scholarly journals Microstructure and Properties of As-Cast and Heat-Treated 2017A Aluminium Alloy Obtained from Scrap Recycling

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 89
Author(s):  
Mrówka-Nowotnik Grażyna ◽  
Kamil Gancarczyk ◽  
Andrzej Nowotnik ◽  
Kamil Dychtoń ◽  
Grzegorz Boczkal
Keyword(s):  
Heat Treatment ◽  
Solution Heat Treatment ◽  
Relative Elongation ◽  
Intermetallic Phase ◽  
Natural Aging ◽  
Strength Properties ◽  
High Dispersion ◽  
Cast State ◽  
Continuous Increase ◽  
Scrap Recycling

The continuous increase in the consumption of aluminium and its alloys has led to an increase in the amount of aluminium scrap. Due to environmental protection, and to reduce the costs of manufacturing aluminum in recent years, a lot of research is devoted to recycling of aluminum alloys. The paper presents the results of research concerning the possibility of manufacturing standardized alloy 2017A from commercial and post-production scrap by continuous casting. Obtained from recycling process ingots were subjected to analysis of chemical composition and intermetallic phase composition. Based on the results of light microscopy (LM), scanning electron microscopy + electron dispersive spectroscopy (SEM + EDS), and X-ray diffraction (XRD) the following phases in the as-cast state were identified: θ-Al2Cu, β-Mg2Si, Al7Cu2Fe, Q-Al4Cu2Mg8Si7, and α-Al15(FeMn)3(SiCu)2. During solution heat treatment most of the primary precipitates of intermetallic phases, like θ-Al2Cu, β-Mg2Si, and Q-Al4Cu2Mg8Si7, were dissolved in the solid solution α-Al, and during natural and artificial aging they precipitate as strengthening phases θ-Al2Cu and Q-Al4Cu2Mg8Si7 with high dispersion. The highest hardness—150.3 HB—of 2017A alloy was obtained after solution heat treatment from 510 °C and aging at 175 °C. In the static tensile test the mechanical (Rm and Rp0.2) and plastic (A5) properties were determined for 2017A alloy in the cast state and after T4 heat treatment. The highest strength properties—tensile strength Rm = 450.5 MPa and yield strength R0.2 = 268.7 MPa with good relative elongation A5 = 14.65%, were obtained after solution heat treatment at 510 °C/6 h/water quenching and natural aging at 25 °C for 70 h. The alloy manufactured from recycled scrap is characterized by relatively high mechanical properties.

TEM and X-Ray Examinations of Intermetallic Phases and Carbides Precipitation in an Fe-Ni Superalloy during Prolonged Ageing

2013 ◽  
Vol 212 ◽  
pp. 15-20
Author(s):  
Kazimierz J. Ducki ◽  
Jacek Mendala ◽  
Lilianna Wojtynek
Keyword(s):  
Heat Treatment ◽  
Solution Heat Treatment ◽  
Intermetallic Phase ◽  
Intermetallic Phases ◽  
Precipitation Process ◽  
Secondary Phases ◽  
X Ray Diffraction ◽  
Solid Samples ◽  
Structural Investigations ◽  
X Ray

The influence of prolonged ageing on the precipitation process of the secondary phases in an Fe-Ni superalloy of A-286 type has been studied. The samples were subjected to a solution heat treatment at 980°C for 2 h and water quenched, and then aged at temperatures of 715, 750 and 780°C at holding times from 0.5 to 500 h. Structural investigations were conducted using TEM and X-ray diffraction methods. The X-ray phase analyses performed on the isolates were obtained by anodic dissolution of the solid samples. After solution heat treatment the alloy has the structure of twinned austenite with a small amount of undissolved precipitates, such as carbide TiC, carbonitride TiC0.3N0.7, nitride TiN0.3, carbosulfide Ti4C2S2, Laves phase Ni2Si, and boride MoB. The application of ageing causes precipitation processes of γ-Ni3(Al,Ti), G (Ni16Ti6Si7), η (Ni3Ti), β (NiTi) and σ (Cr0.46Mo0.40Si0.14) intermetallic phases, as well as the carbide M23C6. It was found that the main phase precipitating during alloy ageing was the γ intermetallic phase.

Precipitate and Age Hardening Response of As-Cast Mg-8Yb-0.5Zr Magnesium Alloy

2011 ◽  
Vol 399-401 ◽  
pp. 17-20
Author(s):  
Wen Bin Yu ◽  
Zhi Qian Chen ◽  
Mang Zhang ◽  
Zhou Yu
Keyword(s):  
Heat Treatment ◽  
Magnesium Alloy ◽  
Grain Boundaries ◽  
Microstructure Evolution ◽  
Solution Heat Treatment ◽  
Artificial Aging ◽  
Precipitation Hardening ◽  
Intermetallic Phase ◽  
Age Hardening ◽  
Maximum Hardness

The precipitation hardening response of as-cast Mg-8Yb-0.5Zr magnesium alloy was investigated in the present work. The microstructure evolution of the alloy illustrated that Mg2Yb intermetallic phase was dissolved by solution heat treatment at 520°C for 12 hours. An apparent precipitation hardening response in Mg-8Yb-0.5Zr was discovered after artificial aging at 150°C, with maximum hardness increment of about 80 percent at the peak condition. It was found that the precipitates of the alloy were in the shape of two conjoined cosh and globe about 50 nm, and precipitated preferentially on grain boundaries and dislocations.

scholarly journals The Microstructure And Mechanical Properties Of The AlSi17Cu5 Alloy After Heat Treatment

2015 ◽  
Vol 60 (3) ◽  
pp. 1813-1818
Author(s):  
J. Piątkowski ◽  
T. Matuła
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Solution Heat Treatment ◽  
Aging Treatment ◽  
Strength Properties ◽  
Silicon Crystals ◽  
Primary Si ◽  
Microstructure And Mechanical Properties ◽  
Favorable Change ◽  
Significant Size

Abstract In the paper results of the microstructure and mechanical properties (HB, Rm and R0,2) of AlSi17Cu5 alloy, subjected by solution heat treatment (500ºC/6h/woda) and aging (200ºC/16h/piec) are presented. In next step the alloy was modified and heated significantly above the Tliq temperature (separately and together). It was found that the increase in the strength properties of the tested alloy after heat treatment compared to alloys without solution heat treatment and aging was due to precipitation hardening. The applied aging treatment of ingots (preceded by solution heat treatment), causes not only increase in concentration in α(Al) solid solution, but also a favorable change of the primary Si crystals morphology. During stereological measurements significant size reduction and change in the morphology of hypereutectic silicon crystals ware found. This effects can be further enhanced by overheating the alloy to a temperature of 920ºC and rapid cooling before casting of the alloy.

scholarly journals Effect of Solution Heat Treatment and Artificial Aging on Compression Behaviour of A356 Alloy

2019 ◽  
Vol 25 (3) ◽  
pp. 281-285
Author(s):  
Dhanashekar MANICKAM ◽  
Senthil Kumar VELUKKUDI SANTHANAM
Keyword(s):  
Heat Treatment ◽  
Compressive Strength ◽  
Solution Heat Treatment ◽  
Artificial Aging ◽  
A356 Alloy ◽  
Natural Aging ◽  
Static Condition ◽  
Corrosion Properties ◽  
Compression Behaviour ◽  
Heat Treated

Aluminium alloys are subjected to heat treatment to increase the strength and corrosion properties. This paper aims to study the effect of heat treatment on the compression behaviour of A356 alloy under quasi static condition and barreling effect. The various heat treatments are: (i) solution heat treatment of 1 h at 540 °C + natural aging 0 h + artificial aging at 180 °C up to 5.5 h, (ii) solution heat treatment of 3 h at 540 °C + natural aging for 20 h + artificial aging at 180 °C up to 5.5 h, and (iii) solution heat treatment of 6 h at 540 °C + natural aging for 20 h + artificial aging at 180 °C up to 5.5 h. Specially to understand the influence of artificial aging at every 0.5 h up to 5.5 h, the specimens were heat treated. From the results, solutionizing for 1 hr have a better compression strength irrespective of the artificial aging. Natural aging had decreased the ductility but increased the strength property. Artificial aging had a significant effect on the compressive strength and peak strength were obtained at 4 h irrespective of solutionizing heat treatment. Compressive strength increased by 33 % for 1 h of solutionizing and 4 h of artificial aged specimen when compared to non-heat treated alloy. Two mathematical relations discussed in literature were used for calculating the radius of the barreled surface followed by validation. DOI: http://dx.doi.org/10.5755/j01.ms.25.3.20442

The Effect of Solution Heat Treatment on Incipient Melting of Al2Cu Intermetallic Phase in Lightweight Materials

2016 ◽  
Vol 857 ◽  
pp. 256-260
Author(s):  
Chung Seok Kim ◽  
Jin Woo Jo ◽  
Hak Min Lee
Keyword(s):  
Heat Treatment ◽  
Solution Heat Treatment ◽  
Intermetallic Phase ◽  
Intermetallic Phases ◽  
Single Step ◽  
Treatment Temperature ◽  
Solution Temperature ◽  
Incipient Melting ◽  
Cast Specimen ◽  
Eutectic Si

The effects of solution heat treatment of Al6Si2Cu aluminum alloy on incipient melting of θ-Al2Cu phase have been investigated. Solution heat treatments, in this study, are applied to improve of mechanical properties through a single-step solution heat treatment. The microstructure of as-cast specimen represents a typical dendrite structure having a secondary dendrite arm spacing of 37um. In addition to the Al matrix, a large amount of coarsen eutectic Si, θ-Al2Cu intermetallic phases and Fe-rich phases are identified. As the solution temperature increases, the Vickers's hardness increases up to 510°C and thereafter hardness decreases at the temperature of 520°C and 530°C. This hardness behavior may closely related with microstructural evolution such as solubility of alloying elements up to 510°C and also melting of θ-Al2Cu intermetallic phases over 510°C in this study. Consequentially, the optimal single-step solution heat treatment temperature should be 510°C to improve mechanical property.

Research on Characteristics of Heat Treatment of Squeeze Cast Al-Cu-Mg Alloy

2013 ◽  
Vol 749 ◽  
pp. 54-60
Author(s):  
Yao Qiang Gan ◽  
Lei Lu ◽  
Da Tong Zhang ◽  
Wei Wen Zhang ◽  
Yuan Yuan Li
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Solution Heat Treatment ◽  
Artificial Aging ◽  
Squeeze Casting ◽  
Natural Aging ◽  
Mg Alloy ◽  
Solute Diffusion ◽  
Aged Alloy ◽  
Casting Alloy

A high strength Al-Cu-Mg alloy was prepared by squeeze casting. The effects of squeeze casting and heat treatment on the microstructures and mechanical properties of the alloy were studied. It was found that squeeze casting refined the microstructure and reduced the micro-segregation markedly, and also accelerated the diffusion process of solute atoms during solution heat treatment. Tensile strength and elongation of squeeze casting alloy were much higher than those of gravity casting alloy under both the as-cast and heat-treated conditions. In addition, the Al-Cu-Mg alloy prepared by squeeze casting showed good natural aging response, and the naturally-aged alloy possessed a slightly lower tensile strength but better elongation compared to full artificial aging. After solution heat treatment at 495 for 9h and further natural aging for 48h or artificial aging at 190 for 6h, the tensile strength of squeeze casting alloy reached to 472MPa and 475MPa, respectively, and the elongation was 18.9% and 12.7% accordingly. Based on the experimental results, the mechanism of microstructural evolution of squeeze casting Al-Cu-Mg alloy during heat treatment was discussed, and the effect of squeeze casting on the kinetics of solute diffusion and aging precipitation was studied.

6XXX Alloys: Chemical Composition and Heat Treatment

2019 ◽  
Author(s):  
Grażyna Mrówka-Nowotnik
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Chemical Composition ◽  
Intermetallic Phase ◽  
Chinese Script ◽  
High Dispersion ◽  
Cu Content ◽  
The Matrix ◽  
Si Content ◽  
Additional Phase

Analysis of the influence of chemical composition, crystallization process and heat treatment on the phase constituents’ morphology, and mechanical properties and crack resistance of 6xxx Al alloys were conducted. The alloys with low Mg and Si content (6063) in the as-cast state are characterized by presence of Si particles and primary intermetallic phases: α-Al8Fe2Si, β-Al5FeSi, β-Mg2Si, and α-Al(FeMn)Si. Higher Mg, Si, and Mn content (6005 and 6082) leads to separation of additional phase particles: Al6Fe, Al6Mn, and Al12(FeMn)Mg3Si6, whereas high Cu content (6061—0.35% and 6066—0.95%, respectively) is responsible for precipitation of additional phase particles: Q-Al5Cu2Mg8Si6 and θ-Al2Cu. It has been established that homogenization results in total dissolution of the θ-Al2Cu and Q-Al5Cu2Mg8Si6 primary phases and partial dissolution of β-Mg2Si. Needle-like and Chinese-script α-Al8Fe2Si and β-Al5FeSi were transformed into spheroidal α-Al(FeMn)Si particles. The maximal consolidation of the 6xxx alloys is a result of precipitation of metastable particles, the transient βʺ, βʹ, and Qʹ/θʹ phases (6061 alloy) with high dispersion. The highest mechanical properties were achieved after holding in the temperature of 565°C/6 h, supersaturated in water, and aging at 175°C/10–20 h (T6). The decohesion process in the presence of tensile stresses in the room temperature proceeds through nucleation, the growth and joining of the voids, as well as the cracking of the primary and secondary large-sized intermetallic phase particles. The increase of deformation temperature up to 300°C causes the changes of the nucleation source and joining of voids—it occurs mainly along the matrix–particle interface.

scholarly journals The role of Zr and T6 heat treatment on microstructure evolution and hardness of AlSi9Cu3(Fe) diecasting alloy

2017 ◽  
Vol 53 (3) ◽  
pp. 423-428 ◽  
Author(s):  
M. Voncina ◽  
S. Kores ◽  
M. Ernecl ◽  
J. Medved
Keyword(s):  
Heat Treatment ◽  
Artificial Aging ◽  
Die Casting ◽  
Intermetallic Phase ◽  
Intermetallic Phases ◽  
Cast State ◽  
T6 Heat Treatment ◽  
Zr Addition ◽  
Cast Alloys

The microstructure features and hardness of AlSi9Cu3(Fe) die casting alloy was investigated in the presence of Zr addition. The cast alloys were undergone the solutionizing treatment 2 h at 500?C followed by artificial aging at 180?C for 5 h. Optical microscopy and electron micro-analyzer were used to study the formation of different intermetallic phases. The hardness was tested for all samples at 25?C. The results revealed that the intermetallic phase, based on (Al,Si)(Zr,Ti), forms when Zr is added in the investigated alloy, while the T6 heat treatment does not influence on the formation of Zr-bearing phase. Results also indicate that the hardness slightly increases in the AlSi9Cu3 alloy in as-cast state when Zr is added, while after T6 heat treatment increases by 50% in the alloy without Zr and by 61% in the alloy with Zr addition.

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