scholarly journals Applying Nanoparticle Tracking Analysis to Characterize the Polydispersity of Aggregates Resulting from Tannin–Polysaccharide Interactions in Wine-Like Media

Molecules ◽  
2019 ◽  
Vol 24 (11) ◽  
pp. 2100 ◽  
Author(s):  
Sijing Li ◽  
Kerry L. Wilkinson ◽  
Agnieszka Mierczynska-Vasilev ◽  
Keren A. Bindon

Interactions between grape seed tannin and either a mannoprotein or an arabinogalactan in model wine solutions of different ethanol concentrations were characterized with nanoparticle tracking analysis (NTA), UV-visible spectroscopy and dynamic light scattering (DLS). NTA results reflected a shift in particle size distribution due to aggregation. Furthermore, the light scattering intensity of each tracked particle measured by NTA demonstrated the presence of aggregates, even when a shift in particle size was not apparent. Mannoprotein and arabinogalactan behaved differently when combined with seed tannin. Mannoprotein formed large, highly light-scattering aggregates, while arabinogalactan exhibited only weak interactions with seed tannin. A 3% difference in alcohol concentration of the model solution (12 vs. 15% v/v) was sufficient to affect the interactions between mannoprotein and tannin when the tannin concentration was high. In summary, this study showed that NTA is a promising tool for measuring polydisperse samples of grape and wine macromolecules, and their aggregates under wine-like conditions. The implications for wine colloidal properties are discussed based on these results.

2015 ◽  
Vol 37 (1) ◽  
pp. 49-53 ◽  
Author(s):  
Tomasz Śliwa ◽  
Maciej Jarzębski ◽  
Kosma Szutkowski

The most popular technique for particle size characterization is the dynamic light scattering (DLS). In recent years new advanced method based on counting each single particle movement was introduced giving perspective for measurement of each component of mixture. This study presents some advantages of nanoparticle tracking analysis (NTA) method in comparison to DLS. For tests standard polystyrene beds were chosen vary diameter of 22, 61 and 150 nm and its mixtures. Experiments showed that the particles size resolution allows to distinguish each population in two population suspension opposed to DLS. The NTA method permits to eliminate the negative effects i.e. dust or aggregates in sample during post processing, that permits to use it in a variety of studies.


1997 ◽  
Author(s):  
Gorden Videen ◽  
Paul Pellegrino ◽  
Dat Ngo ◽  
John S. Videen ◽  
Ronald G. Pinnick

2021 ◽  
Author(s):  
Dillip Kumar Mohapatra ◽  
Philip James Camp ◽  
John Philip

We probe the influence of particle size polydispersity on field-induced structures and structural transitions in magnetic fluids (ferrofluids) using phase contrast optical microscopy, light scattering and Brownian dynamics simulations. Three...


Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2094
Author(s):  
Seok-Ki Jung ◽  
Dae Woon Kim ◽  
Jeongyol Lee ◽  
Selvaponpriya Ramasamy ◽  
Hyun Sik Kim ◽  
...  

The aim of this study was to present a control method for modulating the translucency of lithium disilicate ceramics through thermal refinement. Identical lithium disilicate blocks were thermally refined using four different heat treatment schedules, and the microstructure, translucency, and flexural strength of the ceramics were investigated in detail by SEM, spectroscopy, and a piston-on-three-ball test. The results showed that ceramics treated under higher heat had larger grains, with an average size between 240 and 1080 nm. In addition, a higher transmittance of all wavelengths was observed in ceramics treated under lower heat, and the transmittance in the 550 nm wavelength ranged from 27 to 34%. The results suggest that the translucency of ceramics can be modified through thermal refinement under two conditions: (1) the particle size of the ceramic is small enough to achieve minimal grain-boundary light scattering, and (2) the percentage of particles allowing visible light transmission is altered by the heat treatment.


Sign in / Sign up

Export Citation Format

Share Document