target property using a feed-forward neural network. Using the magnetostriction of polycrystalline Tb0.3Dy0.7Fe2 alloys as an example, we show that a single GNN model with fixed network architecture and hyperparameters allows for a low prediction error of ~10% over a group of remarkably different microstructures as well as quantifying the importance of each feature in each grain of a microstructure to its magnetostriction. Such a microstructure-graph-based GNN model, therefore, enables an accurate and interpretable prediction of the properties of polycrystalline materials.

scholarly journals Frequency Response Evaluation of Guitar Bodies with Different Bracing Systems

Symmetry ◽  
2020 ◽  
Vol 12 (5) ◽  
pp. 795
Author(s):  
Mircea Mihălcică ◽  
Mariana D. Stanciu ◽  
Sorin Vlase
Keyword(s):  
Structural Features ◽  
Dynamic Force ◽  
Classical Guitar ◽  
Elastic Symmetry ◽  
Frequency Responses ◽  
Points Of View ◽  
Coupled Plates ◽  
Natural Composite ◽  
Theoretical Results ◽  
Symmetric Systems

Wood is a natural composite, having a porous structure, with a complex elastic symmetry specific to orthotropic solid, influenced by three mutually perpendicular planes of elastic symmetry. The classical guitar is obtained from different wooden species, each of them having their own elastic properties and, as a whole, forming a lignocellulosic composite structure. Generally, some constructive parts of the classical guitar body are based on symmetry, starting from the structural features of wooden plates, which are symmetrically cut, and some patterns of the stiffening bars. The other elements, such as the strings system, are not symmetric. This study aims to evaluate the frequency responses of the guitar body as a symmetrical mechanical system from constructive points of view. Because theoretical results (analytic and numeric) regarding the symmetrical systems cannot be applied to quasi-symmetric systems, the dynamic response was analyzed from experiments performed on four types of classical guitar body (without neck), different from each other by the pattern of stiffening bars placed inside of the top plate. The experiments were performed using a Brüel&Kjær mini-shaker to excite the structure, and the signal was captured with accelerometers. The symmetric behavior of coupled plates from the guitar body was noticed in the case of an applied dynamic force of 110 Hz and 440 Hz, but in the case of 146 Hz, 588 Hz, 720 Hz, quasi skew symmetrical modes were recorded.

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