scholarly journals The Effects of Electric Field Dynamics on the Quality of Large-Area Nanofibrous Layers

Polymers ◽  
2021 ◽  
Vol 13 (12) ◽  
pp. 1968
Author(s):  
Marek Pokorný ◽  
Jan Klemeš ◽  
Adéla Kotzianová ◽  
Martin Fogl ◽  
Anna Zítková ◽  
...  

This paper presents technological modifications of an electrostatic spinning device, which significantly increase the thickness homogeneity (i.e., quality) of produced layers by creating auxiliary dynamic electric fields in the vicinity of the spinning and collector electrodes. A moving body was installed above the needleless spinning electrode, which destabilized the standing wave occurring on the free surface of the spinning solution. Furthermore, an endless belt design was used for the collector electrode instead of a roll-to-roll design, which made it possible to substantially increase the surface speed of the substrate and, therefore, the dynamics of the electric field at the place of collection of the fibers being spun. As a result, the coefficient of variation of the area weight of 912 samples cut out from the deposited nanofibrous layer, which was (1000 × 500) mm2 in size and had an average area weight of (17.2 ± 0.8) g/m2, was less than 4.5%. These results were obtained only when the dynamics of both the spinning and collector electrodes were increased at the same time. These modifications resulted in a significant increase in the quality of deposited nanofibrous layers up to the standard required for their use in pharmaceutical applications.

2007 ◽  
Vol 10-12 ◽  
pp. 297-302 ◽  
Author(s):  
Yuan Gang Wang ◽  
Fu Ling Zhao

Powder mixed EDM can effectively improve the surface quality of a machined workpiece. In order to study the mechanism of powder mixed EDM process, particles’ activities in working conditions are simulated and corresponding experiments are done. A 3D electric fields model described by finite element method of the particles suspended in working fluid in the electric field is built, the generated field is computed and presented, and the activities of particles in the breakdown process are analyzed. The results show that this method can serve as a good way to learn the activities of particles in the breakdown of discharge.


2013 ◽  
Vol 543 ◽  
pp. 451-454 ◽  
Author(s):  
Shiva Abbaszadeh ◽  
Nicholas Allec ◽  
Karim S. Karim

In this paper, a thin layer of perylene tetracarboxylic bisbenzimidazole (PTCBI) is investigated as a potential hole-blocking contact in an a-Se photodetector. The behavior of the device was characterized as a function of electric field under light and dark conditions. It was found that the PTCBI layer permits operation at high electric fields (>>10 V/μm) while maintaining a dark current density below 200 pA/mm2. Short pulse experiments were performed to assure that charge accumulation at the organic/a-Se interface is negligible and does not reduce the electric field in the a-Se layer. The detector investigated uses a simple low temperature fabrication process based on widely available semiconductor materials that can be easily integrated into current large area digital imager manufacturing processes.


Processes ◽  
2019 ◽  
Vol 7 (7) ◽  
pp. 466
Author(s):  
Urszula Sadowska ◽  
Arkadiusz Matwijczuk ◽  
Agnieszka Niemczynowicz ◽  
Tomasz Dróżdż ◽  
Andrzej Żabiński

In the food industry, the pulsed electric field (PEF) technique is used to support the process of extraction of various substances. The aim of this study was to analyze the effect of a number of PEF pulses applied to peppermint and caraway on both the content of essential oils (EO) and their spectroscopic properties. The examined herb species were placed in a special vessel in the working chamber of the device between two electrodes providing high voltage electric pulses. The pulses were delivered 0, 150, 250, and 350 times per a studied sample of each herb. Essential oils were then obtained by way of hydrodistillation. The infrared spectra for all samples were measured using an FTIR spectrometer in the spectral range of 3700–730 cm−1. The applied electric field of a predetermined number of pulses had no significant effect on the amount of distilled essential oil from caraway fruit, while in the case of peppermint, it caused a slight decrease in relation to the raw material not subjected to PEF exposure. It was found that the analysis of infrared spectra made it possible to compare the quality of the obtained oils with each other and to pre-determine their compositions.


Author(s):  
Zheng Qiao ◽  
Da Qu ◽  
Huiming Wang ◽  
Dongxu Wu ◽  
Bo Wang

The roll-to-roll imprinting technology is considered as the most promising process for manufacturing large-area microstructured surface in a high-precision, high-efficiency and low-cost way. However, the existence of cutting burr of microstructures on roll die will deteriorate the quality of microstructures on target surface in roll-to-roll imprinting processing. For electroplated copper material, this article presents the influence of chip interference on burr in cutting process. The parameter that illustrates the level of chip interference is deduced. The influences of cutting depth and included angle of V-shaped diamond tool on burr height of V-grooves are revealed by analyzing the chip interference. A series of experiments are carried out to verify the theoretical study. The results show good agreement between theoretical derivation and experimental analysis. The reason for chip interference of cutting process is made clear. Then, the optimal process of multi-step cutting process was given as the guidance to enhance the surface quality of micro V-grooves on electroplated copper roll die. With the optimal cutting parameters, the high-quality surface of micro-prism array is achieved.


Author(s):  
G. Lehmpfuhl

Introduction In electron microscopic investigations of crystalline specimens the direct observation of the electron diffraction pattern gives additional information about the specimen. The quality of this information depends on the quality of the crystals or the crystal area contributing to the diffraction pattern. By selected area diffraction in a conventional electron microscope, specimen areas as small as 1 µ in diameter can be investigated. It is well known that crystal areas of that size which must be thin enough (in the order of 1000 Å) for electron microscopic investigations are normally somewhat distorted by bending, or they are not homogeneous. Furthermore, the crystal surface is not well defined over such a large area. These are facts which cause reduction of information in the diffraction pattern. The intensity of a diffraction spot, for example, depends on the crystal thickness. If the thickness is not uniform over the investigated area, one observes an averaged intensity, so that the intensity distribution in the diffraction pattern cannot be used for an analysis unless additional information is available.


2019 ◽  
Author(s):  
Johannes P. Dürholt ◽  
Babak Farhadi Jahromi ◽  
Rochus Schmid

Recently the possibility of using electric fields as a further stimulus to trigger structural changes in metal-organic frameworks (MOFs) has been investigated. In general, rotatable groups or other types of mechanical motion can be driven by electric fields. In this study we demonstrate how the electric response of MOFs can be tuned by adding rotatable dipolar linkers, generating a material that exhibits paralectric behavior in two dimensions and dielectric behavior in one dimension. The suitability of four different methods to compute the relative permittivity κ by means of molecular dynamics simulations was validated. The dependency of the permittivity on temperature T and dipole strength μ was determined. It was found that the herein investigated systems exhibit a high degree of tunability and substantially larger dielectric constants as expected for MOFs in general. The temperature dependency of κ obeys the Curie-Weiss law. In addition, the influence of dipolar linkers on the electric field induced breathing behavior was investigated. With increasing dipole moment, lower field strength are required to trigger the contraction. These investigations set the stage for an application of such systems as dielectric sensors, order-disorder ferroelectrics or any scenario where movable dipolar fragments respond to external electric fields.


Photonics ◽  
2021 ◽  
Vol 8 (4) ◽  
pp. 107
Author(s):  
Haichao Yu ◽  
Feng Tang ◽  
Jingjun Wu ◽  
Zao Yi ◽  
Xin Ye ◽  
...  

In intense-light systems, the traditional discrete optical components lead to high complexity and high cost. Metasurfaces, which have received increasing attention due to the ability to locally manipulate the amplitude, phase, and polarization of light, are promising for addressing this issue. In the study, a metasurface-based reflective deflector is investigated which is composed of silicon nanohole arrays that confine the strongest electric field in the air zone. Subsequently, the in-air electric field does not interact with the silicon material directly, attenuating the optothermal effect that causes laser damage. The highest reflectance of nanoholes can be above 99% while the strongest electric fields are tuned into the air zone. One presentative deflector is designed based on these nanoholes with in-air-hole field confinement and anti-damage potential. The 1st order of the meta-deflector has the highest reflectance of 55.74%, and the reflectance sum of all the orders of the meta-deflector is 92.38%. The optothermal simulations show that the meta-deflector can theoretically handle a maximum laser density of 0.24 W/µm2. The study provides an approach to improving the anti-damage property of the reflective phase-control metasurfaces for intense-light systems, which can be exploited in many applications, such as laser scalpels, laser cutting devices, etc.


2021 ◽  
Vol 5 (1) ◽  
Author(s):  
Marie C. Lefevre ◽  
Gerwin Dijk ◽  
Attila Kaszas ◽  
Martin Baca ◽  
David Moreau ◽  
...  

AbstractGlioblastoma is a highly aggressive brain tumor, very invasive and thus difficult to eradicate with standard oncology therapies. Bioelectric treatments based on pulsed electric fields have proven to be a successful method to treat cancerous tissues. However, they rely on stiff electrodes, which cause acute and chronic injuries, especially in soft tissues like the brain. Here we demonstrate the feasibility of delivering pulsed electric fields with flexible electronics using an in ovo vascularized tumor model. We show with fluorescence widefield and multiphoton microscopy that pulsed electric fields induce vasoconstriction of blood vessels and evoke calcium signals in vascularized glioblastoma spheroids stably expressing a genetically encoded fluorescence reporter. Simulations of the electric field delivery are compared with the measured influence of electric field effects on cell membrane integrity in exposed tumor cells. Our results confirm the feasibility of flexible electronics as a means of delivering intense pulsed electric fields to tumors in an intravital 3D vascularized model of human glioblastoma.


Crystals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 298
Author(s):  
Yannick Minet ◽  
Hans Zappe ◽  
Ingo Breunig ◽  
Karsten Buse

Whispering gallery resonators made out of lithium niobate allow for optical parametric oscillation and frequency comb generation employing the outstanding second-order nonlinear-optical properties of this material. An important knob to tune and control these processes is, e.g., the linear electro-optic effect, the Pockels effect via externally applied electric fields. Due to the shape of the resonators a precise prediction of the electric field strength that affects the optical mode is non-trivial. Here, we study the average strength of the electric field in z-direction in the region of the optical mode for different configurations and geometries of lithium niobate whispering gallery resonators with the help of the finite element method. We find that in some configurations almost 100% is present in the cavity compared to the ideal case of a cylindrical resonator. Even in the case of a few-mode resonator with a very thin rim we find a strength of 90%. Our results give useful design considerations for future arrangements that may benefit from the strong electro-optic effect in bulk whispering gallery resonators made out of lithium niobate.


2021 ◽  
Vol 5 (1) ◽  
Author(s):  
Mohsen Moazzami Gudarzi ◽  
Maryana Asaad ◽  
Boyang Mao ◽  
Gergo Pinter ◽  
Jianqiang Guo ◽  
...  

AbstractThe use of two-dimensional materials in bulk functional applications requires the ability to fabricate defect-free 2D sheets with large aspect ratios. Despite huge research efforts, current bulk exfoliation methods require a compromise between the quality of the final flakes and their lateral size, restricting the effectiveness of the product. In this work, we describe an intercalation-assisted exfoliation route, which allows the production of high-quality graphene, hexagonal boron nitride, and molybdenum disulfide 2D sheets with average aspect ratios 30 times larger than that obtained via conventional liquid-phase exfoliation. The combination of chlorosulfuric acid intercalation with in situ pyrene sulfonate functionalisation produces a suspension of thin large-area flakes, which are stable in various polar solvents. The described method is simple and requires no special laboratory conditions. We demonstrate that these suspensions can be used for fabrication of laminates and coatings with electrical properties suitable for a number of real-life applications.


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