scholarly journals The Evidence of Decisive Effect of Both Surface Microstructure and Speciation of Chalcopyrite on Attachment Behaviors of Extreme Thermoacidophile Sulfolobus metallicus

Minerals ◽  
2018 ◽  
Vol 8 (4) ◽  
pp. 159 ◽  
Author(s):  
Weibo Ling ◽  
Lei Wang ◽  
Hongchang Liu ◽  
Zhenyuan Nie ◽  
Yun Yang ◽  
...  
Keyword(s):  
Surface Microstructure ◽  
Decisive Effect

Preparation of Backthinned Ceramic Specimens

1985 ◽  
Vol 43 ◽  
pp. 182-183
Author(s):  
A. T. Fisher ◽  
P. Angelini
Keyword(s):  
Electron Microscopy ◽  
Analytical Electron Microscopy ◽  
Vacuum System ◽  
Back Surface ◽  
Surface Microstructure ◽  
Ion Milling ◽  
Near Surface ◽  
Depth Profiles ◽  
Analytical Electron ◽  
Ion Implanted

Analytical electron microscopy (AEM) of the near surface microstructure of ion implanted ceramics can provide much information about these materials. Backthinning of specimens results in relatively large thin areas for analysis of precipitates, voids, dislocations, depth profiles of implanted species and other features. One of the most critical stages in the backthinning process is the ion milling procedure. Material sputtered during ion milling can redeposit on the back surface thereby contaminating the specimen with impurities such as Fe, Cr, Ni, Mo, Si, etc. These impurities may originate from the specimen, specimen platform and clamping plates, vacuum system, and other components. The contamination may take the form of discrete particles or continuous films [Fig. 1] and compromises many of the compositional and microstructural analyses. A method is being developed to protect the implanted surface by coating it with NaCl prior to backthinning. Impurities which deposit on the continuous NaCl film during ion milling are removed by immersing the specimen in water and floating the contaminants from the specimen as the salt dissolves.

Surface Microstructure Evolution Upon Silicidation of Ni(Pt) and the Different Responses to Metal Etch

2013 ◽  
Author(s):  
Wentao Qin ◽  
Dorai Iyer ◽  
Jim Morgan ◽  
Carroll Casteel ◽  
Robert Watkins ◽  
...  
Keyword(s):  
Thin Film ◽  
Oxide Film ◽  
Microstructure Evolution ◽  
Depth Profiling ◽  
Surface Microstructure ◽  
The Difference ◽  
Surface Microstructures ◽  
Pt Films

Abstract Ni(5 at.%Pt ) films were silicided at a temperature below 400 °C and at 550 °C. The two silicidation temperatures had produced different responses to the subsequent metal etch. Catastrophic removal of the silicide was seen with the low silicidation temperature, while the desired etch selectivity was achieved with the high silicidation temperature. The surface microstructures developed were characterized with TEM and Auger depth profiling. The data correlate with both silicidation temperatures and ultimately the difference in the response to the metal etch. With the high silicidation temperature, there existed a thin Si-oxide film that was close to the surface and embedded with particles which contain metals. This thin film is expected to contribute significantly to the desired etch selectivity. The formation of this layer is interpreted thermodynamically.

scholarly journals A Comparative Study of Acicular Ferrite Transformation Behavior between Surface and Interior in a Low C–Mn Steel by HT-LSCM

Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 699
Author(s):  
Xiaojin Liu ◽  
Guo Yuan ◽  
Raja. Devesh Kumar Misra ◽  
Guodong Wang
Keyword(s):  
Grain Boundaries ◽  
Cooling Rate ◽  
Acicular Ferrite ◽  
Laser Scanning ◽  
Sample Surface ◽  
Surface Microstructure ◽  
In Situ Observation ◽  
Low Carbon ◽  
Transformation Behavior ◽  
Ferrite Transformation

In this study, the acicular ferrite transformation behavior of a Ti–Ca deoxidized low carbon steel was studied using a high-temperature laser scanning confocal microscopy (HT-LSCM). The in situ observation of the transformation behavior on the sample surface with different cooling rates was achieved by HT-LSCM. The microstructure between the surface and interior of the HT-LSCM sample was compared. The results showed that Ti–Ca oxide particles were effective sites for acicular ferrite (AF) nucleation. The start transformation temperature at grain boundaries and intragranular particles decreased with an increase in cooling rate, but the AF nucleation rate increased and the surface microstructure was more interlocked. The sample surface microstructure obtained at 3 °C/s was dominated by ferrite side plates, while the ferrite nucleating sites transferred from grain boundaries to intragranular particles when the cooling rate was 15 °C/s. Moreover, it was interesting that the microstructure and microhardness of the sample surface and interior were different. The AF dominating microstructure, obtained in the sample interior, was much finer than the sample surface, and the microhardness of the sample surface was much lower than the sample interior. The combined factors led to a coarse size of AF on the sample surface. AF formed at a higher temperature resulted in the coarse size. The available particles for AF nucleation on the sample surface were quite limited, such that hard impingement between AF plates was much weaker than that in the sample interior. In addition, the transformation stress in austenite on the sample surface could be largely released, which contributed to a coarser AF plate size. The coarse grain size, low dislocation concentration and low carbon content led to lower hardness on the sample surface.

Study of phase transformation and surface microstructure of alumina ceramic under irradiation of intense pulsed ion beam

Vacuum ◽  
2021 ◽  
Vol 187 ◽  
pp. 110154
Author(s):  
Shijian Zhang ◽  
Xiao Yu ◽  
Jie Zhang ◽  
Jie Shen ◽  
Haowen Zhong ◽  
...  
Keyword(s):  
Phase Transformation ◽  
Ion Beam ◽  
Alumina Ceramic ◽  
Surface Microstructure

Spindle-Shaped Surface Microstructure Inspired by Directional Water Collection Biosystems to Enhance Interfacial Wetting and Bonding Strength

2021 ◽  
Vol 13 (11) ◽  
pp. 13760-13770
Author(s):  
Hailang Wan ◽  
Junying Min ◽  
Blair E. Carlson ◽  
Jianping Lin ◽  
Chengcheng Sun
Keyword(s):  
Bonding Strength ◽  
Surface Microstructure ◽  
Shaped Surface ◽  
Water Collection
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