scholarly journals Effect of Hot Isostatic Pressing on Porosity and Mechanical Properties of 316 L Stainless Steel Prepared by the Selective Laser Melting Method

Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4377
Author(s):  
Tomas Cegan ◽  
Marek Pagac ◽  
Jan Jurica ◽  
Katerina Skotnicova ◽  
Jiri Hajnys ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Stainless Steel ◽  
Hot Isostatic Pressing ◽  
Microstructural Analysis ◽  
Scanning Speed ◽  
High Yield ◽  
Laser Method ◽  
Preparation Conditions ◽  
Lower Porosity ◽  
316 L Stainless Steel

The manufacturing route primarily determines the properties of materials prepared by additive manufacturing methods. In this work, the microstructural features and mechanical properties of 316 L stainless steel prepared by the selective laser method have been determined. Three types of samples, (i) selective laser melted (SLM), (ii) selective laser melted and hot isostatic pressed (HIP) and (iii) selective laser melted and heat treated (HT), were characterized. Microstructural analysis revealed that SLM samples were formed by melt pool boundaries with fine cellular–dendritic-type microstructure. This type of microstructure disappeared after HT or HIP and material were formed by larger grains and sharply defined grain boundaries. The SLM-prepared samples contained different levels of porosity depending on the preparation conditions. The open interconnected LOF (lack of fusion) pores were observed in the samples, which were prepared with using of scanning speed 1200 mm/s. The blowhole and keyhole type of porosity were observed in the samples prepared by lower scanning speeds. The HIP caused a significant decrease in internal closed porosity to 0.1%, and a higher pressure of 190 MPa was more effective than the usually used pressure of 140 MPa, but for samples with open porosity, HIP was not effective. The relatively high yield strength of 570 MPa, tensile strength of 650 MPa and low ductility of 30–34% were determined for SLM samples with the lower porosity content than 1.3%. The samples after HIP showed lower yield strengths than after SLM (from 290 to 325 MPa) and relatively high ductility of 47.8–48.5%, regardless of the used SLM conditions.

scholarly journals Enhancement of Mechanical Properties and Porosity of Concrete Using Steel Slag Coarse Aggregate

Materials ◽  
2020 ◽  
Vol 13 (12) ◽  
pp. 2865
Author(s):  
Md Jihad Miah ◽  
Md. Munir Hossain Patoary ◽  
Suvash Chandra Paul ◽  
Adewumi John Babafemi ◽  
Biranchi Panda
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Microstructural Analysis ◽  
Steel Slag ◽  
Physical And Mechanical Properties ◽  
Length Change ◽  
Sustainable Building ◽  
Burnt Clay ◽  
Lower Porosity ◽  
Furnace Steel

This paper investigates the possibility of utilizing steel slags produced in the steelmaking industry as an alternative to burnt clay brick aggregate (BA) in concrete. Within this context, physical, mechanical (i.e., compressive and splitting tensile strength), length change, and durability (porosity) tests were conducted on concrete made with nine different percentage replacements (0%, 10%, 20%, 30%, 40%, 50%, 60%, 80%, and 100% by volume of BA) of BA by induction of furnace steel slag aggregate (SSA). In addition, the chemical composition of aggregate through X-ray fluorescence (XRF) analysis and microstructural analysis through scanning electron microscopy (SEM) of aggregates and concrete were performed. The experimental results show that the physical and mechanical properties of concrete made with SSA were significantly higher than that of concrete made with BA. The compressive and tensile strength increased by 73% when SSA fully replaced BA. The expansion of concrete made with SSA was a bit higher than the concrete made with BA. Furthermore, a significant lower porosity was observed for concrete made with SSA than BA, which decreased by 40% for 100% SSA concrete than 100% BA concrete. The relation between compressive and tensile strength with the porosity of concrete mixes are in agreement with the relationships presented in the literature. This study demonstrates that SSA can be used as a full replacement of BA, which is economical, conserves the natural aggregate, and is sustainable building material since burning brick produces a lot of CO2.

scholarly journals Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing

Materials ◽  
2021 ◽  
Vol 14 (23) ◽  
pp. 7110
Author(s):  
Yanbin Pei ◽  
Xuanhui Qu ◽  
Qilu Ge ◽  
Tiejun Wang
Keyword(s):  
Stainless Steel ◽  
Hot Deformation ◽  
True Strain ◽  
Hot Isostatic Pressing ◽  
Microstructural Analysis ◽  
Critical Conditions ◽  
True Strain Rate ◽  
Isostatic Pressing ◽  
Different Temperatures ◽  
Borated Stainless Steel

Borated stainless steel (BSS) specimens have a boron content of 1.86 wt%, and are prepared by hot isostatic pressing (HIP) conducted at different temperatures, ranging from 1000 to 1100 °C and a constant true strain rate (0.01, 0.1, 1 and 10 s−1). These tests, with observations and microstructural analysis, have achieved the hot deformation characteristics and mechanisms of BSS. In this research, the activation energy (Q) and Zener–Hollomon parameter (Z) were contrasted against the flow curves: Q = 442.35 kJ/mol. The critical conditions associated with the initiation of dynamic recrystallization (DRX) for BSS were precisely calculated based on the function between the strain hardening rate with the flow stress: at different temperatures from 1000 to 1100 °C: the critical stresses were 146.69–254.77 MPa and the critical strains were 0.022–0.044. The facts show that the boron-containing phase of BSS prevented the onset of DRX, despite the saturated boron in the austenite initiated DRX. The microstructural analysis showed that hot deformation promoted the generation of borides, which differed from the initial microstructure of HIP. The inhomogeneous distribution of elements in the boron-containing phase was caused by hot compression.

scholarly journals Microstructure and mechanical properties relationship of additively manufactured 316L stainless steel by selective laser melting

2019 ◽  
Vol 5 ◽  
pp. 23 ◽  
Author(s):  
Anne-Helene Puichaud ◽  
Camille Flament ◽  
Aziz Chniouel ◽  
Fernando Lomello ◽  
Elodie Rouesne ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Stainless Steel ◽  
Selective Laser Melting ◽  
316L Stainless Steel ◽  
Hot Isostatic Pressing ◽  
Tensile Tests ◽  
Industrial Applications ◽  
Added Value ◽  
Laser Melting ◽  
Microstructure And Mechanical Properties

Additive manufacturing (AM) is rapidly expanding in many industrial applications because of the versatile possibilities of fast and complex fabrication of added value products. This manufacturing process would significantly reduce manufacturing time and development cost for nuclear components. However, the process leads to materials with complex microstructures, and their structural stability for nuclear application is still uncertain. This study focuses on 316L stainless steel fabricated by selective laser melting (SLM) in the context of nuclear application, and compares with a cold-rolled solution annealed 316L sample. The effect of heat treatment (HT) and hot isostatic pressing (HIP) on the microstructure and mechanical properties is discussed. It was found that after HT, the material microstructure remains mostly unchanged, while the HIP treatment removes the materials porosity, and partially re-crystallises the microstructure. Finally, the tensile tests showed excellent results, satisfying RCC-MR code requirements for all AM materials.

scholarly journals Mechanical Properties and Hydrogen Embrittlement of Laser-Surface Melted AISI 430 Ferritic Stainless Steel

Coatings ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 140 ◽  
Author(s):  
W. K. Chan ◽  
C. T. Kwok ◽  
K. H. Lo
Keyword(s):  
Stainless Steel ◽  
Hydrogen Embrittlement ◽  
Strain Rate ◽  
Ferritic Stainless Steel ◽  
Laser Scanning ◽  
Electron Backscatter Diffraction ◽  
Microstructural Analysis ◽  
Scanning Speed ◽  
Laser Surface ◽  
Aisi 430

In the present study, the feasibility of laser surface melting (LSM) of AISI 430 ferritic stainless steel to minimize hydrogen embrittlement (HE) was investigated. LSM of AISI 430 steel was successfully achieved by a 2.3-kW high power diode laser (HPDL) with scanning speeds of 60 mm/s and 80 mm/s (the samples are designated as V60 and V80, respectively) at a power of 2 kW. To investigate the HE effect on the AISI 430 steel without and with LSM, hydrogen was introduced into specimens by cathodic charging in 0.1 M NaOH solution under galvanostatic conditions at a current density of 30 mA/cm2 and 25 °C. Detail microstructural analysis was performed and the correlation of microstructure with HE was evaluated. By electron backscatter diffraction (EBSD) analysis, the austenite contents for the laser-surface melted specimens V60 and V80 are found to be 0.6 and 1.9 wt%, respectively. The amount of retained austenite in LSM specimens was reduced with lower laser scanning speed. The surface microhardness of the laser-surface melted AISI 430 steel (~280 HV0.2) is found to be increased by 56% as compared with that of the substrate (~180 HV0.2) because of the presence of martensite. The degree of embrittlement caused by hydrogen for the charged and non-charged AISI 430 steel was obtained using slow-strain-rate tensile (SSRT) test in air at a strain rate of 3 × 10−5 s−1. After hydrogen pre-charging, the ductility of as-received AISI 430 steel was reduced from 0.44 to 0.25 while the laser-surface melted AISI 430 steel showed similar tensile properties as the as-received one. After LSM, the value of HE susceptibility Iδ decreases from 43.2% to 38.9% and 38.2% for V60 and V80, respectively, due to the presence of martensite.

scholarly journals Mechanical and Electrochemical Characterization of Supersolidus Sintered Austenitic Stainless Steel (316 L)

2019 ◽  
Vol 38 (2019) ◽  
pp. 792-805 ◽  
Author(s):  
S. Ramakrishna Kandala ◽  
Kantesh Balani ◽  
Anish Upadhyaya
Keyword(s):  
Mechanical Properties ◽  
Stainless Steel ◽  
Electrochemical Impedance ◽  
Rupture Strength ◽  
Electrochemical Behaviour ◽  
Compaction Pressure ◽  
316 L Stainless Steel ◽  
Aisi 316 ◽  
Stainless Steel 316 ◽  
Aisi 316 L

AbstractThe present study compares the mechanical properties and electrochemical behaviour of austenitic (AISI 316 L) stainless steel compacted at different pressures (200, 400 and 600 MPa), which are conventionally sintered at supersolidus temperature of 1,400°C. As expected, increase in compaction pressure (from 200 MPa) to 600 MPa has shown decreased shrinkage (from 7.3% to 4.2% radial and 5.5% to 3.4% axial, respectively) and increased densification (up to ~92%). Their electrochemical behaviour was investigated in 0.1 N H2SO4 solution by potentiodynamic polarization and electrochemical impedance spectroscopy. The mechanical properties (such as yield-, tensile- and transverse rupture strength) and electrochemical behaviour with pressure have been correlated with densification response and microstructure (pore type, volume and morphology). Highest densification (~92% theoretical) achieved at 600 MPa (compaction pressure) and 1,400°C (sintering temperature) resulted in excellent combination of tensile strength and ductility (456 ± 40 MPa and 25 ± 1.1% respectively), while showing lowest corrosion rate (0.1 mmpy or 4.7 mpy) due to the presence of isolated porosity in the sintered samples.

scholarly journals Effect of Annealing Heat Treatment on the Microstructural Evolution and Mechanical Properties of Hot Isostatic Pressed 316L Stainless Steel Fabricated by Laser Powder Bed Fusion

Metals ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 753 ◽  
Author(s):  
Kanwal Chadha ◽  
Yuan Tian ◽  
John Spray ◽  
Clodualdo Aranas
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Stainless Steel ◽  
316L Stainless Steel ◽  
Hot Isostatic Pressing ◽  
Isostatic Pressing ◽  
Heat Treated ◽  
Two Samples ◽  
Annealing Heat Treatment ◽  
Annealing Heat

In this work, the microstructural features and mechanical properties of an additively manufactured 316L stainless steel have been determined. Three types of samples were characterized: (i) as printed (AP), (ii) annealing heat treated (AHT), and (iii) hot isostatic pressed and annealing heat treated (HIP + AHT). Microstructural analysis reveals that the AP sample formed melt pool boundaries with nano-scale cellular structures. These structures disappeared after annealing heat treatment and hot isostatic pressing. The AP and AHT samples have similar grain morphologies; however, the latter has a lower dislocation density and contains precipitates. Conversely, the HIP + AHT sample displays polygon-shaped grains with twin structures; a completely different morphology compared to the first two samples. Optical micrography reveals that the application of hot isostatic pressing reduces the porosity generated after laser processing. The tensile strengths of all the samples are comparable (about 600 MPa); however, the elongation of the HIP + AHT sample (48%) was superior to that of other two samples. The enhanced ductility of the HIP + AHT sample, however, resulted in lower yield strength. Based on these findings, annealing heat treatment after hot isostatic pressing was found to improve the ductility of as-printed 316L stainless steel by as much as 130%, without sacrificing tensile strength, but the sample may have a reduced (40%) yield strength. The tensile strength determined here has been shown to be higher than that of the hot isostatic pressed, additively manufactured 316L stainless steel available from the literature.

The Effect of Stand - Off Distance on the Mechanical Properties of TIG Butt Joints of 316 Stainless Steel

2020 ◽  
Vol 833 ◽  
pp. 59-65
Author(s):  
Hala M. Gnedi ◽  
Khawla T. Snoussi ◽  
Abulmaali M. Taher ◽  
Thoria G. Sharef ◽  
Yousef Arebi
Keyword(s):  
Mechanical Properties ◽  
Stainless Steel ◽  
Base Metal ◽  
Welded Joints ◽  
Hardness Test ◽  
Scanning Speed ◽  
Geometrical Parameters ◽  
Worst Case ◽  
316 Stainless Steel ◽  
Hardness Values

The objective of this study is to investigate and determine the effect of the stand-off distance (distance between the welded plates) on the mechanical properties of the Tungsten Inert Gas (TIG) welded joints. Butt TIG welding was performed for 316 stainless steel (SS) by using different pre welding stand-off distances with fixing the other parameters (thickness of welded plates, voltage, current, groove shape, and scanning speed). The influence of the stand-off distance parameter was examined by using tensile test, hardness test in the three different regions (base metal, heat effected zone, and molten zone), non-destructive testing (including visual inspection, liquid pentrant and X – ray) and microscopic examinations. Results show that the stand-off distance is one of the most important geometrical parameters of the Butt welded joints to end by good mechanical properties. It is found that the optimum stand-off distance was about 1 mm (shows the highest hardness results), but still there were some defects in some spots in the molten metal zone which caused a decrease in the hardness values in these locations. The 2 mm stand-off distance shows reasonable results, and the worst case was recorded for the 0 mm stand-off distance condition. Generally the hardness values of the heat affected zone in all conditions were the highest when compared to both metal welding zone and the base metal zone.

Effect of alloy grain size on oxidation resistance of silica-coated stainless steel

1994 ◽  
Vol 52 ◽  
pp. 676-677
Author(s):  
C. S. McDowell ◽  
S. N. Basu
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Stainless Steel ◽  
Oxidation Resistance ◽  
Powder Processing ◽  
Hot Isostatic Pressing ◽  
Silica Coating ◽  
Austenitic Steels ◽  
Coarse Grained ◽  
Fine Grained

Oxidation resistance of stainless steels, which rely on the formation of a Cr2O3 (chromia) scale, can be further improved through minor alloying additions such as Al or Si, or by application of coatings to the exposed surfaces. Although, additions of Si to austenitic steels have demonstrated an improvement in oxidation resistance, high Si contents can be detrimental to the mechanical properties of these alloys. The application of a silica coating on the surface of the stainless steel provides improved oxidation resistance without detrimental effects on the mechanical properties. This study examines the effect of the grain size of the stainless steel on the effectiveness of a silica coating as an oxidation barrier.Fully austenitic stainless steel of composition Fe-18(wt%)Cr-20Ni-1.5Mn was produced in both coarsegrained and fine-grained form. The coarse-grained alloy, with a grain size of approximately 100 μm, was produced by casting and hot rolling. The fine-grained alloy, with a grain size of approximately 5 μm, was produced by rapid solidification powder processing, followed by consolidated by hot isostatic pressing and swaging.

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