scholarly journals Surface Characterization and Optical Properties of Reinforced Dental Glass-Ceramics Related to Artificial Aging

Molecules ◽  
2020 ◽  
Vol 25 (15) ◽  
pp. 3407
Author(s):  
Liliana Porojan ◽  
Roxana-Diana Vasiliu ◽  
Mihaela-Ionela Bîrdeanu ◽  
Sorin-Daniel Porojan

The development of various dental glass-ceramic materials and the evolution of novel processing technologies lead to an essential change in the clinical and technical workflow. The long-term success of a dental restoration treatment is defined by its durability, which is directly influenced by the oral environment. This study’s purpose was to evaluate the artificial aging behavior of nanostructured, respective microstructured ceramics related to surface topography, roughness, and optical properties. Six monolithic restoration materials were selected: milled lithium disilicate glass-ceramic (LDS-M) MT (medium translucency), hot-pressed lithium disilicate glass-ceramic (LDS-P) MT and HT (high translucency), milled zirconia-reinforced lithium silicate ceramic (ZLS-M) MT and hot-pressed zirconia-reinforced lithium silicate ceramic (ZLS-P) MT and HT, resulting n = 96 surfaces. All the samples were artificially aged by thermal cycling, and all investigations were made before and after thermal cycling. In terms of optical properties, differences recorded between ZLS and LDS ceramics are not significant. Thermal cycling increases the translucency of ZLS and LDS glass-ceramic materials significantly, with the most harmful effect on the pressed and polished samples. Micro- and nano roughness are significantly influenced by in vitro aging and a negative correlation was recorded. Glazed samples are characterized by significant rougher surfaces for all types of materials. On nanolevel, ZLS materials are significantly smoothed by thermal cycling.

Materials ◽  
2020 ◽  
Vol 13 (2) ◽  
pp. 381 ◽  
Author(s):  
Roxana-Diana Vasiliu ◽  
Sorin Daniel Porojan ◽  
Mihaela Ionela Bîrdeanu ◽  
Liliana Porojan

Dental ceramic restorations are widely spread nowadays due to their aesthetics and biocompatibility. In time, the colour and structure of these ceramic materials can be altered by aging processes. How does artificial aging affect the optical and surface roughness of ceramics? This study aims to assess the effect of thermocycling, surface treatments and microstructure upon translucency, opalescence and surface roughness on CAD-CAM and heat-pressed glass-ceramic. Forty-eight samples (1.5 mm thickness) were fabricated from six types of A2 MT ceramic: heat-pressed and milled glass-ceramic (feldspathic, lithium disilicate and zirconia reinforced lithium silicate). The samples were obtained respecting the manufacturer’s instructions. The resulted surfaces (n = 96) were half glazed and half polished. The samples were subjected to thermocycling (10,000 cycles) and roughness values (Ra and Rz), colour coordinates (L*, a*, b*) and microstructural analyses were assessed before and after thermocycling. Translucency (TP) and opalescence (OP) were calculated. Values were statistically analysed using ANOVA test (one way). TP and OP values were significantly different between heat-pressed and milled ceramics before and also after thermocycling (p < 0.001). Surface treatments (glazing and polishing) had a significant effect on TP and OP and surface roughness (p < 0.05). The heat-pressed and milled zirconia reinforced lithium silicate glass-ceramic experienced a loss in TP and OP. Ra and Rz increased for the glazed samples, TP and OP decreased for all the samples after thermocycling. Microstructural analyse revealed that glazed surfaces were more affected by the thermocycling and especially for the zirconia reinforced lithium silicate ceramic. Optical properties and surface roughness of the chosen ceramic materials were affected by thermocycling, surface treatments and microstructural differences. The least affected of the ceramics was the lithium disilicate ceramic heat-pressed polished and glazed.


Author(s):  
O.V. Savvova ◽  
G.K. Voronov ◽  
O.I. Fesenko ◽  
Yu.O. Smirnova ◽  
E. Bairamov

The need to improve the level of dental health of the population of Ukraine was identified. The prospects for the use of ceramic prostheses to provide quality medical care in dentistry have been established. An analytical review of various types of ceramic and glass-ceramic materials used as dental prostheses for tooth replacement: porcelain, alumina, zirconium oxide, glass-ceramics based on leucite and lithium disilicate and mica with the addition of fluorides. Peculiarities of the structure and operational properties of ceramic and glass-ceramic materials for dentistry have been identified, their advantages and disadvantages have been established. The effectiveness of the use of glass-ceramic materials based on lithium disilicate for dental prosthetics is substantiated. The basic lithium silicate system was selected and glasses for obtaining glass-ceramic crowns based on lithium disilicate by the method of high-temperature pressing and calcium phosphate-silicate system for obtaining glass-ceramic coatings were synthesized. The methodological approach to the development of glass-ceramic prostheses based on lithium disilicate is determined. The limits of the compositions of oxide components are determined and raw materials for the synthesis of the glass matrix are selected. The technological parameters of melting (T = 1350 – 1400ºС) and heat treatment with simultaneous formation of products (stage of nucleation T = 600 – 650ºС, τ = 30 – 60 min; stages of formation T = 900ºС, τ ≈ 20 min) are selected. The composition of fluoroapatite glass-ceramic coating for glazing of glass-ceramics and the mode of its firing (T = 800 – 850ºС, τ ≈ 1,0 – 1,5 min) were determined. The serviceability of the developed glass-ceramic samples DL st.glass, which were obtained by the technology of high-temperature pressing, are determined. The comparative analysis of glass-ceramic prostheses for dentistry allowed to establish that the operational properties of the developed glass-ceramic prostheses according to ISO 6872:2015 are at the level of world analogues. This will allow them to successfully compete in the Ukrainian market with well-known foreign counterparts and help ensure the social priorities of the state in the field of health care.


2019 ◽  
Vol 45 (4) ◽  
pp. 442-452 ◽  
Author(s):  
N Ilie ◽  
G Furtos

Clinical Relevance Light transmission through dental materials and tooth structure has direct clinical implication on such factors as selecting an appropriate curing technique during a restorative process. SUMMARY Introduction: This study aims to quantify and compare the amount of light that passes through seven different types of direct and indirect restorative materials comprising light-cured resin based composites (regular and bulk-fill), computer-aided design/computer-aided manufacturing (CAD/CAM) restoratives such as resin based composites, poly(methyl methacrylate) (PMMA) resin, leucite glass-ceramic, lithium silicate glass-ceramic, feldspar ceramic, and the natural tooth structure. Methods and Materials: Individual sets (n=6) of plane-parallel test specimens (2 mm) of 32 restorative materials belonging to the aforementioned seven material types and the tooth structure were prepared. Within the analyzed materials, one leucite glass-ceramic and one lithium disilicate glass-ceramic were considered in two different translucencies. In addition, two light-cured resin composites, one CAD/CAM resin composite, and one lithium disilicate glass-ceramic were considered in two different shades. Optical properties (transmittance, T; absorbance, A; and opacity, O) of each material were calculated from the relationship between incident and transmitted irradiance [I(d)] using a violet-blue light-curing unit. Incident and transmitted irradiance were assessed in real time on a spectrophotometer. A multivariate analysis (general linear model) assessed the effects of various parameters on the optical properties. Results: A very strong influence of the parameter material was identified on I(d) (p&lt;0.001; partial eta squared, ηP2=0.953), T (p&lt;0.001; ηP2=0.951), A (p&lt;0.001; ηP2=0.925), and O (p&lt;0.001; ηP2=0.886), while the effect of the parameter material type was not significant (p=0.079, p=0.05, p=0.05, and p=0.051, respectively). Light attenuation differed significantly by material within each shade category and by shade category within the analyzed material. Conclusions: Attenuation of light through restorative materials and tooth structure is high (59.9% to 94.9%); thus, deficits in polymerization are difficult to compensate for by additional light exposure at the end of the restorative process.


2018 ◽  
Vol 12 (3) ◽  
pp. 391-399 ◽  
Author(s):  
Оksana Savvova ◽  
◽  
Gennadii Voronov ◽  
Vitalii Topchyi ◽  
Yuliya Smyrnova ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document