scholarly journals Superplastic Behavioral Characteristics of Fine-Grained 5A70 Aluminum Alloy

Metals ◽  
2019 ◽  
Vol 9 (1) ◽  
pp. 62 ◽  
Author(s):  
Sheng Li ◽  
Zhongguo Huang ◽  
Shunyao Jin
Keyword(s):  
Grain Boundaries ◽  
Electron Backscatter Diffraction ◽  
Energy Dispersive Spectrometer ◽  
Rate Sensitivity ◽  
Alloy Sheet ◽  
Second Phase ◽  
Fine Grained ◽  
Transmission Electron ◽  
Average Grain Size ◽  
The Matrix

A fine-grained 5A70 alloy sheet was obtained through a combination of rolling and heat treatment, with a total deformation reduction of 90% and an average grain size of 8.48 μm. The alloy was studied at 400, 450, 500, and 550 °C and exhibited excellent elongation-to-failures of 205, 321, 398, and 437% with coefficients for the strain rate sensitivity of 0.42, 0.40, 0.47 and 0.46, respectively. Electron backscatter diffraction (EBSD) results revealed that the massive grain boundaries were high angle boundaries, suggesting that boundary sliding and grain rotation occurred during superplastic deformation. The X-ray diffraction (XRD) and energy dispersive spectrometer (EDS) results indicated that the compositions were the Al6(MnFe) and Mg-rich phase particles of the deformed 5A70 alloy. In addition, the weakening of the pinning effect led to abnormal grain growth at 500 and 550 °C, resulting in strain hardening. Transmission electron microscopy (TEM) examinations demonstrated that the applied stress at the head of the precipitated particles and/or grain boundaries exceeded the matrix-structure-promoted cavity nucleation. Cavities grew, interlinked, and coalesced, which resulted in crack formation that eventually led to superplastic fractures. Filaments formed at the fracture surfaces because of second phase precipitation at grain boundaries and the formation of Mg-rich oxides.

scholarly journals Kinetics of Austenite Grain Growth during a Continuous Heating of a Niobium Microalloyed Steel

2004 ◽  
Vol 467-470 ◽  
pp. 929-934 ◽  
Author(s):  
David San Martín ◽  
Francisca García Caballero ◽  
Carlos Capdevila ◽  
C. Carcía de Andrés
Keyword(s):  
Grain Size ◽  
Grain Boundaries ◽  
Heating Rate ◽  
Grain Growth ◽  
Continuous Heating ◽  
Second Phase ◽  
Austenite Grain Size ◽  
Austenite Grain ◽  
Average Grain Size ◽  
The Matrix

Grain growth is a thermally activated process in which the average grain size increases as temperature and time increases. The driving force for grain growth results from the decrease in the free energy associated with the reduction in total grain boundary energy. There are several known factors that influence the migration of grain boundaries such as second phase particles precipitated in the matrix and the solute elements segregated at grain boundaries. The austenite grain boundaries are revealed using the thermal etching method. Carbon extraction replicas were prepared to determine the composition and size of precipitates present in the matrix. In this work, the evolution of the average prior austenite grain size (PAGS) of a low carbon steel microalloyed with niobium is studied as a function of temperature and heating rate. Austenite grains show a two-stage growth. It has been found that as heating rate increases, the grain coarsening temperature (TGC) increases and the grain size at that temperature decreases. TGC temperature lies around 40-60°C below the temperature for complete dissolution of carbonitrides (TDISS).

scholarly journals Study of Deformation Behavior and Microstructural Evolution in Multiphase Steel

Materials ◽  
2018 ◽  
Vol 11 (11) ◽  
pp. 2285 ◽  
Author(s):  
Jun Lu ◽  
Hao Yu ◽  
Xiaoni Duan ◽  
Chenghao Song
Keyword(s):  
High Performance ◽  
Tensile Deformation ◽  
Electron Backscatter Diffraction ◽  
Bainitic Ferrite ◽  
Tensile Tests ◽  
Dislocation Configuration ◽  
Transmission Electron ◽  
Average Grain Size ◽  
The Matrix ◽  
Multiphase Steel

In the present work, the tensile deformation characteristics of the high performance multiphase steel with complex microstructures are investigated. A mixture of ferrite, bainite, and 14.4 vol% retained austenite (RA) with an average grain size of less than 3 μm of the matrix is obtained after specific heat treatment. Tensile tests are performed with increasing strain, i.e., 0%, 5%, 10%, 15%, and 20%. Then X-ray diffraction, transmission electron microscope and electron backscatter diffraction are utilized to analyze the deformation-transformation behaviors of the complex microstructures. Phase transformation of the RA, which is controlled by its morphology and distribution, contributes to high strain hardening capacity of the steel. The blocky-type RA that locates in ferrite grain boundaries shows less stability and transforms easily at early deformation stage, while the film-like RA that distributes between bainitic ferrite shows higher stability and transforms continuously throughout plastic deformation. Moreover, the substructure formation by dislocation configuration in ferrite grains begins with randomly distributed dislocations and ends up with cellular structures, resulting in ferrite subdivision during deformation and also grain refinement strengthening. As a result, the experimental steel is reinforced not only by the martensite transformation of RA, but also ferrite refinement.

scholarly journals Oxygen Induced Phase Transformation in TC21 Alloy with a Lamellar Microstructure

Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 163
Author(s):  
Shu Wang ◽  
Yilong Liang ◽  
Hao Sun ◽  
Xin Feng ◽  
Chaowen Huang
Keyword(s):  
Electron Microscopy ◽  
Phase Transformation ◽  
Oxygen Uptake ◽  
Titanium Alloys ◽  
Electron Backscatter Diffraction ◽  
Lamellar Microstructure ◽  
Α Phase ◽  
Transmission Electron ◽  
The Matrix ◽  
Oxygen Ingress

The main objective of the present study was to understand the oxygen ingress in titanium alloys at high temperatures. Investigations reveal that the oxygen diffusion layer (ODL) caused by oxygen ingress significantly affects the mechanical properties of titanium alloys. In the present study, the high-temperature oxygen ingress behavior of TC21 alloy with a lamellar microstructure was investigated. Microstructural characterizations were analyzed through optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and transmission electron microscopy (TEM). Obtained results demonstrate that oxygen-induced phase transformation not only enhances the precipitation of secondary α-phase (αs) and forms more primary α phase (αp), but also promotes the recrystallization of the ODL. It was found that as the temperature of oxygen uptake increases, the thickness of the ODL initially increases and then decreases. The maximum depth of the ODL was obtained for the oxygen uptake temperature of 960 °C. In addition, a gradient microstructure (αp + β + βtrans)/(αp + βtrans)/(αp + β) was observed in the experiment. Meanwhile, it was also found that the hardness and dislocation density in the ODL is higher than that that of the matrix.

Recrystallization in Ultra-Fine Grain Structures of AA3104 Alloy Processed by ECAP and HPT

2012 ◽  
Vol 715-716 ◽  
pp. 346-353
Author(s):  
H. Paul ◽  
T. Baudin ◽  
K. Kudłacz ◽  
A. Morawiec
Keyword(s):  
High Pressure Torsion ◽  
Deformation Mode ◽  
Second Phase ◽  
Orientation Measurement ◽  
Angular Pressing ◽  
Second Phase Particles ◽  
Average Grain Size ◽  
The Matrix ◽  
Electron Microscopes ◽  
Different Strains

The objective of this study was to determine the effect of deformation mode on recrystallization behavior of severely deformed material. Commercial purity AA3104 aluminum alloy was deformed via high pressure torsion and equal channel angular pressing to different strains and then annealed to obtain the state of partial recrystallization. The microstructure and the crystallographic texture were analysed using scanning and transmission electron microscopes equipped with orientation measurement facilities. The nucleation of new grains was observed in bulk recrystallized samples and during in-situ recrystallization in the transmission microscope. Irrespective of the applied deformation mode, a large non-deformable second phase particles strongly influenced strengthening of the matrix through deformation zones around them. It is known that relatively high stored energy stimulates the nucleation of new grains during the recrystalization. In most of the observed cases, the growth of recrystallized grains occurred by the coalescence of neighboring subcells. This process usually led to nearly homogeneous equiaxed grains of similar size. The diameter of grains in the vicinity of large second phase particles was only occasionally significantly larger than the average grain size. Large grains were most often observed in places far from the particles. TEM orientation mapping from highly deformed zones around particles showed that orientations of new grains were not random and only strictly defined groups of orientations were observed.

High Strain Rate Superplasticity in a Zr and Sc Modified 7075 Aluminum Alloy Produced by ECAP

2008 ◽  
Vol 584-586 ◽  
pp. 164-169 ◽  
Author(s):  
Krystof Turba ◽  
Premysl Malek ◽  
Edgar F. Rauch ◽  
Miroslav Cieslar
Keyword(s):  
Aluminum Alloy ◽  
High Strain Rate ◽  
Strain Rate ◽  
High Strain ◽  
Rate Sensitivity ◽  
7075 Aluminum Alloy ◽  
Fine Grained ◽  
Angular Pressing ◽  
Average Grain Size ◽  
Elongation To Failure

Equal-channel angular pressing (ECAP) at 443 K was used to introduce an ultra-fine grained (UFG) microstructure to a Zr and Sc modified 7075 aluminum alloy. Using the methods of TEM and EBSD, an average grain size of 0.6 1m was recorded after the pressing. The UFG microstructure remained very stable up to the temperature of 723 K, where the material exhibited high strain rate superplasticity (HSRSP) with elongations to failure of 610 % and 410 % at initial strain rates of 6.4 x 10-2 s-1 and 1 x 10-1 s-1, respectively. A strain rate sensitivity parameter m in the vicinity of 0.45 was observed at temperatures as high as 773 K. At this temperature, the material still reached an elongation to failure of 430 % at 2 x 10-2 s-1. These results confirm the stabilizing effect of the Zr and Sc additions on the UFG microstructure in a 7XXX series aluminum alloy produced by severe plastic deformation.

Microstructure and mechanical properties of 15-5 PH stainless steel under different aging temperature

2021 ◽  
Vol 118 (6) ◽  
pp. 601
Author(s):  
Chunhui Jin ◽  
Honglin Zhou ◽  
Yuan Lai ◽  
Bei Li ◽  
Kewei Zhang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Stainless Steel ◽  
Aging Temperature ◽  
Electron Backscatter Diffraction ◽  
Lath Martensite ◽  
Optical Microscope ◽  
Second Phase ◽  
Strengthening Mechanisms ◽  
Microstructure And Mechanical Properties ◽  
Transmission Electron

The influence of aging temperature on microstructure and mechanical properties of Cr15Ni5 precipitation hardening stainless steel (15-5 PH stainless steel) were investigated at aging temperature range of 440–610 °C. The tensile properties at ambient temperature of the 15-5 PH stainless steel processed by different aging temperatures were tested, and the microstructural features were further analyzed utilizing optical microscope (OM), transmission electron microscope (TEM), electron backscatter diffraction (EBSD) as well as X-ray diffraction (XRD), respectively. Results indicated the strength of the 15-5 PH stainless steel was firstly decreased with increment of aging temperature from 440 to 540 °C, and then increased with the increment of aging temperature from 540 to 610 °C. The strength and ductility were well matched at aging temperature 470 °C, and the yield strength, tensile strength as well as elongation were determined to be 1170 MPa, 1240 MPa and 24%, respectively. The microstructures concerning to different aging temperatures were overall confirmed to be lath martensite. The strengthening mechanisms induced by dislocation density and the second phase precipitation of Cu-enriched metallic compound under different aging temperatures were determined to be the predominant strengthening mechanisms controlling the variation trend of mechanical properties corresponding to different aging temperatures with respect to 15-5 PH stainless steel.

Microstructure of Friction Stir Processed Mg-Y-Zn Alloy

2007 ◽  
Vol 558-559 ◽  
pp. 777-780 ◽  
Author(s):  
Taiki Morishige ◽  
Masato Tsujikawa ◽  
Sung Wook Chung ◽  
Sachio Oki ◽  
Kenji Higashi
Keyword(s):  
Equal Channel Angular Extrusion ◽  
Second Phase ◽  
Ingot Metallurgy ◽  
Friction Stir ◽  
Fine Grained ◽  
Probe Diameter ◽  
Fine Grain ◽  
Second Phase Particles ◽  
The Matrix ◽  
Zn Alloy

Friction stir processing (FSP) is the effective method of the grain refinement for light metals. The aim of this study is to acquire the fine grained bulk Mg-Y-Zn alloy by ingot metallurgy route much lower in cost. Such bulk alloy can be formed by the superplastic forging. The microstructure of as-cast Mg-Y-Zn alloy was dendrite. The dendrite arm spacing was 72.5 [(m], and there are the lamellar structures in it. FSP was conducted on allover the plate of Mg-Y-Zn alloy for both surfaces by the rotational tool with FSW machine. The stirring passes were shifted half of the probe diameter every execution. The dendrite structures disappeared after FSP, but the lamellar structure could be observed by TEM. The matrix became recrystallized fine grain, and interdendritic second phase particles were dispersed in the grain boundaries. By using FSP, cast Mg-Y-Zn alloy could have fine-grained. This result compared to this material produced by equal channel angular extrusion (ECAE) or rapid-solidified powder metallurgy (RS P/M). As the result, as-FSPed material has the higher hardness than materials produced by the other processes at the similar grain size.

scholarly journals Investigation of Primary Recrystallization and Decarbonization with Different Heating Rates of Intermediate Annealing Using Nb-Containing Grain-Oriented Silicon Steel

Metals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1655
Author(s):  
Xin Tian ◽  
Shuang Kuang ◽  
Jie Li ◽  
Jing Guo ◽  
Yunli Feng
Keyword(s):  
Heating Rate ◽  
Electron Backscatter Diffraction ◽  
Optical Microscope ◽  
Primary Recrystallization ◽  
Silicon Steel ◽  
Intermediate Annealing ◽  
Heating Rates ◽  
Average Grain Size ◽  
The Matrix ◽  
20 Nm

An Nb-containing grain-oriented silicon steel was produced through double-stage cold rolling in order to investigate the effect of the heating rate during intermediate annealing on primary recrystallization and decarburization behavior. The microstructure and texture were observed and analyzed by an optical microscope and an electron backscatter diffraction system. A transmission electron microscope was used to observe the precipitation behavior of inhibitors. The decarburization effect during intermediate annealing was also calculated and discussed. The results show that primary recrystallization takes place after intermediate annealing. As the heating rate increases, the average grain size decreases gradually. The textures of {411}<148> and {111}<112> were found to be the strongest along the thickness direction in all of the annealed specimens and are mainly surrounded by HEGB and HAGB (> 45°). A large number of inhibitors with the size of 14~20 nm precipitate are distributed evenly in the matrix. The above results indicate that the higher heating rate during intermediate annealing contributes to both an excellent microstructure and magnetic properties. From the calculation, as the heating rate increases, decarbonization tends to proceed in the insulation stage, and the total amount of carbonization declines.

scholarly journals Study on σ Phase in Fe–Al–Cr Alloys

Metals ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 1092 ◽  
Author(s):  
Jintao Wang ◽  
Shouping Liu ◽  
Xiaoyu Han
Keyword(s):  
Mechanical Properties ◽  
Grain Boundaries ◽  
Grain Growth ◽  
Thermodynamic Calculation ◽  
Second Phase ◽  
Σ Phase ◽  
Austenitic Transformation ◽  
The Matrix ◽  
The Relationship

In this paper, a method of using the second phase to control the grain growth in Fe–Al–Cr alloys was proposed, in order to obtain better mechanical properties. In Fe–Al–Cr alloys, austenitic transformation occurs by adding austenitizing elements, leading to the formation of the second phase and segregation at the grain boundaries, which hinders grain growth. FeCr(σ) phase was obtained in the Fe–Al–Cr alloys, which had grains of several microns and was coherent and coplanar with the matrix (Fe2AlCr). The nucleation of σ phase in Fe–Al–Cr alloy was controlled by the ratio of nickel to chromium. When the Ni/Cr (eq) ratio of alloys was more than 0.19, σ phase could nucleate in Fe–Al–Cr alloy. The relationship between austenitizing and nucleation of FeCr(σ) phase was given by thermodynamic calculation.

scholarly journals Coupling Automated Electron Backscatter Diffraction with Transmission Electron and Atomic Force Microscopies

2000 ◽  
Vol 6 (S2) ◽  
pp. 940-941
Author(s):  
A.J. Schwartz ◽  
M. Kumar ◽  
P.J. Bedrossian ◽  
W.E. King
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Thermomechanical Processing ◽  
Electron Backscatter Diffraction ◽  
Grain Boundary Character Distribution ◽  
Atomic Force ◽  
Transmission Electron ◽  
Electron Backscatter ◽  
Network Engineering ◽  
Backscatter Diffraction

Grain boundary network engineering is an emerging field that encompasses the concept that modifications to conventional thermomechanical processing can result in improved properties through the disruption of the random grain boundary network. Various researchers have reported a correlation between the grain boundary character distribution (defined as the fractions of “special” and “random” grain boundaries) and dramatic improvements in properties such as corrosion and stress corrosion cracking, creep, etc. While much early work in the field emphasized property improvements, the opportunity now exists to elucidate the underlying materials science of grain boundary network engineering. Recent investigations at LLNL have coupled automated electron backscatter diffraction (EBSD) with transmission electron microscopy (TEM)5 and atomic force microscopy (AFM) to elucidate these fundamental mechanisms.An example of the coupling of TEM and EBSD is given in Figures 1-3. The EBSD image in Figure 1 reveals “segmentation” of boundaries from special to random and random to special and low angle grain boundaries in some grains, but not others, resulting from the 15% compression of an Inconel 600 polycrystal.

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