scholarly journals Investigation on the Microstructure of ECAP-Processed Iron-Aluminium Alloys

Materials ◽  
2021 ◽  
Vol 14 (1) ◽  
pp. 219
Author(s):  
Bernd-Arno Behrens ◽  
Kai Brunotte ◽  
Tom Petersen ◽  
Roman Relge
Keyword(s):  
Grain Refinement ◽  
Aluminium Alloys ◽  
Aluminium Content ◽  
Microstructure Development ◽  
Chamber Furnace ◽  
Fine Grained ◽  
Angular Pressing ◽  
Ecap Process ◽  
Average Grain Size ◽  
Forming Temperature

The present work deals with adjusting a fine-grained microstructure in iron-rich iron-aluminium alloys using the ECAP-process (Equal Channel Angular Pressing). Due to the limited formability of Fe-Al alloys with increased aluminium content, high forming temperatures and low forming speeds are required. Therefore, tool temperatures above 1100 °C are permanently needed to prevent cooling of the work pieces, which makes the design of the ECAP-process challenging. For the investigation, the Fe-Al work pieces were heated to the respective hot forming temperature in a chamber furnace and then formed in the ECAP tool at a constant punch speed of 5 mm/s. Besides the chemical composition (Fe9Al, Fe28Al and Fe38Al (at.%—Al)), the influences of a subsequent heat treatment and the holding time on the microstructure development were investigated. For this purpose, the average grain size of the microstructure was measured using the AGI (Average Grain Intercept) method and correlated with the aforementioned parameters. The results show that no significant grain refinement could be achieved with the parameters used, which is largely due to the high forming temperature significantly promoting grain growth. The holding times in the examined area do not have any influence on the grain refinement.

scholarly journals STRUCTURE AND PROPERTIES OF AZ31 MAGNESIUM ALLOY AFTER COMBINATION OF HOT EXTRUSION AND ECAP

2017 ◽  
Vol 23 (3) ◽  
pp. 222 ◽  
Author(s):  
Ondřej Hilšer ◽  
Stanislav Rusz ◽  
Wojciech Maziarz ◽  
Jan Dutkiewicz ◽  
Tomasz Tański ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Magnesium Alloy ◽  
Hot Extrusion ◽  
Az31 Magnesium Alloy ◽  
Initial State ◽  
Fine Grained ◽  
Angular Pressing ◽  
Ecap Process ◽  
Average Grain Size ◽  
Fine Grained Structure

<p>Equal channel angular pressing (ECAP) method was used for achieving very fine-grained structure and increased mechanical properties of AZ31 magnesium alloy. The experiments were focused on the, in the initial state, hot extruded alloy. ECAP process was realized at the temperature 250°C and following route Bc. It was found that combination of hot extrusion and ECAP leads to producing of material with significantly fine-grained structure and improves mechanical properties. Alloy structure after the fourth pass of ECAP tool with helix matrix 30° shows a fine-grained structure with average grain size of 2 µm to 3 µm and high disorientation between the grains. More experimental results are discussed in this article.</p>

Rotary-Die Equal Channel Angular Pressing Method for Light Metals

2010 ◽  
Vol 638-642 ◽  
pp. 1614-1617
Author(s):  
Akira Watazu ◽  
Ichinori Shigematsu ◽  
Masataka Hakamada ◽  
Kazutaka Suzuki ◽  
Xin Sheng Huang ◽  
...  
Keyword(s):  
Magnesium Alloys ◽  
Aluminium Alloys ◽  
Light Metals ◽  
Bulk Materials ◽  
Ecap Processing ◽  
Pressing Method ◽  
Fine Grained ◽  
Angular Pressing ◽  
Ecap Process ◽  
Process Method

A new ECAP process method called rotary-die ECAP (RD-ECAP) was developed to form fine-grained bulk materials such as aluminium alloys, magnesium alloys, aluminium composites, and titanium, all of which can be processed under conditions of 573-773K, at an approximately 0.9-2.4 mm/s punch speed of 300MPa or lower. By the RD-ECAP method, ECAP processing of up to 2 passes can be done without sample removal and samples processed over 30 cycles were obtained.

Numerical Analysis of the Microstructure and Mechanical Properties Evolution during Equal Channel Angular Pressing

2010 ◽  
Vol 638-642 ◽  
pp. 1940-1945
Author(s):  
Lechoslaw Trebacz ◽  
Henryk Paul ◽  
Łukasz Madej ◽  
Maciej Pietrzyk
Keyword(s):  
Equal Channel Angular Pressing ◽  
Aluminium Alloys ◽  
New Technology ◽  
Strength Properties ◽  
Detailed Understanding ◽  
Fine Grained ◽  
Finite Element Software ◽  
Angular Pressing ◽  
Ecap Process ◽  
The Subject

The development of the new technology for manufacturing of multi layer aluminium based materials for heat radiators is the subject of this work. Modern aluminium alloys can be specially processed in a controlled manner to obtain nano(mikro) structures. These ultra fine grained structures play a significant role because they provide a possibility to obtain final product that is characterized by elevated strength properties and, at the same time, good anticorrosion and soldering properties. A detailed understanding of these ultra fined structures using a combination of numerical modelling and experimental analysis is presented in this paper. Particular attention is put on implementation of the microstructure evolution model into the finite element software to simulate Equal Channel Angular Pressing (ECAP) process. Examples of the obtained results are presented and discussed.

High Strain Rate Superplasticity in a Zr and Sc Modified 7075 Aluminum Alloy Produced by ECAP

2008 ◽  
Vol 584-586 ◽  
pp. 164-169 ◽  
Author(s):  
Krystof Turba ◽  
Premysl Malek ◽  
Edgar F. Rauch ◽  
Miroslav Cieslar
Keyword(s):  
Aluminum Alloy ◽  
High Strain Rate ◽  
Strain Rate ◽  
High Strain ◽  
Rate Sensitivity ◽  
7075 Aluminum Alloy ◽  
Fine Grained ◽  
Angular Pressing ◽  
Average Grain Size ◽  
Elongation To Failure

Equal-channel angular pressing (ECAP) at 443 K was used to introduce an ultra-fine grained (UFG) microstructure to a Zr and Sc modified 7075 aluminum alloy. Using the methods of TEM and EBSD, an average grain size of 0.6 1m was recorded after the pressing. The UFG microstructure remained very stable up to the temperature of 723 K, where the material exhibited high strain rate superplasticity (HSRSP) with elongations to failure of 610 % and 410 % at initial strain rates of 6.4 x 10-2 s-1 and 1 x 10-1 s-1, respectively. A strain rate sensitivity parameter m in the vicinity of 0.45 was observed at temperatures as high as 773 K. At this temperature, the material still reached an elongation to failure of 430 % at 2 x 10-2 s-1. These results confirm the stabilizing effect of the Zr and Sc additions on the UFG microstructure in a 7XXX series aluminum alloy produced by severe plastic deformation.

scholarly journals Analysis of Tribological Properties in Disks of AA-5754 and AA-5083 Aluminium Alloys Previously Processed by Equal Channel Angular Pressing and Isothermally Forged

Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 938
Author(s):  
Carmelo J. Luis Pérez ◽  
Rodrigo Luri Irigoyen ◽  
Ignacio Puertas Arbizu ◽  
Daniel Salcedo Pérez ◽  
Javier León Iriarte ◽  
...  
Keyword(s):  
Equal Channel Angular Pressing ◽  
Aluminium Alloys ◽  
Mean Value ◽  
Wear Behaviour ◽  
Volume Loss ◽  
Angular Pressing ◽  
Ring Configuration ◽  
Ecap Process ◽  
Initial States ◽  
Accumulated Deformation

In the present study, the wear behaviour of two aluminium alloys (AA-5754 and AA-5083) is analysed where these have been previously processed by severe plastic deformation (SPD) with equal channel angular pressing (ECAP). In order to achieve the objectives of this study, several disks made of these alloys are manufactured by isothermal forging from different initial states. The microstructures of the initial materials analysed in this study have different accumulated deformation levels. In order to compare the properties of the nanostructured materials with those which have not been ECAP-processed, several disks with a height of 6 mm and a diameter of 35 mm are manufactured from both aluminium alloys (that is, AA-5754 and AA-5083) isothermally forged at temperatures of 150 and 200 °C, respectively. These thus-manufactured disks are tested under a load of 0.6 kN, which is equivalent to a stress mean value of 18 MPa, and at a rotational speed of 200 rpm. In order to determine the wear values, the disks are weighed at the beginning, at 10,000 revolutions, at 50,000 revolutions and at 100,000 revolutions, and then the volume-loss values are calculated. This study was carried out using specific equipment, which may be considered to have a block-on-ring configuration, developed for testing in-service wear behaviour of mechanical components. From this, the wear coefficients for the two materials at different initial states are obtained. In addition, a comparison is made between the behaviour of the previously ECAP-processed aluminium alloys and those that are non-ECAP-processed. A methodology is proposed to determine wear coefficients for the aluminium alloys under consideration, which may be used to predict the wear behaviour. It is demonstrated that AA-5754 and AA-5083 aluminium alloys improve wear behaviour after the ECAP process compared to that obtained in non-ECAP-processed materials.

scholarly journals Designing (Ultra)Fine-Grained High-Entropy Alloys by Spark Plasma Sintering and Equal-Channel Angular Pressing

Crystals ◽  
2020 ◽  
Vol 10 (12) ◽  
pp. 1157
Author(s):  
Lisa-Marie Rymer ◽  
Thomas Lindner ◽  
Philipp Frint ◽  
Martin Löbel ◽  
Thomas Lampke
Keyword(s):  
Tensile Strength ◽  
Grain Refinement ◽  
Spark Plasma Sintering ◽  
Equal Channel Angular Pressing ◽  
High Entropy Alloys ◽  
High Entropy ◽  
Fine Grained ◽  
Angular Pressing ◽  
Plasma Sintering ◽  
Spark Plasma

Single-phase, face-centered cubic (FCC) high-entropy alloys (HEA) are promising materials for future applications. In order to improve the mechanical properties, especially the tensile strength of these materials, this study focuses on the combination of spark plasma sintering (SPS) and equal-channel angular pressing (ECAP). The initial fine-grained microstructure produced by SPS is further refined by ECAP in a 90°-die. Optical microscopy and electron backscatter diffraction (EBSD) confirm this considerable grain refinement, leads to a grain size below 1 µm after 1 ECAP pass. An alternating arrangement of fine-grained areas and much coarser regions, aligned under an angle of approximately 27°, is found. Moreover, a first microstructural investigation of the twin structure is conducted. The mechanical behavior was investigated by hardness measurements and tensile testing. Both the hardness and tensile strength are remarkably increased after ECAP. In contrast, the uniform elongation and elongation at fracture are significantly reduced due to the strengthening mechanisms of strain hardening and grain refinement. It is concluded that the combination of SPS and ECAP is an attractive approach for designing (ultra)fine-grained HEAs with superior properties. The investigated techniques could be applied to understand the underlying microstructural mechanisms.

Grain Refinement and Texture Evolution in AZ31 Alloy during ECAP Process and Their Effects on Mechanical Properties

2005 ◽  
Vol 475-479 ◽  
pp. 549-554 ◽  
Author(s):  
H.S. Kim ◽  
Hyo Tae Jeong ◽  
Ha Guk Jeong ◽  
Woo Jin Kim
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Refinement ◽  
Texture Evolution ◽  
Az31 Alloy ◽  
Mg Alloys ◽  
Fine Grained ◽  
Ecap Process ◽  
Texture Modification ◽  
Similar Texture

The softening of fine-grained ECAPed AZ31 Mg alloys could be ascribed to the texture modification during ECAP. Lower ECAP temperature is more effective in refining the microstructure. The strength of the ECAPed AZ 31 Mg alloys increased with decrease in grain size when they have similar texture.

Mechanical Properties and Texture Evolution of AZ31 Mg Alloy during Equal Channel Angular Pressing

2005 ◽  
Vol 475-479 ◽  
pp. 545-548 ◽  
Author(s):  
Hyo Tae Jeong ◽  
Woo Jin Kim
Keyword(s):  
Mechanical Properties ◽  
Grain Refinement ◽  
Equal Channel Angular Pressing ◽  
Texture Evolution ◽  
Fiber Texture ◽  
Mg Alloy ◽  
Angular Pressing ◽  
Ecap Process ◽  
Az31 Mg Alloy ◽  
Similar Texture

Microstructure and texture evolution in the AZ31 Mg alloy subject to equal channel angular pressing (ECAP) have been investigated and correlated with the mechanical properties. When AZ31 Mg alloy was ECAPed up to 8 passes following the route Bc, grain refinement occurred effectively. Texture was also changed during ECAP. The original fiber texture of the extruded AZ31 Mg alloy changed to a new texture component of ] 1 3 2 5 )[ 1 1 01 ( , and the texture of ] 1 3 2 5 )[ 1 1 01 ( orientation was rotated to ] 0 2 5 7 )[ 6 4 13 ( orientation after 6-pass ECAP process. The variation of the strength with the pass number was explained by the texture and grain size. The strength data of AZ31 Mg alloys followed the standard Hall-Petch relationship when the similar texture was retained during the ECAP process. Otherwise the effect of texture on strength was dominant over the strengthening due to grain refinement.

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