scholarly journals The Effect of Ageing in Water Solution Containing Iron Sulfate on the Mechanical Properties of Epoxy Adhesives

Polymers ◽  
2020 ◽  
Vol 12 (1) ◽  
pp. 218 ◽  
Author(s):  
Anna Rudawska ◽  
Valentina Brunella
Keyword(s):  
Mechanical Properties ◽  
Water Solution ◽  
Compressive Strain ◽  
Testing Machine ◽  
Water Environment ◽  
Compression Modulus ◽  
Iron Sulfate ◽  
Curing Agent ◽  
Adhesive Compound ◽  
Amine Curing

This study investigates the effect of operating factors such as seasoning in water solution containing iron (II) sulfate—FeSO4 (5 different water solution variants were tested) on the mechanical properties of an adhesive compound made of epoxy resin and amine curing agent, in a ratio of 100 g resin to 12 g curing agent. Strength tests of cured adhesive compound samples were performed on the Zwick/Roell Z150 testing machine in compliance with the EN ISO 604 standard. During the tests, compression modulus, compressive strength and compressive strain were measured. Obtained results served as a basis for analyzing the effect of a water environment containing iron sulfate on a given adhesive compound. It has been found that too high iron sulfate content in water has a negative effect on the mechanical properties of adhesive compound samples.

scholarly journals The Effect of the Salt Water Aging on the Mechanical Properties of Epoxy Adhesives Compounds

Polymers ◽  
2020 ◽  
Vol 12 (4) ◽  
pp. 843 ◽  
Author(s):  
Anna Rudawska
Keyword(s):  
Mechanical Properties ◽  
Calcium Carbonate ◽  
Salt Water ◽  
Tap Water ◽  
Testing Machine ◽  
Epoxy Adhesive ◽  
Curing Agent ◽  
Epoxy Adhesives ◽  
Adhesive Compound ◽  
Strength Tests

The objective of this study is to compare the effect of selected operating factors on the mechanical properties of epoxy adhesive compounds aged in salt water. Five different water environments were tested: tap water, normal seawater (reference salinity value), seawater with double reference salinity value, seawater with half of the reference salinity and seawater with a quarter of the reference salinity value. Samples of two different adhesive compounds were prepared using the epoxy resin and triethylenetetramine curing agent. One of the compounds was filled with calcium carbonate. The samples were aged in five different water environments for three months, one month and one week, respectively. Mechanical properties of the cured adhesive compound samples were determined via strength tests performed on the Zwick/Roell Z150 testing machine in compliance with the EN ISO 604 standard. The objective of the experiments was to determine the effect of different seawater environments on selected mechanical properties (including strength) of the fabricated adhesive compounds.

scholarly journals Comparison of the adhesive joints’ strength of the similar and dissimilar systems of metal alloy/polymer composite

2019 ◽  
Vol 7 (1) ◽  
Author(s):  
Anna Rudawska
Keyword(s):  
Epoxy Composite ◽  
Testing Machine ◽  
Lap Joints ◽  
Adhesive Joints ◽  
Curing Agent ◽  
Dissimilar Joints ◽  
Adhesive Compound ◽  
Curing Agents ◽  
Materials Used ◽  
Amine Curing

AbstractThe aim of the present article is to compare the strength of the adhesive lap joints of the selected materials used in aviation. The joints were made in the similar and dissimilar systems with the use of three epoxy adhesives. Three different adherends were used: the EN AW-7075 aluminium alloy, the aramid-epoxy composite and the carbon-epoxy composite. Three adhesive compounds based on the Epidian 53 epoxy resin and three types of curing agents: two amine curing agents—Z1 (triethylenetetramine curing agent) and IDA, and one polyamide curing agent—PAC (polyaminoamide C) were used to make the adhesive joints. Three variants of similar joints and two variants of dissimilar joints were prepared for the tests. The shear strength was defined according to the ISO 4587 standard, with the use of Zwick/Roell 150 testing machine. In addition, the joined materials’ surface roughness was measured. Based on the strength test’s results, it was observed that the highest strength was obtained by the adhesive joints made with the Epidian 53/PAC/100:80 adhesive compound and that, in the majority of cases; similar joints show higher strength.

scholarly journals The Impact of the Seasoning Conditions on Mechanical Properties of Modified and Unmodified Epoxy Adhesive Compounds

Polymers ◽  
2019 ◽  
Vol 11 (5) ◽  
pp. 804 ◽  
Author(s):  
Anna Rudawska
Keyword(s):  
Mechanical Properties ◽  
Ambient Temperature ◽  
Testing Machine ◽  
Negative Temperature ◽  
Epoxy Adhesive ◽  
Adhesive Compound ◽  
Strength Tests ◽  
Curing Agents ◽  
Amine Curing ◽  
The Impact

The aim of this study was to analyse the impact of the adhesive samples seasoning conditions (temperature and time) on selected mechanical properties of four epoxy adhesive compounds (two unmodified and two modified ones). The samples were made of Epidian 53 epoxy resin mixed with the two different amine curing agents in appropriate stoichiometric proportions. A filler in the form of calcium carbonate (CaCO3) powder was used as a modifier. The adhesive compound samples were cured for seven days. Six seasoning variants were used. Four of them were related with the seasoning time at ambient temperature of 24 ± 2 °C for: one month, two months, five months and eight months, respectively. Two other variants were related with seasoning at negative temperature (−10 ± 2 °C) for one month. The last variant (F) also included seasoning at ambient temperature (24 ± 2 °C) for five months right after seasoning in negative temperature. Cured and cylinder-shaped adhesive compound samples were subjected to compressive strength tests (according to the ISO 604 standard). The strength tests were performed using a Zwick/Roell Z150 testing machine. Based on the tests, it was observed that both temperature and time of seasoning influenced the adhesive’s mechanical properties. In the perspective of eight months, these changes were relatively minor for the samples seasoned at ambient temperature. The adhesive samples prepared for the tests were especially sensitive to negative temperature.

A Novel Epoxy Resin Toughened by HTBN Liquid Rubber

1992 ◽  
Vol 274 ◽  
Author(s):  
Xiaozu Han ◽  
Zhankui Yun ◽  
Fenchun Guo
Keyword(s):  
Mechanical Properties ◽  
Epoxy Resin ◽  
Phase Structure ◽  
Curing Agent ◽  
Two Phase ◽  
Liquid Rubber ◽  
Sem And Tem ◽  
Amine Curing Agent ◽  
Rubber Phase ◽  
Amine Curing

ABSTRACTA novel toughened epoxy resin was obtained by using an epoxy-terminated prepolymer prepared from epoxy resin and hydroxy-terminated butadiene-acryl-onitrile copolymer (HTBN), and an amine curing agent. The cured, toughened resin has excellent mechanical properties due to the two-phase structure which was observed using SEM and TEM. When the HTBN content is 15 phr, the rubber phase separates effectively and the specimen presents a fine two-phase structure. However, when the HTBN content reaches 25 phr, the morphology appears continuous.

scholarly journals Effect of Compressive Strain Rate on Microstructure and Mechanical Properties of 7050 Aluminium Alloy

2021 ◽  
Vol 2021 ◽  
pp. 1-8
Author(s):  
Qiang Shen ◽  
Luochuang Huang ◽  
Yan Li ◽  
Kang Yu ◽  
Dezheng Liu
Keyword(s):  
Mechanical Properties ◽  
Strain Rate ◽  
Aluminium Alloy ◽  
Compressive Strain ◽  
Testing Machine ◽  
Fracture Morphology ◽  
Automobile Manufacturing ◽  
Grain Sizes ◽  
Universal Testing ◽  
Microstructure And Mechanical Properties

7050 aluminium alloy is a superior material used in the areas of aerospace and automobile manufacturing. In this work, homogeneous cast cylinder samples of 7050 aluminium alloy with size of Φ80 mm × 100 mm were compressed isothermally at 350°C with compressive strain rate of 0.1 s−1,1 s−1, and 10 s−1, respectively. The samples were then processed into standard tensile specimens, and then tensile testing was done by using the GL8305 universal testing machine. The grain sizes and fracture morphology were analyzed by the SEM observation and cellular automaton (CA) method. The effect of compressive strain rate on microstructure and mechanical properties of 7050 aluminium alloy was investigated. The results show the following. (1) Grain refinement occurred after compression. The grain sizes of the samples decrease with the decrease of compressive strain rate. The grain sizes in the radial edge and the axial center of the cylinder samples are the smallest. (2) The tensile strength and breaking elongation rate were improved when compared to the original alloy. The mechanical properties of samples compressed with compressive strain rate of 0.1 s−1 are the best. (3) The fracture morphology of the samples shows that the fracture of the samples is ductile fracture. The sizes and depths of dimples increased with the decrease of grain sizes.

Comparison of different curing method for mechanical properties of self-curing agent using diapers polymer

2021 ◽  
Author(s):  
Daud Mohamad ◽  
Salmia Beddu ◽  
Ibrahim ◽  
Karim Sherif ◽  
Mahyun Zainoddin ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Curing Agent ◽  
Curing Method

scholarly journals Development of Al–Mg–Si alloy performance by addition of grain refiner Al–5Ti–1B alloy

2021 ◽  
Vol 104 (2) ◽  
pp. 003685042110294
Author(s):  
Khaled Abd El-Aziz ◽  
Emad M Ahmed ◽  
Abdulaziz H Alghtani ◽  
Bassem F Felemban ◽  
Hafiz T Ali ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Corrosion Resistance ◽  
Testing Machine ◽  
Dendritic Structure ◽  
Grain Refiner ◽  
Corrosion Properties ◽  
Average Grain Size ◽  
Structural Applications ◽  
Alloy Addition

Aluminum alloys are the most essential part of all shaped castings manufactured, mainly in the automotive, food industry, and structural applications. There is little consensus as to the precise relationship between grain size after grain refinement and corrosion resistance; conflicting conclusions have been published showing that reduced grain size can decrease or increase corrosion resistance. The effect of Al–5Ti–1B grain refiner (GR alloy) with different percentages on the mechanical properties and corrosion behavior of Aluminum-magnesium-silicon alloy (Al–Mg–Si) was studied. The average grain size is determined according to the E112ASTM standard. The compressive test specimens were made as per ASTM: E8/E8M-16 standard to get their compressive properties. The bulk hardness using Vickers hardness testing machine at a load of 50 g. Electrochemical corrosion tests were carried out in 3.5 % NaCl solution using Autolab Potentiostat/Galvanostat (PGSTAT 30).The grain size of the Al–Mg–Si alloy was reduced from 82 to 46 µm by the addition of GR alloy. The morphology of α-Al dendrites changes from coarse dendritic structure to fine equiaxed grains due to the addition of GR alloy and segregation of Ti, which controls the growth of primary α-Al. In addition, the mechanical properties of the Al–Mg–Si alloy were improved by GR alloy addition. GR alloy addition to Al–Mg–Si alloy produced fine-grained structure and better hardness and compressive strength. The addition of GR alloy did not reveal any marked improvements in the corrosion properties of Al–Mg–Si alloy.

scholarly journals Acoustic Emission and K-S Metric Entropy as Methods for Determining Mechanical Properties of Composite Materials

Sensors ◽  
2020 ◽  
Vol 21 (1) ◽  
pp. 145
Author(s):  
Lesław Kyzioł ◽  
Katarzyna Panasiuk ◽  
Grzegorz Hajdukiewicz ◽  
Krzysztof Dudzik
Keyword(s):  
Mechanical Properties ◽  
Acoustic Emission ◽  
Composite Material ◽  
Composite Materials ◽  
Testing Machine ◽  
Measurement Data ◽  
Entropy Method ◽  
Displacement Sensor ◽  
Metric Entropy ◽  
Plastic Phase

Due to the unique properties of polymer composites, these materials are used in many industries, including shipbuilding (hulls of boats, yachts, motorboats, cutters, ship and cooling doors, pontoons and floats, torpedo tubes and missiles, protective shields, antenna masts, radar shields, and antennas, etc.). Modern measurement methods and tools allow to determine the properties of the composite material, already during its design. The article presents the use of the method of acoustic emission and Kolmogorov-Sinai (K-S) metric entropy to determine the mechanical properties of composites. The tested materials were polyester-glass laminate without additives and with a 10% content of polyester-glass waste. The changes taking place in the composite material during loading were visualized using a piezoelectric sensor used in the acoustic emission method. Thanks to the analysis of the RMS parameter (root mean square of the acoustic emission signal), it is possible to determine the range of stresses at which significant changes occur in the material in terms of its use as a construction material. In the K-S entropy method, an important measuring tool is the extensometer, namely the displacement sensor built into it. The results obtained during the static tensile test with the use of an extensometer allow them to be used to calculate the K-S metric entropy. Many materials, including composite materials, do not have a yield point. In principle, there are no methods for determining the transition of a material from elastic to plastic phase. The authors showed that, with the use of a modern testing machine and very high-quality instrumentation to record measurement data using the Kolmogorov-Sinai (K-S) metric entropy method and the acoustic emission (AE) method, it is possible to determine the material transition from elastic to plastic phase. Determining the yield strength of composite materials is extremely important information when designing a structure.

scholarly journals Formation conditions and mechanical properties of aggregates produced in tephra–water–snow flows

2020 ◽  
Vol 72 (1) ◽  
Author(s):  
Hirofumi Niiya ◽  
Kenichi Oda ◽  
Daisuke Tsuji ◽  
Hiroaki Katsuragi
Keyword(s):  
Mechanical Properties ◽  
Mixing Time ◽  
Testing Machine ◽  
Small Scale ◽  
Scaling Analysis ◽  
Compression Tests ◽  
Ice Slurry ◽  
Experimental Conditions ◽  
Formation Conditions ◽  
Snow And Ice

Abstract The formation of aggregates consisting of snow, water, and tephra has been reported in small-scale experiments on three-phase flows containing tephra, water, and snow, representing lahars triggered by snowmelt. Such aggregates reduce the mobility of mud flow. However, the formation mechanism of such aggregates under various conditions has not been investigated. To elucidate the formation conditions and mechanical properties of the aggregates, we performed mixing experiments with materials on a rotating table and compression tests on the resulting aggregates with a universal testing machine in a low-temperature room at $$0\,^{\circ }\text {C}$$ 0 ∘ C . From experiments with varying component ratios of the mixture and tephra diameter, the following results were obtained: (i) the aggregate grew rapidly and reached maturity after a mixing time of 5 min; (ii) the mass of aggregates increased with snow concentration, exhibiting an approximately linear relationship; (iii) single aggregates with large mass formed at lower and higher tephra concentrations, whereas multiple aggregates with smaller mass were observed at intermediate concentrations; (iv) the shape of the aggregate satisfied the similarity law for an ellipsoid; (v) the compressive mechanical behavior could be modeled by an empirical nonlinear model. The obtained mechanical properties of the aggregates were independent of the experimental conditions; (vi) scaling analysis based on the Reynolds number and the strength of the aggregates showed that the aggregates cannot form in ice-slurry lahars. Our findings suggest that low-speed lahars containing snow and ice are likely to generate aggregates, but snow and ice in the ice-slurry lahars are dispersed without such aggregates.

scholarly journals Development of Novel Lightweight Al-Rich Quinary Medium-Entropy Alloys with High Strength and Ductility

Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4223
Author(s):  
Po-Sung Chen ◽  
Yu-Chin Liao ◽  
Yen-Ting Lin ◽  
Pei-Hua Tsai ◽  
Jason S. C. Jang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Compressive Strength ◽  
Compressive Strain ◽  
High Strength ◽  
Fine Tuning ◽  
Face Centered Cubic ◽  
Transportation Industry ◽  
High Entropy ◽  
Good Potential ◽  
Face Centered

Most high-entropy alloys and medium-entropy alloys (MEAs) possess outstanding mechanical properties. In this study, a series of lightweight nonequiatomic Al50–Ti–Cr–Mn–V MEAs with a dual phase were produced through arc melting and drop casting. These cast alloys were composed of body-centered cubic and face-centered cubic phases. The density of all investigated MEAs was less than 5 g/cm3 in order to meet energy and transportation industry requirements. The effect of each element on the microstructure evolution and mechanical properties of these MEAs was investigated. All the MEAs demonstrated outstanding compressive strength, with no fractures observed after a compressive strain of 20%. Following the fine-tuning of the alloy composition, the Al50Ti20Cr10Mn15V5 MEA exhibited the most compressive strength (~1800 MPa) and ductility (~34%). A significant improvement in the mechanical compressive properties was achieved (strength of ~2000 MPa, strain of ~40%) after annealing (at 1000 °C for 0.5 h) and oil-quenching. With its extremely high specific compressive strength (452 MPa·g/cm3) and ductility, the lightweight Al50Ti20Cr10Mn15V5 MEA demonstrates good potential for energy or transportation applications in the future.

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