scholarly journals Evaluating Polishability of Zirconia Impregnated PMMA Nanocomposite for Denture Base Application

Symmetry ◽  
2021 ◽  
Vol 13 (6) ◽  
pp. 976
Author(s):  
Saleh Zidan ◽  
Nikolaos Silikas ◽  
Julfikar Haider ◽  
Javad Jahantigh ◽  
Ahmed Alhareb ◽  
...  

Artificial biomaterials are being developed for use in denture base with symmetrical properties to restore the aesthetics and functionalities. The rough surface of denture base resin promotes the adhesion of microorganisms and plaque accumulation. This study aimed to explore the consequences of polishing times on the surface roughness of high-impact (HI) heat-polymerized PMMA denture base acrylic resin reinforced with zirconia nanoparticles (nanocomposite). Thirty specimens (25 ± 0.50 mm in diameter and 2 ± 0.10 mm thickness) were fabricated from HI PMMA by adding zirconia nanoparticles at different concentrations of (0 wt.%, 1.5 wt.%, 3 wt.%, 5 wt.%, 7 wt.%, and 10 wt.%). Specimens were divided into six groups (n = 5) and surface roughness (Ra) was measured before and after polishing with a standard protocol for one and two minutes. The addition of zirconia in PMMA at low concentrations (1.5 wt.%, 3 wt.%, and 5 wt.%) did not negatively affect the surface finish of the denture base composites following conventional polishing and remained below the clinically acceptable limit (0.2 µm). After one minute of polishing, only the 10 wt.% zirconia (0.17 ± 0.03 µm) demonstrated a substantial rise in median surface roughness, in comparison with the control group (0.11 ± 0.01 µm). It is concluded that the group containing 3 wt.% (0.10 ± 0.01 µm) of zirconia is the optimum concentration to obtain the best symmetrical surface finish after two minutes of polishing.

2021 ◽  
Vol 17 (1) ◽  
pp. 22-26
Author(s):  
Kadek Ayu Wirayuni ◽  
◽  
I Made Hendri Dwi Saputra ◽  

Introduction: The denture base is the part of the removable denture that is supported by good adaptation to the underlying oral tissue. Most of the denture bases are made of acrylic or polymethyl methacrylate resin, better known as PMMA. However, the acrylic resin also has disadvantages such as easily broken and absorbs liquids both water and chemicals. The chemical absorption like alcohol, ethanol, and some drinks that contain acidic materials will chemically be induced with acrylic resin and settle in the pores of the acrylic resin. The chemical damage or defect creates roughness on the surface of the acrylic resin which can cause cracking or crazing and a decrease in surface strength and hardness. Materials and Methods: The method used in this research was a laboratory experimental design with a post-test-only control group using 12 samples consisting of 2 different types of samples by measuring the surface roughness of the acrylic resin after immersing the sample with a predetermined time. Results and Discussions: One-way ANOVA test results showed a significant difference in surface roughness after the samples immersion with a value of p = 0.006 (p <0.05). Conclusions: Based on this research, can be concluded that there is an increase in the surface roughness of the heated polymerized acrylic resin for 3 hours and 4 hours of immersion. The longer the heated polymerized acrylic resin is soaked in arak hence the level of surface roughness increases.


2015 ◽  
Vol 9 (1) ◽  
pp. 402-408 ◽  
Author(s):  
A.A.R. Khaledi ◽  
M. Bahrani ◽  
S. Shirzadi

Statement of the Problem: Bonding failure between acrylic resin and soft liner material and also gradual loss of soft liner resiliency over time are two impending challenges frequently recognized with a denture base embraced with a resilient liner. Since patients drink various beverages, it is crucial to assess the influences of these beverages on physical characteristics of soft liners. Purpose: This in vitro study envisioned to assess the influence of food simulating agents (FSA) on the hardness of a silicone soft liner by employing a Shore A durometer test and also evaluate its bond strength to a denture base resin by using tensile bond strength test. Materials and Methods: To test the hardness of samples, 50 rectangular samples (40 mm × 10 mm × 3 mm) were prepared from a heat-polymerized polymethyl methacrylate (Meliodent). Mollosil, a commercially available silicone resilient liner, was provided and applied on the specimens following the manufacturer’s directions. In order to test tensile bond strength, 100 cylindrical specimens (30 mm × 10 mm) were fabricated. The liners were added between specimens with the thicknesses of 3 mm. The specimens were divided into 5 groups (n=10) and immersed in distilled water, heptane, citric acid, and 50% ethanol. For each test, we used 10 specimens as a baseline measurement; control group. All specimens were kept in dispersed containers at 37ºC for 12 days and all solutions were changed every day. The hardness was verified using a Shore A durometer and the tensile bond strength was examined by an Instron testing machine at a cross-head speed of 5 mm/min. The records were analyzed employing one-way ANOVA, Tukey’s HSD, and LSD tests. Results: The mean tensile bond strength ± standard deviation (SD) for Mollosil was as follows for each group: 3.1 ± 0.4 (water), 1.8 ± 0.4 (citric acid), 3.0 ± 0.4 (heptane), 1.2 ± 0.3 (50% ethanol), and 3.8 ± 0.4 (control). The hardness values for each group were: 28.7 ± 2.11 (water), 33.2 ± 2.82 (citric acid), 39.2 ± 4.8 (heptane), 32.3 ± 3.56 (50% ethanol) and 22.2 ± 2.08 (control). Mean values for hardness indicated that all of the food simulating agents significantly increased hardness of the Mollosil soft liner compared to the control group (p<0.05). The results of tensile bond strength depicted that water and FSA decreased the bond strength of the soft liner -denture base resin compared to the control group and it was statistically significant (p<0.05). Conclusion: The food simulating agents could influence the mechanical properties of silicone soft liners; hence, clinicians should inform their patients concerning their possible adverse effects and complications.


Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1067
Author(s):  
Salwa O. Bajunaid ◽  
Bashayer H. Baras ◽  
Abdulrahman A. Balhaddad ◽  
Michael D. Weir ◽  
Hockin H. K. Xu

Candida albicans (C. albicans) biofilm is a common etiological factor in denture stomatitis. The purpose of this study was to investigate the effects of incorporating 2-methacryloyloxyethyl phosphorylcholine (MPC) as a protein repellent into a new high-impact denture acrylic (HIPA) resin on the surface roughness, solution pH, and C. albicans biofilm adhesion to the denture base. The new acrylic denture resin base was formulated by mixing MPC into HIPA resin at mass fractions of 1.5%, 3%, and 4.5%. Surface roughness was measured using a Mitutoyo surface roughness tester. C. albicans biofilm growth and viability were assessed via colony forming unit counts. The pH of the biofilm growth medium was measured using a digital pH meter. Adding MPC to the HIPA resin at percentages of 1.5% and 3% increased the roughness values significantly (p < 0.05), while adding 4.5% MPC resulted in no difference in roughness values to that of the control group (p > 0.05). All experimental groups demonstrated neutral pH values (pH ≅ 7) and were not significantly different from each other (p > 0.05). Incorporating 2-methacryloyloxyethyl phosphorylcholine at 4.5% resulted in a significant (≅1 log) colony-forming unit reduction compared with the control group with 0% MPC (p < 0.05). A fungal-retarding denture acrylic resin was developed through the incorporation of MPC for its protein-repelling properties. This newly developed denture acrylic material has the potential to prevent oral microbial infections, such as denture stomatitis.


2016 ◽  
Vol 17 (4) ◽  
pp. 322-326 ◽  
Author(s):  
M Kalavathi ◽  
Mallikarjuna Ragher ◽  
G Vinayakumar ◽  
Sanketsopan Patil ◽  
Aishwarya Chatterjee ◽  
...  

ABSTRACT Objective The objective of this study was to evaluate and compare changes in the flexural strength of heat-cured denture base resins when treated using denture cleansers. Study design A total of 40 specimens with dimension 65 mm length, 10 mm width, and 3 mm thickness were prepared as per ISO 1567 specification. A total of 10 specimens were immersed in distilled water to be used as control. Of the remaining 30 samples, 10 were treated with Clinsodent, 10 with VI-Clean, and 10 with Clanden denture cleansers. Specimens in each group were subjected to three-point flexural load in universal testing machine at a cross-head speed of 5 mm/min. The peak load (N) was recorded and flexural strength was calculated. The findings were analyzed using Kruskal–Wallis analysis of variance and Mann–Whitney test. Results Heat-cured denture base resin selected for this study showed significant difference in flexural strength after immersion in denture cleansers Clinsodent, VI-Clean, and Clanden solutions, when compared with the control group. Conclusion Findings of this study showed that denture cleansers altered the flexural strength of heat polymerized acrylic resins that endured soaking cycles which simulated 180 days of use. Hence, denture cleansers should be used with caution, once a day after brushing the dentures. It is advisable for patients to follow the manufacturer's instructions. How to cite this article Ragher M, Vinayakumar G, Patil S, Chatterjee A, Mallikarjuna DM, Dandekeri S, Swetha V, Pradeep MR. Variations in Flexural Strength of Heat-polymerized Acrylic Resin after the Usage of Denture Cleansers. J Contemp Dent Pract 2016;17(4):322-326.


Materials ◽  
2020 ◽  
Vol 13 (17) ◽  
pp. 3732
Author(s):  
Saleh Zidan ◽  
Nikolaos Silikas ◽  
Julfikar Haider ◽  
Julian Yates

Exposure of denture base acrylic resins to the oral environment and storage media for extended periods of time results in sorption of saliva or water, leading to a reduction in physical properties and thus clinical service life. The purpose of this in vitro study was to assess the sorption and solubility of high-impact heat-polymerised denture base acrylic resin (HI PMMA) impregnated with zirconia nanoparticles after being stored for 180 days in distilled water (DW) and artificial saliva (AS). The specimens were divided into six groups for each storage medium, according to the concentration of zirconia nanoparticles (0, 1.5, 3.0, 5.0, 7.0, and 10.0 wt.%). Data were statistically analysed for sorption and solubility using one-way and two-way ANOVA statistical tests. Sorption in DW and AS for all groups containing zirconia showed sorption values lower than the control group at 90 days, though not significantly different (p > 0.05) compared to the control group. For both the DW and AS groups, the lowest solubility value was measured in the group containing 3 wt.% zirconia, however, there was no significant difference compared to the control group except when observing 10 wt.% zirconia in AS, which showed a significantly higher solubility (p < 0.05). High-impact PMMA, impregnated with low concentrations of ZrO2, showed the lowest sorption and solubility in both media, but was not significantly different compared to pure HI PMMA.


2018 ◽  
Vol 6 (2) ◽  
pp. 339
Author(s):  
Afthin Maritta Noviyanti ◽  
Rahardyan Parnaadji ◽  
FX Ady Soesetijo

The most used denture base materials is heat cured acrylic resin. The disadvantages of acrylic resin are easy to absorb water and porosity that can increase surface roughness. The surface roughness can facilitate the attachment of microorganisms and accumulation of plaque. The cleansing of mechanical denture use electric toothbrush and denture cleanser paste. This paste uses natural materials from robusta coffee beans that decrease surface roughness. To determine the effectivity of robusta coffee beans paste as a denture cleanser to the surface roughness of heat cured acrylic resin.  This study was an experimental laboratory with the research design the post test only  control group design. Total sample of 36 samples in size (65 x 10 x 2,5) mm which consisted of 4 groups: control group without brushing, group A  brushed with electric toothbrush and a placebo paste, group B brushed with electric toothbrush and robusta coffee beans paste 25%, and group C  brushed with electric toothbrush and robusta coffee beans paste 50%. Brushing was done for 22 minutes, then measured the surface roughness of dentures. Robusta coffee bean paste was less effective as a denture cleanser agent against the surface roughness of the heat cured acrylic resin. Robusta coffee beans paste 50% can be used as a denture cleanser. Keyword: acrylic resin, electric toothbrush, robusta coffee bean paste, surface roughness  


2018 ◽  
Vol 1 (1) ◽  
pp. 171-175
Author(s):  
Kholidina Imanda Harahap ◽  
Lasminda Syafiar ◽  
Sintiya Karolina Tarigan

To mantain digestive health, people usually consume yogurt that has acidity 4-5. Acidic solutions can cause the surface roughness of acrylic resin heat cured is used as denture base material. Denture with rough surfaces facilitate the attachment of plaque and bacteria that can degrade the cleanliness and health of the patient. The purpose of this study was to analyze the surface roughness of acrylic resin heat cured after being immersed in yogurt with different immersion time. Thirty acrylic resin heat cured specimens (12 mm in length, 12 mm in wide and 2 mm height) were prepared and divided into three experimental groups (n=10): I ( specimens immersed in yogurt for 60 minutes), II (specimens immersed in yogurt for 120 minutes) and III (specimens immersed in yogurt for 180 minutes). Surface roughness before and after immersion was measured using Profilometer. Data will be analyzed using T test (p<0,05). After immersion, the specimens showed significantly different on surface roughness (p=0,04). Among the experimental groups, immersion for 180 minutes showed the highest surface roughness value than 60 and 120 minutes. It can be concluded that yogurt can make surface roughness of acrylic resin heat cured. Increasing surface roughness depends on exposure time of yogurt on acrylic resin heat cured. To mantain a digestive health, people usually consume yogurt that has acidity of 4-5. Acidic solutions can cause the surface roughness of heat cured acrylic resin which is used as denture base material. Denture with rough surfaces facilitates the presence of plaque and bacteria that can degrade the cleanliness and health of the patient. The objective of this study was to analyze the surface roughness of heat cured acrylic resin after immersed in yogurt with different immersion time. Thirty heat cured acrylic resin specimens (12 mm in length, 12 mm in wide and 2 mm in height) were prepared and divided into three experimental groups (n=10): I ( specimens were immersed in yogurt for 60 minutes), II (specimens were immersed in yogurt for 120 minutes) and III (specimens were immersed in yogurt for 180 minutes). Surface roughness before and after immersion was measured using Profilometer. Data were analyzed using T test (p<0,05). After immersion, the specimens showed significantly different on surface roughness (p=0,04). Among the experimental groups, immersion for 180 minutes showed the highest surface roughness value than 60 and 120 minutes. It could be concluded that yogurt could make surface roughness of heat cured acrylic resin . Increasing surface roughness depended on exposure time of yogurt on heat cured acrylic resin.


2020 ◽  
Vol 5 (1) ◽  
pp. 36-43
Author(s):  
Gladis Aprilla Rizki ◽  
Sri Wahyuningsih Rais ◽  
Martha Mozartha

Alcoholic beverages can be consumed in any group age, and it may be consumed by an individual using denture. Fluid absorption by heat-cured acrylic resin as a material of a denture base was able to cause an increase in its surface roughness. Absorption of an organic solvent such as the ethanol in an alcoholic beverage(s) could even increase the effect. This study aimed to evaluate the effect of alcohol beverages on surface roughness of heat-cured acrylic resin denture base. Samples (n=24) were prepared from heat-cured acrylic resin (25x25x5 mm). They were divided into 4 groups and the pre-test surface roughness was measured. Samples of each group were immersed for 10 minutes into the solution (distilled water as the control group, beer, wine, and whiskey as the test groups). After stored in artificial saliva for 23 hours, the samples were immersed into the solution, completing a period of 24 hours. This procedure was performed for 7 consecutive days and the post-test surface roughness was measured. Data were statistically analyzed using the Kruskal-Walis test. There was a significant difference in surface roughness measurement before and after the immersion (p<0.05). Whiskey was most affecting the surface roughness of heat-cured acrylic resin denture base. Alcoholic beverages could increase the surface roughness of heat cure acrylic resin denture base. Keywords: Alcoholic beverages; Heat-cured acrylic denture base; Surface roughness


2016 ◽  
Vol 10 (1) ◽  
pp. 124-130
Author(s):  
Youssef S. Al Jabbari ◽  
Spiros Zinelis ◽  
Sara M. Al Taweel ◽  
William W. Nagy

Purpose The debonding load of heat-activated polymethylmethacrylate (PMMA) denture base resin material to a nickel-chromium-beryllium (Ni-Cr-Be) alloy conditioned by three different surface treatments and utilizing two different commercial bonding systems was investigated. Materials and Methods Denture resin (Lucitone-199) was bonded to Ni-Cr-Be alloy specimens treated with Metal Primer II, the Rocatec system with opaquer and the Rocatec system without opaquer. Denture base resin specimens bonded to non-treated sandblasted Ni-Cr-Be alloy were used as controls. Twenty samples for each treatment condition (80 specimens) were tested. The 80 specimens were divided into two categories, thermocycled and non-thermocycled, containing four groups of ten specimens each. The non-thermocycled specimens were tested after 48 hours’ storage in room temperature water. The thermocycled specimens were tested after 2,000 cycles in 4°C and 55°C water baths. The debonding load was calculated in Newtons (N), and collected data were subjected by non parametric test Kruskal-Wallis One Way Analysis of Variance on Ranks and Dunn’s post hoc test at the α = 0.05. Results The Metal Primer II and Rocatec system without opaquer groups produced significantly higher bond strengths (119.9 and 67.6 N), respectively, than did the sandblasted and Rocatec system with opaquer groups, where the bond strengths were 2.6 N and 0 N, respectively. The Metal Primer II was significantly different from all other groups (P<0.05). The bond strengths of all groups were significantly decreased (P<0.05) after thermocycling. Conclusions Although thermocycling had a detrimental effect on the debonding load of all surface treatments tested, the Metal Primer II system provided higher values among all bonding systems tested, before and after thermocycling.


2018 ◽  
Vol 2 (2) ◽  
pp. 120-131
Author(s):  
Fahd Ikram

Despite the development of many denture base material like chrome-cobalt, fluid and plastic material but the heat cure polymethylmethacrylate considered as the most widely used denture base material. The aims of this study to evaluate and compare the impact strength and surface roughness of heat cured denture base resin after immersing incoca-cola drink for two and four weeks. Methods: A total number of 40 samples were prepared, 30 samples for impact strength test and 10 samples for surface roughness test. The samples were divided into three group; A (control), B (2 weeks immersed in coca cola drink), and C (4 weeks immersed in coca cola drink). Result: Data analyzed by using SPSS software with ANOVA test indicated a non significant differences between the different tested groups, however the samples that were immersed in coca cola drink for 4 weeks revealed non dramatic increase in surface roughness, while the samples that were immersed for 2 weeks showed a non dramatic decrease in the impact strength. Conclusions: The coca cola drink non significantly caused dropping in the tested properties in comparison to the control group.


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