scholarly journals Complex Study of Eutectoidal Phase Transformation of 2507-Type Super-Duplex Stainless Steel

Materials ◽  
2019 ◽  
Vol 12 (13) ◽  
pp. 2205 ◽  
Author(s):  
István Mészáros ◽  
Bálint Bögre

The aim of this work was to study expansively the process of the eutectoidal phase transformation of 2507-type super-duplex stainless steel. Three sample sets were prepared. The first sample set was made to investigate the effect of the previous cold rolling and heat treatment for the eutectoidal phase transformation. Samples were cold rolled at seven different rolling reductions which was followed by heat treatment at five different temperatures. The second sample set was prepared to determine the activation energy of the eutectoidal decomposition process using the Arrhenius equation. Samples were cold rolled at seven different rolling reductions and were heat treated at the same temperature during eight different terms. A third sample set was made to study how another plastic-forming technology, beside the cold rolling, can influence the eutectoidal decomposition. Samples were elongated by single axis tensile stress and were heat treated at the same temperature. The results of the first and the third sample sets were compared. The rest δ-ferrite contents were calculated using the results of AC and DC magnetometer measurements. DC magnetometer was used as a feritscope device in this work. Light microscope and electron back scattering diffraction (EBSD) images demonstrated the process of the eutectoidal decomposition. The thermoelectric power and the hardness of the samples were measured. The results of the thermoelectric power measurement were compared with the results of the δ-ferrite content measurement. The accurate value of the coercive field was determined by a Foerster-type DC coercimeter device.

2017 ◽  
Vol 885 ◽  
pp. 184-189 ◽  
Author(s):  
István Mészáros ◽  
Bálint Bögre

The aim of this study was to investigate the effect of the previously applied cold rolling and the latter heat treatment for the eutectoidal decomposition of δ-ferrite in 2507 type superduplex stainless steel (SDSS). The samples were cold rolled at seven different deformation rates which was followed by heat treatment at were 20, 700, 750, 800 and 850 °C temperatures. The rolled and heat treated samples were investigated by hardness tester, AC magnetometer and thermoelectric power measurement. The activation energy of the decomposition was determined by the Arrhenius equation through the results of the AC magnetometer measurement.


2020 ◽  
Vol 64 (2) ◽  
pp. 150-158
Author(s):  
Bálint Bögre ◽  
István Mészáros

In this work five different methods – AC magnetometer, DC magnetometer, Feritscope, EBSD and X-ray diffraction - were compared with each other. These methods were used to determine the δ-ferrite content of samples. The limits, disadvantages and advantages of the applied methods were analyzed. The tested material was 2507 type super-duplex stainless steel. The samples were cold rolled and heat treated to modify their ferrite content.


2013 ◽  
Vol 746 ◽  
pp. 467-472 ◽  
Author(s):  
In June Moon ◽  
Bok Su Jang ◽  
Jin Hyun Koh

The purpose of this study was to investigate the effect of heat treatment (930°C, 1080°C, 1230°C) followed by quenching on the pitting corrosion resistance, sigma phase precipitation, and microstructural change of a super duplex stainless steel (UNS S32750) welds made by gas tungsten arc (GTA). Based on the microstructural examination, the σ phase was formed in welds heat treated at 930°C while there were little σ phases formed in welds experienced the relatively fast cooling from 1080°C and 1230°C. Accordingly, the most weight loss due to pitting corrosion occurred in the as received base and weld metals heat treated at 930°C. It was confirmed that the pitting corrosion occurred in the phase boundaries of ferrite/sigma and austenite/sigma.


2014 ◽  
Vol 783-786 ◽  
pp. 2154-2159 ◽  
Author(s):  
Andreas Johnsson ◽  
Mats Karlberg

During the annealing heat treatment following cold rolling of a 304L austenitic stainless steel sheet material, the material goes through changes in microstructure and mechanical properties. The cold rolling history together with the time/temperature trajectory in the annealing furnace can be used to model the final microstructure. In this work, physically based models for recrystallization and the following grain growth was created for the prediction of the microstructure evolution-both grain size and grain size distribution-, and an artificial neural network, ANN, was added for secondary effects. This is more commonly referred to as a hybrid model. The microstructure hybrid model was tested and validated against cold rolled and annealed production sheet material of various thicknesses and reductions, where the grain size and grain size distribution was measured by Electron Back Scatter Diffraction, EBSD. The recrystallization and grain growth parameters and functionality were fitted for non-isothermal conditions, against experimental tests of cold rolled material. Given process history and time/temperature data from the annealing heat treatment, the model can predict the microstructure, average grain size and grain size distribution with high accuracy and the executing time is short which makes it suitable for in-line use.


2010 ◽  
Vol 163 ◽  
pp. 151-156 ◽  
Author(s):  
Janusz Ryś ◽  
Małgorzata Witkowska

The present examination is a part of project concerning a deformation behavior of duplex type ferritic-austenitic stainless steels. The investigations included the analysis of ferrite and austenite microstructures formed in cold-rolled sheet of super-duplex stainless steel, major deformation mechanisms operating in both constituent phases and changes in morphology of two-phase structure after the thermo-mechanical treatment and subsequent cold-rolling. Duplex type stainless steels develop the band-like ferrite-austenite morphology in the course of hot- and cold-rolling. This specific two-phase structure creates different conditions for plastic deformation in comparison to single phase steels. The interaction of both phases upon deformation exerts fairly significant influence on structure and texture formation in both constituent phases and in consequence affects the material properties and its behavior upon further processing.


2021 ◽  
Vol 28 (3) ◽  
pp. 440-449
Author(s):  
K. Bin Tayyab ◽  
A. Farooq ◽  
A. Ahmed Alvi ◽  
A. Basit Nadeem ◽  
K. M. Deen

Author(s):  
Abhijit Biswas ◽  
Suman Kalyan Das ◽  
Prasanta Sahoo

The microstructural changes of electroless Ni–P–Cu coating at various heat-treatment conditions are investigated to understand its implications on the tribological behavior of the coating. Coatings are heat-treated at temperatures ranging between 200°C and 800 °C and for 1–4 h duration. Ni–P–Cu coatings exhibit two-phase transformations in the temperature range of 350–450 °C and the resulting microstructural changes are found to significantly affect their thermal stability and tribological attributes. Hardness of the coating doubles when heat-treated at 452 °C, due to the formation of harder Ni3P phase and crystalline NiCu. Better friction and wear performance are also noted upon heat treatment of the coating at the phase transformation regime, particularly at 400 °C. Wear mechanism is characterized by a mixed adhesive cum abrasive wear phenomena. Heat treatment at higher temperature (600 °C and above) and longer duration (4 h) results in grain coarsening phenomenon, which negatively influences the hardness and tribological characteristics of the coating. Besides, diffusion of iron from the ferrous substrate as well as greater oxide formation are noticed when the coating is heat-treated at higher temperatures and for longer durations (4 h).


2019 ◽  
Vol 141 (10) ◽  
Author(s):  
Mengjiao Wang ◽  
Yunxia Wang ◽  
Jianzhang Wang ◽  
Na Fan ◽  
Fengyuan Yan

Super duplex stainless steel (SDSS) has excellent mechanical properties and corrosion resistance. However, currently, there are few researches conducted on its fretting wear performance. This paper studies the influence of different heat treatment temperatures and medium environment on the fretting wear performance of SAF 2507 SDSS. Results show that the combined effect of the sigma phase and seawater lubrication can significantly improve the wear resistance of SAF 2507 SDSS. After treated with different heat treatment temperatures, different contents of sigma phases are precipitated out of SAF 2507 SDSS, which improves the wear resistance of the material to different degrees. In addition, the fretting wear performance of SAF 2507 SDSS also relates to the lubrication medium. In air, the friction and wear performance of SAF 2507 SDSS is poor, while in seawater, solution and corrosion products that acted as a lubricant dramatically improve the wear resistance of the material. Under the combined action of heat treatment and seawater lubrication medium, the friction coefficient and wear reduce by 70% and 91%, respectively.


2013 ◽  
Vol 795 ◽  
pp. 492-495 ◽  
Author(s):  
Mohd Noor Mazlee ◽  
Alvin Tan Yin Zhen ◽  
Shamsul Baharin Jamaludin ◽  
Nur Farhana Hayazi ◽  
Shaiful Rizam Shamsudin

Tensile shear strength and ageing treatment of dissimilar 6063 aluminum alloy-316L stainless steel joint fabricated by spot welding were investigated. The results showed that tensile shear strength increased with the increasing of welding current. The enhancement of tensile shear strength of the joints was due to the enlargement of the nugget diameter. It was also found that the tensile shear strength values for heat treated joint almost similar to that of non-heat treated joint.


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