scholarly journals Instrumented Indentation of Super-Insulating Silica Compacts

Materials ◽  
2019 ◽  
Vol 12 (5) ◽  
pp. 830 ◽  
Author(s):  
Belynda Benane ◽  
Sylvain Meille ◽  
Geneviève Foray ◽  
Bernard Yrieix ◽  
Christian Olagnon

Highly porous silica compacts for superinsulation were characterized by instrumented indentation. Samples showed a multi-scale stacking of silica particles with a total porous fraction of 90 vol %. The two main sources of silica available for the superinsulation market were considered: fumed silica and precipitated silica. The compacts processed with these two silica displayed different mechanical properties at a similar porosity fraction, thus leading to different usage properties, as the superinsulation market requires sufficient mechanical properties at the lowest density. The measurement of Young’s modulus and hardness was possible with spherical indentation, which is an efficient method for characterizing highly porous structures. Comparison of the mechanical parameters measured on silica compacts and silica aerogels available from the literature was made. Differences in mechanical properties between fumed and precipitated compacts were explained by structural organization.

CivilEng ◽  
2021 ◽  
Vol 2 (2) ◽  
pp. 523-540
Author(s):  
Imed Beghoura ◽  
Joao Castro-Gomes

This study focuses on the development of an alkali-activated lightweight foamed material (AA-LFM) with enhanced density. Several mixes of tungsten waste mud (TWM), grounded waste glass (WG), and metakaolin (MK) were produced. Al powder as a foaming agent was added, varying from 0.009 w.% to 0.05 w.% of precursor weight. Expanded granulated cork (EGC) particles were incorporated (10% to 40% of the total volume of precursors). The physical and mechanical properties of the foamed materials obtained, the effects of the amount of the foaming agent and the percentage of cork particles added varying from 10 vol.% to 40% are presented and discussed. Highly porous structures were obtained, Pore size and cork particles distribution are critical parameters in determining the density and strength of the foams. The compressive strength results with different densities of AA-LFM obtained by modifying the foaming agent and cork particles are also presented and discussed. Mechanical properties of the cured structure are adequate for lightweight prefabricated building elements and components.


2019 ◽  
Vol 274 ◽  
pp. 03002
Author(s):  
Imed Beghoura ◽  
Joao Castro-Gomes ◽  
Haroon Ihsan ◽  
John Pickstone ◽  
Nuno Estrada

Several mixes of alkali activated foams from tungsten mud waste (MW), grounded glass (GG) and metakaolin (MK) were developed incorporating expanded granulated cork (EGC). This study presents preliminary results of the expansion process obtained with the addition of aluminium (AL) powder as a foaming agent. 0.3 wt.%, 0.4 wt.% to 0.5wt.% of AL powder were added to the alkali activated matrix. The physical and mechanical properties of the obtained foams, the effects of the type and amount of the foaming agent added are presented and discussed. Highly porous structures were obtained, with overall expansion up to 68.2% when the AL powder was added. The size and distribution of pores are shown. The compressive strength of foams in the case of highly porous structures achieved of 1.2 MPa for the samples containing 0.5 wt.% of AL powder. Mechanical and thermal properties of the cured structure are good and can therefore be used for applications in acoustic panels and lightweight prefabricated components for thermal insulation purposes.


2012 ◽  
Vol 142 (9) ◽  
pp. 1061-1066 ◽  
Author(s):  
Danilo Loche ◽  
Maria F. Casula ◽  
Anna Corrias ◽  
Sergio Marras ◽  
Pietro Moggi

1991 ◽  
Vol 24 (5) ◽  
pp. 781-787 ◽  
Author(s):  
A. Emmerling ◽  
R. Gerlach ◽  
R. Goswin ◽  
J. Gross ◽  
G. Reichenauer ◽  
...  

Polymers ◽  
2021 ◽  
Vol 13 (15) ◽  
pp. 2413
Author(s):  
Mariapaola Staropoli ◽  
Vincent Rogé ◽  
Enzo Moretto ◽  
Joffrey Didierjean ◽  
Marc Michel ◽  
...  

The improvement of mechanical properties of polymer-based nanocomposites is usually obtained through a strong polymer–silica interaction. Most often, precipitated silica nanoparticles are used as filler. In this work, we study the synergetic effect occurring between dual silica-based fillers in a styrene-butadiene rubber (SBR)/polybutadiene (PBD) rubber matrix. Precipitated Highly Dispersed Silica (HDS) nanoparticles (10 nm) have been associated with spherical Stöber silica nanoparticles (250 nm) and anisotropic nano-Sepiolite. By imaging filler at nano scale through Scanning Transmission Electron Microscopy, we have shown that anisotropic fillers align only in presence of a critical amount of HDS. The dynamic mechanical analysis of rubber compounds confirms that this alignment leads to a stiffer nanocomposite when compared to Sepiolite alone. On the contrary, spherical 250 nm nanoparticles inhibit percolation network and reduce the nanocomposite stiffness.


2020 ◽  
Vol 40 (6) ◽  
pp. 2480-2488 ◽  
Author(s):  
Fei Peng ◽  
Yonggang Jiang ◽  
Junzong Feng ◽  
Liangjun Li ◽  
Huafei Cai ◽  
...  

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