scholarly journals Effects of Silicon Content and Tempering Temperature on the Microstructural Evolution and Mechanical Properties of HT-9 Steels

Materials ◽  
2020 ◽  
Vol 13 (4) ◽  
pp. 972 ◽  
Author(s):  
Junkai Liu ◽  
Wenbo Liu ◽  
Zhe Hao ◽  
Tiantian Shi ◽  
Long Kang ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Microstructural Evolution ◽  
Charpy Impact ◽  
Hardness Test ◽  
Mechanical Tests ◽  
Fourth Generation ◽  
Martensitic Steels ◽  
Microscopic Mechanism ◽  
Tempering Temperature

Two kinds of experimental ferritic/martensitic steels (HT-9) with different Si contents were designed for the fourth-generation advanced nuclear reactor cladding material. The effects of Si content and tempering temperature on microstructural evolution and mechanical properties of these HT-9 steel were studied. The microstructure of experimental steels after quenching and tempering were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM); the mechanical properties were investigated by means of tensile test, Charpy impact test, and hardness test. The microscopic mechanism of how the microstructural evolution influences mechanical properties was also discussed. Both XRD and TEM results showed that no residual austenite was detected after heat treatment. The results of mechanical tests showed that the yield strength, tensile strength, and plasticity of the experimental steels with 0.42% (% in mass) Si are higher than that with 0.19% Si, whereas hardness and toughness did not change much; when tempered at 760 °C, the strength and hardness of the experimental steels decreased slightly compared with those tempered at 710 °C, whereas plasticity and toughness increased. Further analysis showed that after quenching at 1050 °C for 1 h and tempering at 760 °C for 1.5 h, the comprehensive mechanical properties of the 0.42% Si experimental steel are the best compared with other experimental steels.

scholarly journals Basic mechanical properties of layered steels

2013 ◽  
Vol 61 (1) ◽  
pp. 25-38 ◽  
Author(s):  
Michal Černý ◽  
Josef Filípek ◽  
Pavel Mazal ◽  
Petr Dostál
Keyword(s):  
Mechanical Properties ◽  
Impact Test ◽  
Charpy Impact ◽  
Charpy Impact Test ◽  
Mechanical Tests ◽  
Tempering Temperature ◽  
Technical Practice ◽  
Steel Bars ◽  
Multilayer Steel ◽  
Quenching And Tempering

This article deals with identifying attributes of layered steel materials (damask steel) with the help of mechanical tests. Experimentally verify basic mechanical properties of layered steel and subsequently assessed it in comparison with the values obtained for the classic steel materials. In conclusion, there are listed the possibilities of using multilayer steel materials in technical practice, depending on the economics of production.The damask steel was prepared by forge welding from a packet consisting of 17 layers (9 layers of tool steel 19 133 (ČSN) with the thickness of 6 mm and 8 layers 80NiCr11 steel in the form of saw bands with the thickness of 1.2 mm. The packet was cut into 8 parts, folded 3 times and forged together, which provided damask steel with 136 layers. The resulting steel bars were used to make semi-finished products with the approximate dimensions of the test specimens. For evaluation of mechanical properties were applied the following tests: tensile test, Charpy impact test, hardness and microhardness measurementsThe results of tests proved that the properties of damask steel are dependent not only on the direction led impact quality forge weld layers and content iof nhomogeneities in the place of discord, but also on the quenching and tempering temperature, resp. on the choice of quenching bath, which determine the final structure of steel and the resulting hardness, respectively microhardness.

scholarly journals Correlation between Microstructural Evolution and Mechanical Properties of 2000 MPa Cold-Drawn Pearlitic Steel Wires during Galvanizing Simulated Annealing

Metals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 326 ◽  
Author(s):  
Xiuyu Lu ◽  
Jing Liu ◽  
Guifeng Zhou ◽  
Lulu Feng ◽  
Zhen Wang
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Simulated Annealing ◽  
Microstructural Evolution ◽  
Hardness Test ◽  
Pearlitic Steel ◽  
Torsion Test ◽  
Dissolved Carbon ◽  
Steel Wires ◽  
Dislocation Pinning

In the present experiment, hot-dip galvanizing simulated annealing of 2000 MPa cold-drawn pearlitic steel wires was carried out at 450 °C. The effects of microstructural evolution on the mechanical properties of the as-prepared wires were analyzed through scanning electron microscopy (SEM), transmission electron microscopy (TEM), tensile test, torsion test, and Vickers hardness test. In addition, the relationship between torsion laps and microstructural evolution of cold-drawn pearlitic steel wires was investigated in detail. It was found that the torsional performance of the wires deteriorated after annealing at 450 °C for 2–5 min, and the corresponding microstructural evolution was accompanied by the partial degradation of lamellar pearlites due to the diffusion and dislocation pinning of dissolved carbon atoms in ferrites, and it is not feasible to achieve the matching of strength and torsion laps by prolonging the holding time. The deterioration in torsional performance can be attributed to the microstructural difference between the surface and the center of the annealed wires. When the proportion of non-lamellar structure between the surface and the center in each specimen exceeded 8%, the microhardness difference was found to be greater than 40 HV and the torsion lap was less than 3 circles.

MECHANICAL PROPERTIES OF EPOXY RESIN BASED GRAPHENE NANO PARTICLES COMPOSITE

2020 ◽  
Vol 15 (4) ◽  
Author(s):  
Durgaprasad Kollipara ◽  
Prabhakar Gope VNB ◽  
Raja Loya
Keyword(s):  
Mechanical Properties ◽  
Epoxy Resin ◽  
Epoxy Composite ◽  
Hardness Test ◽  
Industrial Applications ◽  
Mechanical Tests ◽  
Nano Particles ◽  
Potential Candidate ◽  
Matrix Composites ◽  
Reinforcing Material

Composites have tremendous applicability due to their excellent capabilities. The performance of composites mainly depends on the reinforcing material applied. A Graphene nanoparticle (GNP) is successful as an efficient reinforcing material due to its versatile as well as superior properties. Even at very low content, graphene can dramatically improve the properties of polymer and metal matrix composites. In this paper the effects of GNP on composites based on epoxy resin were analyzed. Different contents of GNP (0 – 4.5 vol. %) were added to the epoxy resin. The GNP/epoxy composite was fabricated under room temperature. Mechanical tests result such as tensile, flexural and hardness test show enhancements of the mechanical properties of the GNP/epoxy composite. The experimental results clearly show an improvement in Young’s modulus, tensile strength, and hardness as compared to pure epoxy. The results of this research are strong evidence for GNP/epoxy composites being a potential candidate for use in a variety of industrial applications, especially for automobile parts, aircraft components, and electronic parts such as super capacitors, transistors, etc.

Mechanical Properties and Microstructure of LR Grade a Thick Plate Welded by Double Side Gas Metal Arc Welding

2016 ◽  
Vol 851 ◽  
pp. 168-172
Author(s):  
Yustiasih Purwaningrum ◽  
Triyono ◽  
Tegar Rileh Argihono ◽  
Ryan Sutrisno
Keyword(s):  
Mechanical Properties ◽  
Gas Flow ◽  
Gas Metal Arc Welding ◽  
Charpy Impact ◽  
Hardness Test ◽  
Charpy Impact Test ◽  
Optical Microscope ◽  
Steel Plates ◽  
Weld Metals ◽  
Metal Arc Welding

Mechanical and microstructure of double side weld with various angle groove was studied in this research. LR Gr A steel plates (12 mm thickness) were welded using GMAW with corresponding 180 A, 23 V, and 20 l/min respectively with current, voltage, and gas flow. Shielding gas and filler metals used are argon and ER 70S-6. The angle groove that used were 20⁰, 40⁰ and 60⁰. The measured of mechanical properties with regard to hardness, toughness and strength using, Vickers hardness test, Charpy impact test and tensile test respectively The microstructure examined with optical microscope. The results show that the highest hardness values found in welds with groove angle 40ͦ. The transition temperatures of weld metals are at temperatures between -20°C to 0°C. Weld metals with all variations of the groove angle has a value of less than 0.1 mmpy. Microstructure of base metals and HAZ were ferrite and pearlite. While the microstructure of weld metals are accicular ferrite, grain boundary ferrite and Widmanstatten ferrite.

scholarly journals SEM ANALYSIS AND STUDY OF MECHANICAL PROPERTIES OF UV AGED PVC/CORN COB COMPOSITES

2018 ◽  
Vol 6 (1) ◽  
pp. 347-353
Author(s):  
Krisztina Roman ◽  
Zita Szabo ◽  
Bence Szeman ◽  
Tamas Szabo
Keyword(s):  
Mechanical Properties ◽  
Hardness Test ◽  
Mechanical Tests ◽  
Sem Analysis ◽  
Corn Cob ◽  
Sem Micrographs ◽  
Analysis And Study

In this study, the aged mechanical properties and the modifier structure were determined. Bio-materials are often used as additives to plastics, in order to make the degradation easier in the environment. We examined the differences of the properties of samples differently aged; the ages of the samples were 1 and 3 years. The properties that were gathered from the mechanical tests, such as tensile-, flexural-, impact-, and hardness-test, show changes depending on the ages of the samples. Due to the aging, decrease of mechanical properties was experienced. The microcellular structures of the composites were studied by SEM analysis in order to understand the changes of the structures. It can be seen on the recording that the corn cob strengthens and sticks to the cells wall. The internal changes of the structure that were caused by the aging cannot be seen on the SEM micrographs.

Review on Accumulative Roll Bonding (ARB) Techniques for Improving the Mechanical Properties of Multi-Layered Materials

2020 ◽  
Vol 979 ◽  
pp. 84-88
Author(s):  
A. Arun ◽  
Lakshmanan Poovazhgan
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Accumulative Roll Bonding ◽  
Nanocrystalline Structure ◽  
Hardness Test ◽  
Roll Bonding ◽  
Transmission Electron ◽  
Ultrafine Grained ◽  
Materials Used ◽  
Number Of Passes

Accumulative Roll Bonding (ARB) is one among the techniques in Severe Plastic Deformation (SPD) which is used to produce ultrafine grains and nanocrystalline structure in the materials used. Tensile test, micro hardness test, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and bending tests are the various tests carried out to understand the grain refinement of ARB materials. ARB is carried out in homogenous and heterogeneous materials to bring out the useful applications of ultrafine grained materials. ARB process mainly carried out in room, warm and hot temperature. The variations in the structure of the material are obtained by changing the load applied on the roller and by increasing the number of passes. This review paper brings out how the mechanical properties of the materials are improved by ARB process

scholarly journals Effect of Two-Stage Homogenization Heat Treatment on Microstructure and Mechanical Properties of AA2060 Alloy

Crystals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 40
Author(s):  
Chaoyang Chaoyang ◽  
Guangjie Guangjie ◽  
Lingfei Lingfei ◽  
Fei Fei ◽  
Lin Lin
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Cast Alloy ◽  
Hardness Test ◽  
Test Methods ◽  
Al Alloy ◽  
Two Stage ◽  
Homogenization Treatment ◽  
Transmission Electron ◽  
The Matrix

The microstructure evolution of AA2060 Al alloy containing Li during two-stage homogenization treatment was investigated by optical microscopy (OM), scanning electron microscopy (SEM) equipped with energy dispersive X-ray spectroscopy (EDS), differential scanning calorimeter (DSC), transmission electron microscopy (TEM), mechanical properties and Vickers micro-hardness test methods. The results demonstrate that severe precipitation of θ(Al2Cu) and S(Al2CuMg) phase existed in the as-cast alloy, especially in the center position. Cu elements were concentrated at grain boundary and gradually decreased from the boundary to the interior. Numerous eutectic phases of θ(Al2Cu) and S (Al2CuMg) containing Zn and Ag elements were segregated at grain boundaries. The overheating temperature of the as-cast alloy is 497 °C. After two-stage homogenization treatment, the θ(Al2Cu) and S (Al2CuMg) in the surface, middle and center positions were completely dissolved into the matrix, thus achieved uniform homogenization effect. Moreover, water cooling could prevent the precipitation after homogenization, which provided good performance of the studied alloy. The optimum two-stage homogenization treatment of AA2060 alloy was 460 °C/4 h + 490 °C/2 4 h. The homogenization kinetic analysis was discussed as well.

Preparation of Al2O3/Al-Si Composites by In Situ Reaction of Fe2O3+MnO2/Al System

2015 ◽  
Vol 816 ◽  
pp. 48-53
Author(s):  
Jing Zhang ◽  
Hua Shun Yu ◽  
Xin Ting Shuai ◽  
Hong Mei Chen ◽  
Guang Hui Min
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Electron Probe ◽  
Room Temperature ◽  
Manganese Content ◽  
Hardness Test ◽  
Test Results ◽  
Electron Probe Micro Analyzer ◽  
Transmission Electron ◽  
Polygonal Shape

Al2O3 particles reinforced ZL109 composites were prepared by in-situ reaction between Fe2O3+MnO2 and Al in this paper. The influence of ratio of Mn to Fe on the morphologies of Al-Si-Mn-Fe phase and mechanical properties of the composites was investigated. The microstructure was studied by electron probe micro-analyzer (EPMA) and transmission electron microscopy (TEM). The results show that the Al2O3 particles displaced by the Fe2O3+MnO2/Al system are in nanosize. The acicular Al-Si-Fe phases change from acicular to polygonal shape and become smaller with the increase manganese content. The hardness test results have no big difference on the composites. However, the ultimate tensile strength at room temperature and 350°C enhance evidently with the increasing of Mn/Fe.

scholarly journals Welding Soundness of a Thick-Walled 9Cr-1Mo Steel

2010 ◽  
Vol 654-656 ◽  
pp. 408-411
Author(s):  
Woo Seog Ryu ◽  
Sung Ho Kim ◽  
Dae Whan Kim
Keyword(s):  
Mechanical Properties ◽  
Weld Metal ◽  
Base Metal ◽  
Hardness Test ◽  
Ultimate Tensile Stress ◽  
Narrow Gap ◽  
Martensitic Steels ◽  
Narrow Gap Welding ◽  
Self Energy ◽  
Welding Processes

High Cr ferritic/martensitic steels are demanded to join using favorable welding processes with economical and metallurgical advantages in order to apply to the thick-walled reactor pressure vessel of a very high temperature gas cooled reactor. Narrow gap welding technology was adopted to weld a thick-walled 9Cr-1Mo-1W steel with thickness of 110mm. The welding integrity was checked by non-destructive examination, optical microscopy and hardness test, and the homogeneity through welding depth was checked by absorbed impact energy and tensile strength. The optimizing welding conditions resulted that a narrow U-grooved gap with almost parallel edges was sound in actual practice, and the coarse grain zone was minimized in the heat affected zone. The absorbed energy of 75±25 J through welding depth was acceptable in scatter band to check the uniformity through the welding depth. The ultimate tensile stress and yield stress were about the same through welding depth at 650±10 MPa and 500±10 MPa, indicating no difference through welding depth. Elongation was also almost same through depth, and the fracture surface was appeared as a normal. The weld metal had similar mechanical properties to base metal. The upper self energy of weld metal was 194J, and the ductile-brittle transition temperature was 30°C. The tensile behavior was the typical trend with temperature, and YS and UTS of weldment were slightly higher than base metal by nearly below 10%. Thus, it concluded that the soundness of the narrow gap welding of a thick-walled 9Cr-1Mo-1W steel was confirmed in terms of the welding uniformity through the depth and mechanical properties.

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