scholarly journals Vickers Micro-Hardness of New Restorative CAD/CAM Dental Materials: Evaluation and Comparison after Exposure to Acidic Drink

Materials ◽  
2019 ◽  
Vol 12 (8) ◽  
pp. 1246 ◽  
Author(s):  
Marco Colombo ◽  
Claudio Poggio ◽  
Alessandro Lasagna ◽  
Marco Chiesa ◽  
Andrea Scribante

CAD/CAM (computer-aided design/computer-aided manufacturing) for indirect restorative materials has been recently introduced in dentistry. The purpose of this study was to evaluate the change of the surface micro-hardness of different restorative CAD/CAM materials after exposure to a carbonated acidic drink (Coca-Cola, Coca-Cola Company, Milan, Italy). One hundred and eighty specimens of identical size (2 mm thickness) were obtained by sectioning each tested CAD/CAM block of four materials: a hybrid ceramic (CERASMART™, GC Corporation, Tokyo, Japan), a resin nano ceramic (Lava™ Ultimate, 3M, Monrovia, CA, USA), a nanohybrid composite (Grandio blocs, VOCO GmbH, Cuxhaven, Germany), and a zirconia-reinforced lithium silicate glass ceramic (VITA SUPRINITY® PC; VITA Zahnfabrik, Bad Sackingen, Germany). Forty-five specimens of each material were tested. Micro-hardness was measured at baseline, after 7 days and after 28 days. The data were analyzed. The micro-hardness of each material varied significantly after immersion in Coca-Cola. The nanohybrid composite had a high initial micro-hardness and the greatest percentage loss after acid exposure. The hybrid ceramic and the resin nano ceramic had similar percentage losses of micro-hardness values even if the second material had higher initial values. The zirconia-reinforced lithium silicate glass ceramic had the highest baseline values and the lowest percentage loss of micro-hardness. The different CAD/CAM materials presented different micro-hardness values before and after acid exposure.

2019 ◽  
Vol 45 (4) ◽  
pp. 442-452 ◽  
Author(s):  
N Ilie ◽  
G Furtos

Clinical Relevance Light transmission through dental materials and tooth structure has direct clinical implication on such factors as selecting an appropriate curing technique during a restorative process. SUMMARY Introduction: This study aims to quantify and compare the amount of light that passes through seven different types of direct and indirect restorative materials comprising light-cured resin based composites (regular and bulk-fill), computer-aided design/computer-aided manufacturing (CAD/CAM) restoratives such as resin based composites, poly(methyl methacrylate) (PMMA) resin, leucite glass-ceramic, lithium silicate glass-ceramic, feldspar ceramic, and the natural tooth structure. Methods and Materials: Individual sets (n=6) of plane-parallel test specimens (2 mm) of 32 restorative materials belonging to the aforementioned seven material types and the tooth structure were prepared. Within the analyzed materials, one leucite glass-ceramic and one lithium disilicate glass-ceramic were considered in two different translucencies. In addition, two light-cured resin composites, one CAD/CAM resin composite, and one lithium disilicate glass-ceramic were considered in two different shades. Optical properties (transmittance, T; absorbance, A; and opacity, O) of each material were calculated from the relationship between incident and transmitted irradiance [I(d)] using a violet-blue light-curing unit. Incident and transmitted irradiance were assessed in real time on a spectrophotometer. A multivariate analysis (general linear model) assessed the effects of various parameters on the optical properties. Results: A very strong influence of the parameter material was identified on I(d) (p<0.001; partial eta squared, ηP2=0.953), T (p<0.001; ηP2=0.951), A (p<0.001; ηP2=0.925), and O (p<0.001; ηP2=0.886), while the effect of the parameter material type was not significant (p=0.079, p=0.05, p=0.05, and p=0.051, respectively). Light attenuation differed significantly by material within each shade category and by shade category within the analyzed material. Conclusions: Attenuation of light through restorative materials and tooth structure is high (59.9% to 94.9%); thus, deficits in polymerization are difficult to compensate for by additional light exposure at the end of the restorative process.


Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4239
Author(s):  
Roxana-Diana Vasiliu ◽  
Sorin Daniel Porojan ◽  
Liliana Porojan

The accuracy of newly developed ceramic materials is still being studied. Marginal and internal adaptation are known factors that have an essential impact on the long term success of dental restorations. The aim of this in vitro study was to evaluate the marginal and internal fit of heat-pressed and milled monolithic glass-ceramic restorations based on their ceramic type, processing technique, and in vitro thermocycling. Thirty-two crowns were studied and divided into four groups (n = 8), according to the ceramic material (feldspathic glass-ceramic (F) and zirconia reinforced lithium silicate glass-ceramic (ZLS)) and to their technological obtaining processes (milling (M) and heat-pressing (P)). A typodont preparation was scanned with a D2000 3D scanner to obtain identical 32 resin 3D-printed abutment teeth. Marginal and internal gaps were measured using the silicone replica technique under 40× magnification. The crowns were further cemented and thermally aged for 10,000 cycles After cementation and thermocycling of the samples, marginal and internal gaps were assessed using micro-CT (micro-computed tomography)) analysis. Data were statistically analyzed using statistical tests. Significant differences were found before and after cementation and thermocycling among the tested materials (p < 0.05). Related to technological processing, significant differences were seen in the marginal area between FP and FM (p < 0.05) Significant differences were also found in the axial and occlusal areas between the ZLSP and ZLSM. Thermocycling and cementation did not have a significant effect on the tested materials (p < 0.05). The technological processes influenced the marginal and internal fit of the crowns in favor of the CAD/CAM (computer aided design/computer aided manufacturing)technologies. Thermal aging had little effect on marginal adaptability; it increased the values for all the tested samples in a small way, but the values remained in their clinically acceptable range for all of the crowns.


Author(s):  
Youssef Y. Ashour

Background: Veneered all-ceramic restorations are associated with a high incidence of chipping and veneer delamination from the inner core. Monolithic all-ceramic crowns facilitate the fabrication process and minimize residual stresses between core and veneer. A new material,zirconia-reinforced lithium silicate(ZRL), Celtra Duo was recently introduced for fabrication of monolithic anterior crowns to overcome the aesthetic drawbacks of traditional zirconia and also to improve the strength of the lithium disilicate. Aim of the study: To examine the marginal fit of CAD/CAM: zirconia reinforced lithium disilicatand to evaluate it with Lithium silicate glass-ceramic crowns. Materials and methods: Thirty monolithic ceramic specimens will be fabricated and divided into THREE main groups; Group I: CAD/CAM ZLS Celtra Duo milled and polished, Group II CAD /CAM ZLS Celtra Duo milled and glazed & Group III: CAD/CAM Lithium silicate glass-ceramic (e.max CAD). For evaluation of the marginal fit 30 ceramic crown specimens ten specimens from each material(N=10), subgroups Ia, IIa, IIIa will be fabricated according to the manufacturers’ instructions and thermocycled to simulate one year clinical service. Marginal fit will be measured for the same specimens by using CBCT (Ia, IIa, IIIa). For evolution of marginal fit 30 ceramic crowns will be fabricated, ten crowns from each material (N=10), subgroups Ia, IIa, IIIa. Results: Will be arrangeand statistically analyzed.


Materials ◽  
2020 ◽  
Vol 13 (2) ◽  
pp. 381 ◽  
Author(s):  
Roxana-Diana Vasiliu ◽  
Sorin Daniel Porojan ◽  
Mihaela Ionela Bîrdeanu ◽  
Liliana Porojan

Dental ceramic restorations are widely spread nowadays due to their aesthetics and biocompatibility. In time, the colour and structure of these ceramic materials can be altered by aging processes. How does artificial aging affect the optical and surface roughness of ceramics? This study aims to assess the effect of thermocycling, surface treatments and microstructure upon translucency, opalescence and surface roughness on CAD-CAM and heat-pressed glass-ceramic. Forty-eight samples (1.5 mm thickness) were fabricated from six types of A2 MT ceramic: heat-pressed and milled glass-ceramic (feldspathic, lithium disilicate and zirconia reinforced lithium silicate). The samples were obtained respecting the manufacturer’s instructions. The resulted surfaces (n = 96) were half glazed and half polished. The samples were subjected to thermocycling (10,000 cycles) and roughness values (Ra and Rz), colour coordinates (L*, a*, b*) and microstructural analyses were assessed before and after thermocycling. Translucency (TP) and opalescence (OP) were calculated. Values were statistically analysed using ANOVA test (one way). TP and OP values were significantly different between heat-pressed and milled ceramics before and also after thermocycling (p < 0.001). Surface treatments (glazing and polishing) had a significant effect on TP and OP and surface roughness (p < 0.05). The heat-pressed and milled zirconia reinforced lithium silicate glass-ceramic experienced a loss in TP and OP. Ra and Rz increased for the glazed samples, TP and OP decreased for all the samples after thermocycling. Microstructural analyse revealed that glazed surfaces were more affected by the thermocycling and especially for the zirconia reinforced lithium silicate ceramic. Optical properties and surface roughness of the chosen ceramic materials were affected by thermocycling, surface treatments and microstructural differences. The least affected of the ceramics was the lithium disilicate ceramic heat-pressed polished and glazed.


1995 ◽  
Vol 78 (4) ◽  
pp. 1115-1117 ◽  
Author(s):  
Sylvia M. Johnson ◽  
Robert H. Lamoreau ◽  
Ronald E. Loehman

2019 ◽  
Vol 10 (2) ◽  
pp. 120-127
Author(s):  
Sevki Cinar ◽  
Bike Altan ◽  
Gokhan Akgungor

Objective: To compare the bond strength of monolithic CAD-CAM materials to resin cement using different surface treatment methods. Materials and Methods: Lithium disilicate glass ceramic (IPS e-max CAD), zirconia-reinforced lithium silicate ceramic (Vita Suprinity), resin nanoceramic (Lava Ultimate), and hybrid ceramic (Vita Enamic) were used. Five groups of CAD-CAM blocks were treated as follows: control (C), HF etching (HF), HF etching + silanization (HF + S), sandblasting (SB), and sandblasting + silanization (SB + S). After surface treatments, SEM analyses were conducted. Specimens were cemented with self-adhesive resin cement (Theracem) and stored in distilled water at 37°C for 24 h. Shear bond strength (SBS) was measured, and failure types were categorized. Results were analyzed using two-way ANOVA and the post-hoc Tukey test. Results: Statistical analysis revealed significant differences between SBS values obtained for different surface treatments and CAD-CAM block types ( P < .001). Among the CAD-CAM materials, the highest SBS was reported in the HF + S group for Vita Enamic. Although IPS e.max CAD, Vita Suprinity, and Vita Enamic showed higher bond strength when treated with HF + S, Lava Ultimate has the highest bond strength value when treated with SB + S. Conclusions: The bond strength of CAD-CAM materials was influenced by surface treatment. Additionally, silanization significantly improved the bond strength of all materials except Lava Ultimate.


Polymers ◽  
2019 ◽  
Vol 11 (9) ◽  
pp. 1446 ◽  
Author(s):  
Rizo-Gorrita ◽  
Herráez-Galindo ◽  
Torres-Lagares ◽  
Serrera-Figallo ◽  
Gutiérre-Pérez

Four polymer and ceramic computer-aided design/computer-aided manufacturing (CAD/CAM) materials from different manufacturers (VITA CAD-Temp (polymethyl methacrylate, PMMA), Celtra Duo (zirconia-reinforced lithium silicate ceramic, ZLS), IPS e.max CAD (lithium disilicate (LS2)), and VITA YZ (yttrium-tetragonal zirconia polycrystal, Y-TZP)) were tested to evaluate the cytotoxic effects and collagen type I secretions on human gingival fibroblasts (HGFs). A total of 160 disc-shaped samples (Ø: 10 ± 2 mm; h: 2 mm) were milled from commercial blanks and blocks. Direct-contact cytotoxicity assays were evaluated at 24, 48, and 72 h, and collagen type I (COL1) secretions were analysed by cell-based ELISA at 24 and 72 h. Both experiments revealed statistically significant differences (p < 0.05). At 24 and 48 h of contact, cytotoxic potential was observed for all materials. Later, at 72 h, all groups reached biologically acceptable levels. LS2 showed the best results regarding cell viability and collagen secretion in all of the time evaluations, while Y-TZP and ZLS revealed intermediate results, and PMMA exhibited the lowest values in both experiments. At 72 h, all groups showed sharp decreases in COL1 secretion regarding the 24-h values. According to the results obtained and the limitations of the present in vitro study, it may be concluded that the ceramic materials revealed a better cell response than the polymers. Nevertheless, further studies are needed to consolidate these findings and thus extrapolate the results into clinical practice.


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