scholarly journals Recoverable Extensional Flow of Polymer Melts and Its Relevance for Processing

Polymers ◽  
2020 ◽  
Vol 12 (7) ◽  
pp. 1512
Author(s):  
Helmut Münstedt
Keyword(s):  
Polymer Melts ◽  
Extensional Flow ◽  
Elongational Flow ◽  
Fused Deposition Modelling ◽  
Extrudate Swell ◽  
Fused Deposition ◽  
Rigid Particles ◽  
Experimental Parameters ◽  
Slit Die

While the uniaxial elongational viscosity is widely investigated, and its relevance for processing is described in the literature, much less has been published on the recoverable extensional flow of polymer melts. This paper presents a short overview of the dependencies of the recoverable elongation on the molecular structure of a polymer, and on some experimental parameters. Its main focus lies on the discussion of processing operations and applications that are largely affected by the elastic components of elongational flow. The recoverable portions of stretched films are considered, and the exploitation of the shrinkage of films, due to the recovery of frozen recoverable deformations, and its role for applications are addressed. The analysis of measurements of velocity fields in the entry region of a slit die and results on the determination of the recoverable elongation from uniaxial experiments, according to the literature, lead to the conclusion of dominant elastic extensions. Considering these facts, the assumptions for Cogswell’s widely used method of determining elongational viscosities under processing conditions from entrance flow are not realistic. As examples of a direct application of extrudate swell from short dies for processing, pelletizing and fused deposition modelling within additive manufacturing are addressed. The special features of extrudate swell from short dies, and uniaxial recoverable elongation for a polymer filled with rigid particles in comparison to an immiscible polymer blend, are presented and discussed.

scholarly journals The Influence of Manufacturing Parameters on the Mechanical Behaviour of PLA and ABS Pieces Manufactured by FDM: A Comparative Analysis

Materials ◽  
2018 ◽  
Vol 11 (8) ◽  
pp. 1333 ◽  
Author(s):  
Adrián Rodríguez-Panes ◽  
Juan Claver ◽  
Ana Camacho
Keyword(s):  
Tensile Strength ◽  
Mechanical Behaviour ◽  
Mechanical Performance ◽  
Acrylonitrile Butadiene Styrene ◽  
Polymer Materials ◽  
Fused Deposition Modelling ◽  
Fused Deposition ◽  
Layer Orientation ◽  
Lower Variability

This paper presents a comparative study of the tensile mechanical behaviour of pieces produced using the Fused Deposition Modelling (FDM) additive manufacturing technique with respect to the two types of thermoplastic material most widely used in this technique: polylactide (PLA) and acrylonitrile butadiene styrene (ABS). The aim of this study is to compare the effect of layer height, infill density, and layer orientation on the mechanical performance of PLA and ABS test specimens. The variables under study here are tensile yield stress, tensile strength, nominal strain at break, and modulus of elasticity. The results obtained with ABS show a lower variability than those obtained with PLA. In general, the infill percentage is the manufacturing parameter of greatest influence on the results, although the effect is more noticeable in PLA than in ABS. The test specimens manufactured using PLA perform more rigidly and they are found to have greater tensile strength than ABS. The bond between layers in PLA turns out to be extremely strong and is, therefore, highly suitable for use in additive technologies. The methodology proposed is a reference of interest in studies involving the determination of mechanical properties of polymer materials manufactured using these technologies.

Analysis of the influence of polylactic acid (PLA) colour on FDM 3D printing temperature and part finishing

2018 ◽  
Vol 24 (8) ◽  
pp. 1305-1316 ◽  
Author(s):  
Juliana Breda Soares ◽  
João Finamor ◽  
Fabio Pinto Silva ◽  
Liane Roldo ◽  
Luis Henrique Cândido
Keyword(s):  
Polylactic Acid ◽  
Three Dimensional ◽  
Mechanical Analysis ◽  
Fused Deposition Modelling ◽  
Process Conditions ◽  
Content Type ◽  
3D Print ◽  
Fused Deposition ◽  
3D Printed

Purpose This paper aims to analyse the effect of different polylactic acid (PLA) colours used on fused deposition modelling (FDM), considering the product finishing quality produced with the same process conditions. Design/methodology/approach The methodology adopted was to design a virtual modelling object and three-dimensional (3D) print it with FDM with different PLA colours (natural, green and black), using the same parameters. 3D scanning and scanning electron microscopy was used to analyse the model finishing of each sample. Fourier-transform infrared spectroscopy analysis, thermogravimetric analysis and dynamic mechanical analysis were used to characterize the material and verify if the colour affected its thermal behaviour. Findings Findings showed that different PLA colours lead to distinct 3D printed finishings under the same process conditions. Thermal analysis showed a reason for the printing finishing difference. The degradation temperatures and the glass temperatures vary depending on the PLA colour. This affects the FDM working temperature. Originality/value This study will contribute to improving the finishing quality of 3D printed products by collaborating to the determination of its process conditions.

Experimental Determination of the Elongational Viscosity of Polymer Solutions

1991 ◽  
Vol 44 (11S) ◽  
pp. S46-S50 ◽  
Author(s):  
A. E. Chavez ◽  
O. Manero ◽  
H. Y. Bao ◽  
R. K. Gupta
Keyword(s):  
Polymer Solutions ◽  
Extensional Flow ◽  
Elongational Flow ◽  
Fiber Spinning ◽  
Momentum Balance ◽  
Test Fluid ◽  
Sodium Acrylate ◽  
Flow Data ◽  
Hydrodynamic Friction

A comparative study is performed between elongational flow data obtained from fiber spinning and a numerical scheme based on the expressions derived from an anisotropic FENE dumbbell model, with conformation-dependent hydrodynamic friction, coupled with a differential momentum balance made along the spinning filament. Extensional flow data was obtained by using the Gupta-Sridhar extensional viscometer. The test fluid was an aqueous solution of a copolymer of sodium acrylate and acrylamide (Alcomer 120). From the information obtained by this comparison, we assess the influence of preshearing and other factors on the rheological behavior of polymer solutions using this technique.

Evaluation of geometrical benchmark artifacts containing multiple overhang lengths fabricated using material extrusion technique

2020 ◽  
Vol 14 (3) ◽  
pp. 7296-7308
Author(s):  
Siti Nur Humaira Mazlan ◽  
Aini Zuhra Abdul Kadir ◽  
N. H. A. Ngadiman ◽  
M.R. Alkahari
Keyword(s):  
3D Model ◽  
Laser Scanner ◽  
Dimensional Accuracy ◽  
Fused Deposition Modelling ◽  
Layer By Layer ◽  
Fused Deposition ◽  
Layer Technique ◽  
Subtractive Manufacturing ◽  
Manufacturing Features ◽  
Layer Problem

Fused deposition modelling (FDM) is a process of joining materials based on material entrusion technique to produce objects from 3D model using layer-by-layer technique as opposed to subtractive manufacturing. However, many challenges arise in the FDM-printed part such as warping, first layer problem and elephant food that was led to an error in dimensional accuracy of the printed parts especially for the overhanging parts. Hence, in order to investigate the manufacturability of the FDM printed part, various geometrical and manufacturing features were developed using the benchmarking artifacts. Therefore, in this study, new benchmarking artifacts containing multiple overhang lengths were proposed. After the benchmarking artifacts were developed, each of the features were inspected using 3D laser scanner to measure the dimensional accuracy and tolerances. Based on 3D scanned parts, 80% of the fabricated parts were fabricated within ±0.5 mm of dimensional accuracy as compared with the CAD data. In addition, the multiple overhang lengths were also successfully fabricated with a very significant of filament sagging observed.

Optimization of Extraction Parameters of Reverse Iontophoretic Determination of Blood Glucose in an Artificial Skin Model

2020 ◽  
Vol 16 (6) ◽  
pp. 722-737
Author(s):  
Cigdem Yengin ◽  
Emrah Kilinc ◽  
Fatma Gulay Der ◽  
Mehmet Can Sezgin ◽  
Ilayda Alcin
Keyword(s):  
Ionic Strength ◽  
Body Fluids ◽  
Extraction Time ◽  
Artificial Skin ◽  
Dialysis Membrane ◽  
Skin Model ◽  
Non Invasive ◽  
Electrode Distance ◽  
Experimental Parameters

Background: Reverse İontophoresis (RI) is one of the promising non-invasive technologies. It relies on the transition of low magnitude current through the skin and thus glucose measurement becomes possible as it is extracted from the surface during this porter current flow. Objective: This paper deals with the development and optimization of an RI determination method for glucose. CE dialysis membrane based artificial skin model was developed and the dependence of RI extraction on various experimental parameters was investigated. Method: Dependence of RI extraction performance on noble electrodes (platinum, silver, palladium, ruthenium, rhodium) was checked with CA, CV and DPV, in a wide pH and ionic strength range. Optimizations on inter-electrode distance, potential type and magnitude, extraction time, gel type, membrane MWCO, usage frequency, pretreatment, artificial body fluids were performed. Results: According to the optimized results, the inter-electrode distance was 7.0 mm and silver was the optimum noble metal. Optimum pH and ionic strength were achieved with 0.05M PBS at pH 7.4. Higher glucose yields were obtained with DPV, while CA and CV achieved almost the same levels. During CA, +0.5V achieved the highest glucose yield and higher potential even caused a decrease. Glucose levels could be monitored for 24 hours. CMC gel was the optimum collection media. Pretreated CE membrane with 12kD MWCO was the artificial skin model. Pretreatment affected the yields while its condition caused no significant difference. Except PBS solution (simulated as artificial plasma), among the various artificial simulated body fluids, intestinal juice formulation (AI) and urine formulation U2 were the optimum extraction media, respectively. Conclusion: In this study, various experimental parameters (pretereatment procedure, type and MWCO values of membranes, inter-electrode distance, electrode material, extraction medium solvents, ionic strength and pH, collection medium gel type, extraction potential type and magnitude, extraction time and etc) were optimized for the non-invasive RI determination of glucose in a CE dialysis membrane-based artificial skin model and various simulated artificial body fluids.

scholarly journals Current State and Challenges of Natural Fibre-Reinforced Polymer Composites as Feeder in FDM-Based 3D Printing

Polymers ◽  
2021 ◽  
Vol 13 (14) ◽  
pp. 2289
Author(s):  
Nishata Royan Rajendran Royan ◽  
Jie Sheng Leong ◽  
Wai Nam Chan ◽  
Jie Ren Tan ◽  
Zainon Sharmila Binti Shamsuddin
Keyword(s):  
Mechanical Properties ◽  
Natural Fibre ◽  
Critical Discussion ◽  
Fused Deposition Modelling ◽  
Preparation Methods ◽  
Fused Deposition ◽  
Current State ◽  
Future Challenges ◽  
Raster Angle ◽  
Fibre Reinforced Polymer

As one of the fastest-growing additive manufacturing (AM) technologies, fused deposition modelling (FDM) shows great potential in printing natural fibre-reinforced composites (NFRC). However, several challenges, such as low mechanical properties and difficulty in printing, need to be overcome. Therefore, the effort to improve the NFRC for use in AM has been accelerating in recent years. This review attempts to summarise the current approaches of using NFRC as a feeder for AM. The effects of fibre treatments, composite preparation methods and addition of compatibilizer agents were analysed and discussed. Additionally, current methods of producing feeders from NFRCs were reviewed and discussed. Mechanical property of printed part was also dependent on the printing parameters, and thus the effects of printing temperature, layer height, infill and raster angle were discussed, and the best parameters reported by other researchers were identified. Following that, an overview of the mechanical properties of these composites as reported by various researchers was provided. Next, the use of optimisation techniques for NFRCs was discussed and analysed. Lastly, the review provided a critical discussion on the overall topic, identified all research gaps present in the use of NFRC for AM processes, and to overcome future challenges.

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