Comparison of different curing method for mechanical properties of self-curing agent using diapers polymer

2021 ◽  
Author(s):  
Daud Mohamad ◽  
Salmia Beddu ◽  
Ibrahim ◽  
Karim Sherif ◽  
Mahyun Zainoddin ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Curing Agent ◽  
Curing Method

scholarly journals Comparison of Mechanical Properties of PMMA Disks for Digitally Designed Dentures

Polymers ◽  
2021 ◽  
Vol 13 (11) ◽  
pp. 1745
Author(s):  
Tamaki Hada ◽  
Manabu Kanazawa ◽  
Maiko Iwaki ◽  
Awutsadaporn Katheng ◽  
Shunsuke Minakuchi
Keyword(s):  
Mechanical Properties ◽  
Flexural Strength ◽  
Water Sorption ◽  
Water Solubility ◽  
Flexural Modulus ◽  
Manufacturing Method ◽  
Heat Curing ◽  
Significant Difference ◽  
Cad Cam ◽  
Curing Method

In this study, the physical properties of a custom block manufactured using a self-polymerizing resin (Custom-block), the commercially available CAD/CAM PMMA disk (PMMA-disk), and a heat-polymerizing resin (Conventional PMMA) were evaluated via three different tests. The Custom-block was polymerized by pouring the self-polymerizing resin into a special tray, and Conventional PMMA was polymerized with a heat-curing method, according to the manufacturer’s recommended procedure. The specimens of each group were subjected to three-point bending, water sorption and solubility, and staining tests. The results showed that the materials met the requirements of the ISO standards in all tests, except for the staining tests. The highest flexural strength was exhibited by the PMMA-disk, followed by the Custom-block and the Conventional PMMA, and a significant difference was observed in the flexural strengths of all the materials (p < 0.001). The Custom-block showed a significantly higher flexural modulus and water solubility. The water sorption and discoloration of the Custom-block were significantly higher than those of the PMMA-disk, but not significantly different from those of the Conventional PMMA. In conclusion, the mechanical properties of the three materials differed depending on the manufacturing method, which considerably affected their flexural strength, flexural modulus, water sorption and solubility, and discoloration.

scholarly journals Thermal analysis of halogenated rubber cured with a new cross-linking system

2019 ◽  
Vol 138 (6) ◽  
pp. 4395-4405 ◽  
Author(s):  
Anna Dziemidkiewicz ◽  
Magdalena Maciejewska ◽  
Martyna Pingot
Keyword(s):  
Mechanical Properties ◽  
Cross Linking ◽  
Curing Agent ◽  
Metal Acetylacetonates ◽  
Damping Properties ◽  
Rubber Blends ◽  
Rubber Compounds ◽  
Curing Agents ◽  
Brominated Butyl Rubber ◽  
Thermal Stability Of

Abstract The aim of this work was to examine the influence of new curing agents proposed for brominated butyl rubber (BIIR) on the cross-linking process of rubber compounds and the thermal behavior of the vulcanizates. Rubber blends that were filled with carbon black and contained acetylacetonates of different transition metals in the presence of triethanolamine (TEOA) as new cross-linking agents were prepared. The performed studies showed that metal acetylacetonates (Me(acac)) are effective cross-linking agents for BIIR, which was confirmed by high values of the torque increment (∆M) and significant cross-linking degree of the vulcanizates (α(T)). The most active curing agent seems to be iron acetylacetonate (Fe(acac)). Its application results in a shorter optimal vulcanization time, lower onset vulcanization temperature and similar vulcanization enthalpy compared to the BIIR cured with a sulfur curing system. The BIIR vulcanizates cured with Me(acac) reveal good mechanical properties with tensile strengths in the range of 9–14 MPa and better damping properties comparing to the sulfur-cured rubber. The proposed curing agents do not significantly affect the thermal stability of the BIIR vulcanizates.

scholarly journals The effect of curing conditions on the mechanical properties of SIFCON

2021 ◽  
Vol 20 (1) ◽  
pp. 37-51
Author(s):  
Kubilay Akçaözoğlu ◽  
◽  
Adem Kıllı ◽  
Keyword(s):  
Mechanical Properties ◽  
Flexural Strength ◽  
Steel Fiber ◽  
Impact Resistance ◽  
Strength Properties ◽  
Fiber Reinforced Concrete ◽  
Curing Conditions ◽  
Accelerated Curing ◽  
Aspect Ratios ◽  
Curing Method

In this study, the effect of curing conditions on the mechanical properties of slurry infiltrated fiber reinforced concrete (SIFCON) was investigated. For this purpose, SIFCON samples containing 4% and 8% steel fiber with two different aspect ratios were produced. The samples were subjected to three different curing types, namely standard, dry and accelerated curing methods. Ultrasonic wave velocity, flexural strength, fracture toughness, compressive strength, impact resistance and capillary water absorption tests were performed on the samples. The highest flexural strength was found to be achieved in the samples with an aspect ratio of 55 and a content of 8% steel fiber. The most suitable curing method was determined as the standard curing method and the best flexural strength was achieved at the rate of 8%. According to the test results, the best strength properties were achieved in the samples exposed to the standard curing method. In addition, the samples exposed to the accelerated curing method showed satisfactory values. The accelerated curing method can be used as an alternative in SIFCON production especially in applications requiring mass production.

Lechugilla natural fiber as internal curing agent in self compacting concrete (SCC): Mechanical properties, shrinkage and durability

2020 ◽  
Vol 112 ◽  
pp. 103686
Author(s):  
R. Dávila-Pompermayer ◽  
L.G. Lopez-Yepez ◽  
P. Valdez-Tamez ◽  
C.A. Juárez ◽  
A. Durán-Herrera
Keyword(s):  
Mechanical Properties ◽  
Natural Fiber ◽  
Internal Curing ◽  
Curing Agent ◽  
Self Compacting Concrete

The Research on the Mechanical Properties of the same Curing Agent of Different Soil Dredged Mud

2013 ◽  
Vol 800 ◽  
pp. 181-188
Author(s):  
Xiao Yan Yang ◽  
Wen Bai Liu ◽  
Jia Jun Wang ◽  
Wen Hui Shi
Keyword(s):  
Mechanical Properties ◽  
Shear Strength ◽  
Compression Test ◽  
Direct Shear Test ◽  
Shear Test ◽  
Silty Sand ◽  
Curing Agent ◽  
Direct Shear ◽  
Confined Compression ◽  
Silty Soil

Through confined compression test and direct shear test, studied the mechanical properties of the same curing agent of different soil dredged mud, compared the difference of the same curing agent of different soil dredged mud. By confined compression test, the compression modulus of clay, silty sand and silty soil dredged mud after curing increases by 603.7%, 529.0% , 603.7% respectively. By direct shear test, the shear strength of clay dredged mud after curing increases to infinity; silty sands shear strength after curing increases by 209.1% in average; silty soils shear strength increases after curing by 147.5% in average. The compression and shear resistance of this kind of special curing agent for clay is best, silty sand second, but for the silty soil only has a little effect.

Curing study and evaluation of epoxy resin with amine functional chloroaniline acetaldehyde condensate

2015 ◽  
Vol 44 (1) ◽  
pp. 19-25
Author(s):  
T. Maity ◽  
B.C. Samanta
Keyword(s):  
Mechanical Properties ◽  
Molecular Weight ◽  
Epoxy Resin ◽  
Ph Value ◽  
Kinetic Studies ◽  
Diglycidyl Ether ◽  
Curing Agent ◽  
Scanning Calorimetry ◽  
Content Type ◽  
Curing Reaction

Purpose – The purpose of this paper was to check effectiveness of amine functional chloroaniline acetaldehyde condensate (AFCAC) as a new curing agent for diglycidyl ether of bisphenol A (DGEBA) resin. For this purpose, first AFCAC was synthesised, characterised and then curing reaction was carried out. Design/methodology/approach – Equimolecular mixture of AFCAC and DGEBA was subjected to curing reaction, and the reaction was followed by differential scanning calorimetry (DSC) analysis. The kinetic studies of this curing reaction were also carried out from those DSC exotherms. The mechanical properties, dynamic mechanical analysis (DMA) and thermogravimetric analysis (TGA) of cured epoxy were also reported. Findings – DSC results reflected the effective first order curing reaction of AFCAC with epoxy resin. Mechanical properties reflected appreciable rigidity of AFCAC cured epoxy matrix and TGA showed that the cured epoxy networks were thermally stable up to around 297°C. Research limitations/implications – The curing agent AFCAC was synthesised by using chloroaniline and acetaldehyde in acid medium. There are some limitations for this procedure. The synthetic procedure is pH dependent. So reaction cannot be done at any pH value. The reaction must also be carried out at room temperature without any heating. To obtain low molecular weight curing agent, chloroaniline and acetaldehyde cannot be taken in equimolecular ratio because the equimolecular mixture of them produces high molecular weight condensate. This was shown in our previous publication. Some implications are also there. By changing amine and aldehyde other curing agents could be synthesised and the curing efficiency of those for epoxy resin could also be studied. Originality/value – Experimental results revealed the greater suitability of AFCAC as curing agent for DGEBA resin and novelty of AFCAC cured matrix in the field of protective coating, casting, adhesives, etc.

Enhancement of the mechanical properties at the macro and nanoscale of thermosetting systems modified with a polystyrene-block-polymethyl methacrylate block copolymer

RSC Advances ◽  
2015 ◽  
Vol 5 (123) ◽  
pp. 102085-102095 ◽  
Author(s):  
Laida Cano ◽  
Junkal Gutierrez ◽  
Agnieszka Tercjak
Keyword(s):  
Mechanical Properties ◽  
Block Copolymer ◽  
Polymethyl Methacrylate ◽  
Curing Agent

An epoxy-based thermosetting system was modified with varying contents of polystyrene-block-polymethyl methacrylate (PS-b-PMMA) block copolymer by two methods and cured with a 4,4′-methylenebis(3-chloro-2,6-diethylaniline) (MCDEA) curing agent.

Mechanical Properties of Epoxy Clay Nanocomposites

2010 ◽  
Vol 123-125 ◽  
pp. 145-148 ◽  
Author(s):  
Sahar Ghafarloo ◽  
Mehrdad Kokabi
Keyword(s):  
Mechanical Properties ◽  
Diglycidyl Ether ◽  
Good Evidence ◽  
Layered Silicates ◽  
Clay Nanocomposites ◽  
Curing Agent ◽  
Test Results ◽  
X Ray Diffraction ◽  
Cloisite 30B ◽  
Diffraction Patterns

Achievement of exfoliated structure of polymer/ Clay nanocomposites is of particular interest for the improvement of mechanical properties. In this work, the morphology and mechanical properties of epoxy/ clay nanocomposites has been investigated. Diglycidyl ether of bis-phenol A (DGEBA) epoxy resin (EPON828) and Jeffamine D400 curing agent was used. To obtain perfect dispersion, nanoclay (Cloisite 30B) was sonicated in acetone. The mixture was then mixed with polymer. Afterwards, the curing process was performed by addition of curing agent and degassing. Disappearing of peaks in X-Ray diffraction patterns of nanocomposites containing less than 5wt% nanoclay, is a good evidence of perfect dispersion of layered silicates in matrix, i.e. formation of exfoliated morphology. Based on tensile test results, it is deduced that as the amount of nanoclay increases, the elastic modulus and elongation at break of the nanocomposites containing 1wt% and 5wt% nanoclay increases by 12% and 31%, respectively. Therefore, obtaining perfect dispersion of layered silicates in epoxy matrix and exfoliated morphology, results in better mechanical properties of the nanocomposites.

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