scholarly journals Facile Low Temperature Hydrothermal Synthesis of BaTiO3 Nanoparticles Studied by In Situ X-ray Diffraction

Crystals ◽  
2018 ◽  
Vol 8 (6) ◽  
pp. 253 ◽  
Author(s):  
Ola Grendal ◽  
Anders Blichfeld ◽  
Susanne Skjærvø ◽  
Wouter van Beek ◽  
Sverre Selbach ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Low Temperature ◽  
X Ray Diffraction ◽  
X Ray ◽  
Batio3 Nanoparticles

Dimethyl-, Disilyl- and Digermylsulfide: Different Intermolecular Contacts in the Solid State

2004 ◽  
Vol 59 (6) ◽  
pp. 635-638 ◽  
Author(s):  
Norbert W. Mitzel ◽  
Udo Losehand
Keyword(s):  
Solid State ◽  
Low Temperature ◽  
Crystal Structures ◽  
X Ray Diffraction ◽  
X Ray ◽  
Intermolecular Contacts

The compounds (H3C)2S, (H3Si)2S and (H3Ge)2S have been crystallised in situ on a diffractometer and their crystal structures determined by low-temperature X-ray diffraction. The molecules are present as monomers in the crystals. The aggregation of the molecules through secondary intermolecular contacts in the crystal is different: (H3C)2S is weakly associated into dimers by S···S contacts, whereas (H3Si)2S and (H3Ge)2S form Si···S and Ge···S contacts in an ice-analogous aggregation motif. Important geometry parameters are (H3C)2S: C-S 1.794(av) Å , C-S-C 99.2(1)°; (H3Si)2S: Si- S 2.143(1) Å , Si-S-Si 98.4°; (H3Ge)2S Ge-S 2.223(2) and 2.230(2) Å , Ge-S-Ge 98.2(1)◦.

Hydrothermal Synthesis and in Situ Powder X-ray Diffraction Study of Bismuth-Substituted Ceria Nanoparticles

2015 ◽  
Vol 15 (8) ◽  
pp. 3628-3636 ◽  
Author(s):  
Kasper Houlberg ◽  
Espen D. Bøjesen ◽  
Christoffer Tyrsted ◽  
Aref Mamakhel ◽  
Xueqin Wang ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Diffraction Study ◽  
Ceria Nanoparticles ◽  
X Ray Diffraction ◽  
X Ray

scholarly journals In situlaser irradiation setup for a Bruker three-circle goniometer

2017 ◽  
Vol 50 (5) ◽  
pp. 1556-1558
Author(s):  
Dmitry S. Yufit
Keyword(s):  
Low Temperature ◽  
Single Crystals ◽  
Laser Irradiation ◽  
Diffraction Experiment ◽  
X Ray Diffraction ◽  
X Ray

A new design of a setup forin situlaser irradiation of single crystals during an X-ray diffraction experiment is presented. The system is designed for use with a Bruker three-circle goniometer in combination with a Helix ultra-low-temperature cryostat and consists of a laser mount and a set of three adjustable mirrors. The main advantages of the presented system include a stationary laser mount, the ability to irradiate a sample inside the Be nozzle and no impediments to the goniometer movements.

Ni/GeSn solid-state reaction monitored by combined X-ray diffraction analyses: focus on the Ni-rich phase

2018 ◽  
Vol 51 (4) ◽  
pp. 1133-1140 ◽  
Author(s):  
Andrea Quintero ◽  
Patrice Gergaud ◽  
Joris Aubin ◽  
Jean-Michel Hartmann ◽  
Vincent Reboud ◽  
...  
Keyword(s):  
Solid State ◽  
Low Temperature ◽  
Solid State Reaction ◽  
Metastable Phase ◽  
Hexagonal Structure ◽  
X Ray Diffraction ◽  
Rich Phase ◽  
X Ray ◽  
Pole Figures

The Ni/Ge0.9Sn0.1 solid-state reaction was monitored by combining in situ X-ray diffraction, in-plane reciprocal space map measurements and in-plane pole figures. A sequential growth was shown, in which the first phase formed was an Ni-rich phase. Then, at 518 K, the mono-stanogermanide phase Ni(Ge0.9Sn0.1) was observed. This phase was stable up to 873 K. Special attention has been given to the nature and the crystallographic orientation of the Ni-rich phase obtained at low temperature. It is demonstrated, with in-plane pole figure measurements and simulation, that it was the ∊-Ni5(Ge0.9Sn0.1)3 metastable phase with a hexagonal structure.

Kinetically asymmetric charge and discharge behavior of LiNi0.5Mn1.5O4 at low temperature observed by in situ X-ray diffraction

2014 ◽  
Vol 2 (37) ◽  
pp. 15414-15419 ◽  
Author(s):  
Ikuma Takahashi ◽  
Haruno Murayama ◽  
Kenji Sato ◽  
Takahiro Naka ◽  
Koji Kitada ◽  
...  
Keyword(s):  
Low Temperature ◽  
Low Temperatures ◽  
X Ray Diffraction ◽  
X Ray ◽  
Discharge Behavior

Thermodynamically reversible LiNi0.5Mn1.5O4 electrodes kinetically behave asymmetrically during charging and discharging at low temperatures.

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