scholarly journals Effect of Two-Stage Homogenization Heat Treatment on Microstructure and Mechanical Properties of AA2060 Alloy

Crystals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 40
Author(s):  
Chaoyang Chaoyang ◽  
Guangjie Guangjie ◽  
Lingfei Lingfei ◽  
Fei Fei ◽  
Lin Lin
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Cast Alloy ◽  
Hardness Test ◽  
Test Methods ◽  
Al Alloy ◽  
Two Stage ◽  
Homogenization Treatment ◽  
Transmission Electron ◽  
The Matrix

The microstructure evolution of AA2060 Al alloy containing Li during two-stage homogenization treatment was investigated by optical microscopy (OM), scanning electron microscopy (SEM) equipped with energy dispersive X-ray spectroscopy (EDS), differential scanning calorimeter (DSC), transmission electron microscopy (TEM), mechanical properties and Vickers micro-hardness test methods. The results demonstrate that severe precipitation of θ(Al2Cu) and S(Al2CuMg) phase existed in the as-cast alloy, especially in the center position. Cu elements were concentrated at grain boundary and gradually decreased from the boundary to the interior. Numerous eutectic phases of θ(Al2Cu) and S (Al2CuMg) containing Zn and Ag elements were segregated at grain boundaries. The overheating temperature of the as-cast alloy is 497 °C. After two-stage homogenization treatment, the θ(Al2Cu) and S (Al2CuMg) in the surface, middle and center positions were completely dissolved into the matrix, thus achieved uniform homogenization effect. Moreover, water cooling could prevent the precipitation after homogenization, which provided good performance of the studied alloy. The optimum two-stage homogenization treatment of AA2060 alloy was 460 °C/4 h + 490 °C/2 4 h. The homogenization kinetic analysis was discussed as well.

The effect of ageing duration on the mechanical properties of Al alloy 6061-garnet composites

2001 ◽  
Vol 215 (2) ◽  
pp. 113-119
Author(s):  
S C Sharma
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Compressive Strength ◽  
Al Alloy ◽  
Destructive Testing ◽  
Transmission Electron ◽  
Heat Treated ◽  
The Matrix ◽  
Reinforcing Particle ◽  
Alloy 6061

A well-consolidated composite of Al alloy 6061 reinforced with 4, 8 and 12 wt% garnet was prepared by a liquid metallurgy technique, the composite was heat treated for different ageing durations (T6 treatment), and its mechanical properties were determined by destructive testing. The results of the study indicated that, as the garnet particle content in the composites increased, there were marked increases in the ultimate tensile strength, compressive strength and hardness but there was a decrease in the ductility. There was an improvement in the tensile strength, compressive strength, and hardness with ageing due to precipitation. Precipitation in Al alloy 6061, with and without garnet particulate reinforcement, was studied using transmission electron microscopy. The fracture behaviour of the composites was altered significantly by the presence of garnet particles and the crack propagation through the matrix, and the reinforcing particle clusters resulted in final fracture.

Review on Accumulative Roll Bonding (ARB) Techniques for Improving the Mechanical Properties of Multi-Layered Materials

2020 ◽  
Vol 979 ◽  
pp. 84-88
Author(s):  
A. Arun ◽  
Lakshmanan Poovazhgan
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Accumulative Roll Bonding ◽  
Nanocrystalline Structure ◽  
Hardness Test ◽  
Roll Bonding ◽  
Transmission Electron ◽  
Ultrafine Grained ◽  
Materials Used ◽  
Number Of Passes

Accumulative Roll Bonding (ARB) is one among the techniques in Severe Plastic Deformation (SPD) which is used to produce ultrafine grains and nanocrystalline structure in the materials used. Tensile test, micro hardness test, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and bending tests are the various tests carried out to understand the grain refinement of ARB materials. ARB is carried out in homogenous and heterogeneous materials to bring out the useful applications of ultrafine grained materials. ARB process mainly carried out in room, warm and hot temperature. The variations in the structure of the material are obtained by changing the load applied on the roller and by increasing the number of passes. This review paper brings out how the mechanical properties of the materials are improved by ARB process

scholarly journals TEM observation of precipitates and their role to mechanical properties in Ti-5553 alloy heated to some temperatures up to 923 K

2020 ◽  
Vol 321 ◽  
pp. 11035
Author(s):  
E. Sukedai ◽  
E. Aeby-Gautier ◽  
M. Dehmas
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Hardening Mechanism ◽  
Transmission Electron ◽  
The Matrix ◽  
Higher Temperature ◽  
Shearing Mechanism ◽  
Hardness Values ◽  
Measured Hardness

A Ti-5553 specimen was continuously heated to 923 K and simultaneously in-situ HEXRD profiles were taken. In addition, specimens heated at the same rate to several temperatures up to 923 K and further quenched were observed by transmission electron microscopy. Based on both results obtained, transformation sequence was clarified, precipitations of ω-, α”iso- and α-phases were confirmed, and size and density of these precipitates were measured. Hardness values of those specimens were also measured. The hardening mechanism was considered as shearing-mechanism for specimens aged at lower temperatures and by-pass one for specimens aged at higher temperature. An attempt of distinction between α”iso - and α-precipitates was also tried. Both precipitates were in needle-like shape and a possibility was suggested by measuring angles between two needle-shape precipitates on {110} of the matrix and comparing with each other.

scholarly journals Enhancement of Mechanical and Thermal Properties of Polylactic Acid/Polycaprolactone Blends by Hydrophilic Nanoclay

2013 ◽  
Vol 2013 ◽  
pp. 1-11 ◽  
Author(s):  
Chern Chiet Eng ◽  
Nor Azowa Ibrahim ◽  
Norhazlin Zainuddin ◽  
Hidayah Ariffin ◽  
Wan Md. Zin Wan Yunus ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Polylactic Acid ◽  
Mechanical Analysis ◽  
Basal Spacing ◽  
Mechanical And Thermal Properties ◽  
X Ray Diffraction ◽  
Transmission Electron ◽  
The Matrix ◽  
Thermal Stability Of

The effects of hydrophilic nanoclay, Nanomer PGV, on mechanical properties of Polylactic Acid (PLA)/Polycaprolactone (PCL) blends were investigated and compared with hydrophobic clay, Montmorillonite K10. The PLA/PCL/clay composites were prepared by melt intercalation technique and the composites were characterized by X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), Thermogravimetric Analysis (TGA), Dynamic Mechanical Analysis (DMA), Scanning Electron Microscopy (SEM), and Transmission Electron Microscopy (TEM). FTIR spectra indicated that formation of hydrogen bond between hydrophilic clay with the matrix. XRD results show that shifting of basal spacing when clay incorporated into polymer matrix. TEM micrographs reveal the formation of agglomerate in the composites. Based on mechanical properties results, addition of clay Nanomer PGV significantly enhances the flexibility of PLA/PCL blends about 136.26%. TGA showed that the presence of clay improve thermal stability of blends. DMA show the addition of clay increase storage modulus and the presence of clay Nanomer PGV slightly shift two Tg of blends become closer suggest that the presence of clay slightly compatibilizer the PLA/PCL blends. SEM micrographs revealed that presence of Nanomer PGV in blends influence the miscibility of the blends. The PLA/PCL blends become more homogeneous and consist of single phase morphology.

Preparation of Al2O3/Al-Si Composites by In Situ Reaction of Fe2O3+MnO2/Al System

2015 ◽  
Vol 816 ◽  
pp. 48-53
Author(s):  
Jing Zhang ◽  
Hua Shun Yu ◽  
Xin Ting Shuai ◽  
Hong Mei Chen ◽  
Guang Hui Min
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Electron Probe ◽  
Room Temperature ◽  
Manganese Content ◽  
Hardness Test ◽  
Test Results ◽  
Electron Probe Micro Analyzer ◽  
Transmission Electron ◽  
Polygonal Shape

Al2O3 particles reinforced ZL109 composites were prepared by in-situ reaction between Fe2O3+MnO2 and Al in this paper. The influence of ratio of Mn to Fe on the morphologies of Al-Si-Mn-Fe phase and mechanical properties of the composites was investigated. The microstructure was studied by electron probe micro-analyzer (EPMA) and transmission electron microscopy (TEM). The results show that the Al2O3 particles displaced by the Fe2O3+MnO2/Al system are in nanosize. The acicular Al-Si-Fe phases change from acicular to polygonal shape and become smaller with the increase manganese content. The hardness test results have no big difference on the composites. However, the ultimate tensile strength at room temperature and 350°C enhance evidently with the increasing of Mn/Fe.

Electron Microscopy of Irradiated and Mechanically Tested Tungsten

1967 ◽  
Vol 25 ◽  
pp. 314-315
Author(s):  
Robert C. Rau ◽  
Robert L. Ladd ◽  
John Moteff
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Physical And Mechanical Properties ◽  
Threshold Region ◽  
Body Centered Cubic ◽  
Defect Clusters ◽  
Neutron Fluences ◽  
Transmission Electron ◽  
Abrupt Changes ◽  
The Matrix

As part of a program investigating the effects of neutron irradiation on the physical and mechanical properties of body centered cubic refractory metals, transmission electron microscopy has been carried out on irradiated tungsten after tensile and creep-rupture testing. These observations have shown the existence of a fluence threshold region between 5.9 × 1018 and 3.8 × 1019 nvt (E < 1 MeV) over which both microstructure and mechanical properties undergo abrupt changes.A series of specimens irradiated at pile ambient temperature (∼ 70°C) to various fast neutron fluences and subsequently tensile tested at 400°C showed dramatic evidence of the build-up of defect clusters with increasing exposure. The starting microstructure present in undeformed button heads of unirradiated control specimens consisted of large tungsten grains divided into many small subgrains by hexagonal dislocation networks, as shown in Figure 1. Irradiation to neutron fluences of 4.0 and 5.9 × 1018 nvt produced tiny dot clusters in the matrix, as shown in Figure 2.

Investigation on B, Cr Doped Ni3Al Alloy Prepared by Self-Propagation High-Temperature Synthesis and Hot Extrusion

2013 ◽  
Vol 747-748 ◽  
pp. 124-131 ◽  
Author(s):  
Li Yuan Sheng ◽  
Jian Ting Guo ◽  
Chao Yuan ◽  
F. Yang ◽  
G.S. Li ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
High Temperature ◽  
Hot Extrusion ◽  
The Self ◽  
Al Alloy ◽  
Temperature Synthesis ◽  
X Ray ◽  
High Temperature Synthesis ◽  
Transmission Electron

The Ni3Al and Ni3Al-B-Cr alloys were fabricated by the self-propagation high-temperature synthesis with hot extrusion method. Their microstructure and mechanical properties were studied by using combination of X-ray diffraction, optical microscopy, transmission electron microscopy and compression test. Analysis of X-ray spectra exhibited that the elemental powders had been transformed to the Ni3Al phase after the self-propagation high-temperature synthesis processing. Microstructure examination showed that the alloy without extrusion consisted of coarse and fine grains, but the subsequent hot extrusion procedure homogenized the grain size and densified the alloy obviously. Transmission electron microscopy observations on the Ni3Al alloy revealed that Ni3Al, γ-Ni and Al2O3 particles were the main phases. When the boron and chromium were added, besides the β-NiAl phase, α-Cr phase and some Cr7Ni3 particles with stacking faults inside were observed. In addition, a lot of substructure and high-density dislocation arrays were observed in the extruded part, which indicated that the subsequent extrusion had led to great deformation and partly recrystallizing in the alloy. Moreover, the subsequent extrusion procedure redistributed the Al2O3 particles and eliminated the γ-Ni. These changes were helpful to refine the microstructure and weaken the misorientation. The mechanical test showed that the self-propagation high-temperature synthesis with hot extrusion improved the mechanical properties of the Ni3Al alloy significantly. The addition of B and Cr in Ni3Al alloy increased the mechanical properties further, but the compressive strength of the alloy was still lower than that synthesized by combustion. Finally, the self-propagation high-temperature synthesis with hot extrusion was a good method to prepare Ni3Al alloy from powder.

scholarly journals Enhancement of the mechanical properties of HDPE mineral nanocomposites by filler particles modulation of the matrix plastic/elastic behavior

2022 ◽  
Vol 11 (1) ◽  
pp. 312-320
Author(s):  
Yousef Murtaja ◽  
Lubomír Lapčík ◽  
Harun Sepetcioglu ◽  
Jakub Vlček ◽  
Barbora Lapčíková ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Mechanical Performance ◽  
Plant Production ◽  
Elastic Behavior ◽  
Indentation Modulus ◽  
Transmission Electron ◽  
The Matrix ◽  
Poly Ethylene ◽  
Mineral Fillers

Abstract Two different nanosized mineral fillers (nano calcium carbonate and nanoclay) were used in the high density poly(ethylene) (HDPE) composites pilot plant production. Structural and mechanical properties of the prepared composites were examined in this study. The homogenous filler distribution was confirmed in the tested samples by scanning electron microscopy, transmission electron microscopy, and energy dispersive spectroscopy analyses. The fillers’ fortifying effect on polymer composites’ mechanical performance was confirmed as indicated by the increased elastic modulus and indentation modulus. Additionally, the possible modulation of the plastic-elastic mechanical behavior was confirmed by the type of the filler as well as its concentration used in the final composites testing articles.

Microstructural and Mechanical Properties of Polyester/Nanoclay Nanocomposites: Microstructure-Mixing Strategy Correlation

2011 ◽  
Vol 1312 ◽  
Author(s):  
Hamid Dalir ◽  
Rouhollah D. Farahani ◽  
Vireya Nhim ◽  
Benjamin Samson ◽  
Martin Lévesque ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fracture Strain ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Roll Mill ◽  
The Matrix ◽  
Polyester Matrix ◽  
Excellent Improvement

ABSTRACTDifferent nanoclay mixing strategies using a three-roll mill and ultrasonication is proposed to obtain the desired polyester/nanoclay dispersion, intercalation, and exfoliation. The dispersion states of the modified nanoclay in polymer with 2, 4 and 6 wt% loading were characterized with X-ray diffraction, scanning electron microscopy (SEM), and low and high magnification transmission electron microscopy (TEM). The mechanical properties of the clay-reinforced polyester nanocomposites were a function of the nature and the content of the clay in the matrix. The nanocomposite containing 4 wt% modified Cloisite® 15A exhibits excellent improvement in modulus (by ~51%) and tensile strength (by ~12%) with a decrease in fracture strain (by ~26%) and fracture energy (by ~17%). These mechanical characteristic changes can be attributed to the dispersion, intercalation, and exfoliation of the nanoclays inside the polyester matrix.

scholarly journals Tribo-mechanical properties evaluation of HA/TiO2/CNT nanocomposite

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Erfan Zalnezhad ◽  
F. Musharavati ◽  
Tianyi Chen ◽  
Fadi Jaber ◽  
Kaan Uzun ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Hot Isostatic Pressing ◽  
Surface Hardness ◽  
Hardness Test ◽  
X Ray ◽  
In Vitro Biocompatibility ◽  
Transmission Electron ◽  
Nanocomposite Powders

AbstractIn this study, a combination of reverse microemulsion and hydrothermal techniques were used to synthesize HA. A hydrothermal method was used to synthesize HA/TiO2/CNT nanocomposite powders. Cold and hot isostatic pressing techniques were used to fabricate tablet-shaped samples. To investigate the biocompatibility and tribo-mechanical properties of HA/TiO2 and HA/TiO2/CNTs, four samples were prepared with different percentages of CNTs, namely, HA/TiO2 (S0), HA/TiO2/CNT (S1.0), HA/TiO2/CNT (S2.0), and HA/TiO2/CNT (S3.0). The microstructure and morphology of the HA/TiO2/CNTs were characterized by transmission electron microscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction. Hardness test results show that S3.0 displayed the highest surface hardness (285 HV) compared to other samples. The wear rate of HA/TiO2/CNT with the highest CNT content showed a decrease compared with those of the other samples. The results from nanoindentation tests showed that Young’s modulus of the S3.0 sample was 58.1% greater than that of the S0 sample. Furthermore, the human MDA-MB-231 cell line demonstrated good binding to the surface of the samples in the in-vitro biocompatibility evaluation of the HA/TiO2/CNT composites.

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