scholarly journals Deformation Features of Super-Deep Diamonds

Minerals ◽  
2019 ◽  
Vol 10 (1) ◽  
pp. 18 ◽  
Author(s):  
Alexey Ragozin ◽  
Dmitry Zedgenizov ◽  
Vladislav Shatsky ◽  
Konstantin Kuper ◽  
Hiroyuki Kagi

The paper presents new data on the internal structure of super-deep (sublithospheric) diamonds from Saõ-Luiz river placers (Brazil) and from alluvial placers of the northeastern Siberian platform (Yakutia). The sublithospheric origin of these diamonds is supported by the presence of mineral inclusions corresponding to associations of the transition zone and lower mantle. The features of morphology and internal structure have been studied by optical and scanning electron microscopy (SEM), cathodoluminescence topography (CL), and electron backscatter diffraction (EBSD) techniques. Diamonds typically have complicated growth histories displaying alternating episodes of growth, dissolution, and post-growth deformation and crushing processes. Most crystals have endured both plastic and brittle deformation during the growth history. Abundant deformation and resorption/growth features suggest a highly dynamic growth environment for super-deep diamonds. High temperatures expected in the transition zone and lower mantle could explain the plastic deformations of super-deep diamonds with low nitrogen content.

2016 ◽  
Vol 49 (6) ◽  
pp. 2145-2154 ◽  
Author(s):  
Chang Xu ◽  
Shan-Rong Zhao ◽  
Chuan Li ◽  
Xu He

Twins in plagioclase, which are abundant in rocks, have important implications for the growth history and subsequent transformation. There are many twin laws in plagioclase and some of them are difficult to identify. This paper presents an electron backscatter diffraction (EBSD) analysis combined with electron microprobe analysis of plagioclase twinning in the Niutoushan alkali basalt. Theoretical pole figures of 12 different twin laws for plagioclase were generated. By comparing the pole figures obtained from EBSD with the theoretical ones, 11 twin laws have been identified in the alkali basalt, and their frequency has also been determined: Albite (28%), Carlsbad (25%), Albite–Carlsbad (34%), Pericline (3%), Ala (2%), Manebach (1%), Albite–Ala (1%), Prism {110} (2%), Prism {1\bar 10} (1%), Prism {130} (1%) and Prism {1\bar 30} (1%). All the plagioclase twins in the alkali basalt are growth twins. The anorthite content of the plagioclase has a negative correlation with the frequency of the Pericline and Albite twin laws but a positive correlation with the frequency of all the other twin laws, which is consistent with previous results. The theoretical pole figures of twin laws for plagioclase introduced in this paper can be applied to investigating plagioclase twin laws in all plagioclase-bearing rocks, and the relationship between twin pattern and crystallization conditions of the rocks can be established.


Geology ◽  
2021 ◽  
Author(s):  
Sanna Holm-Alwmark ◽  
Timmons M. Erickson ◽  
Aaron J. Cavosie

Little is known about the microstructural behavior of magnetite during hypervelocity impact events, even though it is a widespread accessory mineral and an important magnetic carrier in terrestrial and extraterrestrial rocks. We report systematic electron backscatter diffraction crystallographic analysis of shock features in magnetite from a transect across the 52-km-diameter ca. 380 Ma Siljan impact structure in Sweden. Magnetite grains in granitoid samples contain brittle fracturing, crystal-plasticity, and lamellar twins. Deformation twins along {111} with shear direction of <112> are consistent with spinel-law twins. Inferred bulk shock pressures for the investigated samples, as constrained by planar deformation features (PDFs) in quartz and shock twins in zircon, range from 0 to 20 GPa; onset of shock-induced twinning in magnetite is observed at >5 GPa. These results highlight the utility of magnetite to record shock deformation in rocks that experience shock pressures >5 GPa, which may be useful in quartz-poor samples. Despite significant hydrothermal alteration and the variable transformation of host magnetite to hematite, shock effects are preserved, which demonstrates that magnetite is a reliable mineral for preserving shock deformation over geologic time.


Author(s):  
Aaron J. Cavosie ◽  
Luigi Folco

ABSTRACT With an age of less than ~5000 yr and a diameter of 45 m, Kamil crater in Egypt is one of the youngest and smallest terrestrial impact craters known to date. Abundant evidence of shock-deformed sandstone has been reported from Kamil crater, including shatter cones, vesicular impact glass, high-pressure polymorphs of silica and car bon, planar deformation features (PDFs) and planar fractures (PFs) in quartz, dissociated zircon, melt veins, and intergranular melt, giving rise to a range of estimated shock pressures from ~20 to ~60 GPa. Here, we investigated shocked zircon from Kamil crater through characterization of microstructures in a centimeter-sized clast of shocked nonporous sandstone ejecta, previously described as containing quartz grains with PDFs and PFs, coesite, stishovite, diamond, and lechatelierite. Orientation analysis by electron backscatter diffraction (EBSD) showed that the quartz arenite consists of damaged detrital quartz grains surrounded by a matrix of either comminuted quartz or intergranular melt. Individual quartz grains are pervasively fractured (abundant PFs and PDFs); apparent isotropic crushing resulted in uniformly and highly dispersed orientation clusters on pole figures. Zircon grains are not abundant; however, four of 19 grains analyzed by EBSD contained {112} deformation twin lamellae, with individual lamellae ranging in length from 1 to 2 µm. Lengths of twin lamellae in Kamil zircon grains are anomalously short compared to those report-ed in shocked zircon from other impact structures, where individual lamellae are tens of micrometers long. Previous empirical studies have suggested that {112} twin lamellae in zircon form at ~20 GPa in non-porous target rocks, a finding supported by their coexistence, in some impactites, with high-pressure phases such as reidite. The only available experimental constraint, by diamond anvil cell, found {112} twins in zircon powder quenched at 20 GPa. The presence of coesite, stishovite, lechatelierite, and shocked quartz with PDFs in the studied sample is consistent with empirically derived pressure estimates of ~20 GPa for {112} twin formation in zircon in the ejecta sample from Kamil crater. Kamil thus represents the smallest and youngest impact structure where shock-twinned zircon has been reported. Given the apparent efficiency of {112} twin formation (21% of grains), shock-twinned zircon is here shown to provide a robust and readily identifiable record of shock deformation in a relatively common mineral at one of the smallest known terrestrial impact craters.


Author(s):  
Frank Altmann ◽  
Jens Beyersdorfer ◽  
Jan Schischka ◽  
Michael Krause ◽  
German Franz ◽  
...  

Abstract In this paper the new Vion™ Plasma-FIB system, developed by FEI, is evaluated for cross sectioning of Cu filled Through Silicon Via (TSV) interconnects. The aim of the study presented in this paper is to evaluate and optimise different Plasma-FIB (P-FIB) milling strategies in terms of performance and cross section surface quality. The sufficient preservation of microstructures within cross sections is crucial for subsequent Electron Backscatter Diffraction (EBSD) grain structure analyses and a high resolution interface characterisation by TEM.


2020 ◽  
Vol 837 ◽  
pp. 41-45
Author(s):  
Shuai Sun ◽  
Kai Hua Liu

In order to determine the evolution features of deformation twins for TA2 commercial pure titanium (cp-TA2), the TA2 samples were bent under different bending angles in three-point bending tests via a universal testing machine. The electron backscatter diffraction (EBSD) technique was applied to identify the grain boundaries (GBs) and twin boundaries (TBs) in the bending areas. The results reveal that the type of deformation area would effect the evolution of different deformation twins. It is inferred that the state of stress would promote the multiplication of the same type of deformation twins.


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