scholarly journals Integrated Green Process for the Extraction of Red Grape Pomace Antioxidant Polyphenols Using Ultrasound-Assisted Pretreatment and β-Cyclodextrin

Beverages ◽  
2021 ◽  
Vol 7 (3) ◽  
pp. 59
Author(s):  
Aggeliki Alibante ◽  
Achillia Lakka ◽  
Eleni Bozinou ◽  
Arhontoula Chatzilazarou ◽  
Stavros Lalas ◽  
...  
Keyword(s):  
Antiradical Activity ◽  
Maximum Yield ◽  
Extraction Process ◽  
Extraction Methods ◽  
Grape Pomace ◽  
Waste Biomass ◽  
Total Polyphenols ◽  
Red Grape ◽  
Solid Liquid ◽  
Optimized Conditions

Winemaking is a process that generates a large volume of solid waste biomass, which is currently under extensive investigation as a bioresource of precious polyphenolic compounds. These substances are retrieved from vinification side streams principally by deploying solid–liquid extraction methods. In this frame, the present investigation had as objective the development of an alternative, green extraction process for polyphenols, through integration of ultrasonication as a pretreatment stage, and subsequent extraction with aqueous β-cyclodextrin. Polyphenol recovery from red grape pomace (RGP) was shown to be significantly enhanced by ultrasonication pretreatment, and the use of β-cyclodextrin effectively boosted the aqueous extraction. Under optimized conditions, established by response surface methodology, the maximum yield in total polyphenols was 57.47 mg GAE g−1 dm, at 80 °C, requiring a barrier of 10.95 kJ mol−1. The extract produced was significantly enriched in catechin and quercetin, compared to the aqueous extract, exhibiting also increased antiradical activity. These findings highlighted the value of the process developed for targeted recovery of certain polyphenols and the preparation of task-specific extracts.

scholarly journals Comparison between Two Solid-Liquid Extraction Methods for the Recovery of Steviol Glycosides from Dried Stevia Leaves Applying a Numerical Approach

Processes ◽  
2018 ◽  
Vol 6 (8) ◽  
pp. 105 ◽  
Author(s):  
Monica Gallo ◽  
Andrea Formato ◽  
Gaetano Formato ◽  
Daniele Naviglio
Keyword(s):  
Stevia Rebaudiana ◽  
Value Added ◽  
Numerical Approach ◽  
Extraction Process ◽  
Extraction Methods ◽  
Liquid Extraction ◽  
Steviol Glycosides ◽  
Stevia Rebaudiana Bertoni ◽  
Solid Liquid Extraction ◽  
Solid Liquid

Abstract: Stevia rebaudiana Bertoni is a perennial shrub belonging to the Asteraceae family. The leaves contain a mixture of steviol glycosides with extraordinary sweetening properties, among which the most important are stevioside and rebaudioside A. These components have a high sweetening power, which is about 300 times that of sucrose, and a negligible calorie content. However, their extraction and purification are not easy. In this paper, the extraction technique under cyclic pressure, known as rapid solid-liquid dynamic extraction (RSLDE), was compared using a Naviglio extractor (NE) with conventional maceration. The aim was to identify an efficient and economically viable method for obtaining high amounts of steviol glycosides in a short time. Furthermore, a numerical model was set up for the solid-liquid extraction process of value-added compounds from natural sources. Several parameters must be evaluated in relation to the characteristics of the parts of the plant subjected to extraction. Therefore, since diffusion and osmosis are highly dependent on temperature, it is necessary to control the temperature of the extraction system. On the other hand, the final aim of this work was to provide a scientific and quantitative basis for RSLDE. Therefore, the results obtained from stevia extracts using the corresponding mathematical model allowed hypothesizing the application of this model to the extraction processes of other vegetable matrices.

scholarly journals Citrus Bioactive Limonoid Extraction using Environment-friendly Hydrotropy

HortScience ◽  
2006 ◽  
Vol 41 (4) ◽  
pp. 1008C-1008
Author(s):  
Deepak Dandekar ◽  
G. K. Jayaprakasha ◽  
Bhimanagouda Patil
Keyword(s):  
Extraction Efficiency ◽  
Design Method ◽  
Maximum Yield ◽  
Extraction Process ◽  
Extraction Methods ◽  
Raw Material ◽  
Extraction Temperature ◽  
Optimum Conditions ◽  
Environment Friendly ◽  
Health Promoting

Citrus consumption has been shown to promote human health due to presence of several bioactive compounds. In the process of understanding the health benefits of citrus, we need to isolate and characterize these compounds. Limonoids are one of such prominent, but lesser-known phytonutrients that have been shown to prevent cancers of the mouth, skin, lung, breast, and colon. With the growing interest in the health-promoting properties of citrus limonoids, the demand for these bioactives has significantly increased. It has been critical to explore environment-friendly extraction methods rather than using hazardous organic solvents. A water-based hydrotropic extraction of limonoid aglycones from sour orange (Citrus aurantium L.) seeds was developed. Two hydrotropes, sodium salicylate (Na-Sal) and sodium cumene sulfonate (Na-CuS), were studied for extraction efficiency using the Box Behnken experiment design method. The extraction efficiency of prominent aglycone limonin was observed depending on hydrotrope concentration, extraction temperature, and percentage of raw material loading. Response Surface Analysis (RSA) of data predicted the optimum conditions for maximum yield. Recovery of aglycones from filtered extract is also easily achieved by mere dilution using water at pH 3 or 7 or by partitioning the extract with dichloromethane. At optimum conditions, limonin yield of 0.46 mg/g seeds in the case of Na-Sal extraction and 0.65 mg/g seeds in the case of Na-CuS extraction was achieved. The results demonstrated that the hydrotropic extraction process of limonoid aglycones has practical commercial importance. This project is based upon work supported by the USDA–CSREES IFAFS #2001 52102 02294 and USDA–CSREES #2005-34402-14401 “Designing Foods for Health” through the Vegetable and Fruit Improvement Center.

scholarly journals Study of Extraction Kinetics of Total Polyphenols from Curry Leaves

2021 ◽  
Vol 2021 ◽  
pp. 1-8
Author(s):  
Sunita S. Patil ◽  
Umesh B. Deshannavar ◽  
M. Ramasamy ◽  
Sampath Emani ◽  
Nima Khalilpoor ◽  
...  
Keyword(s):  
Experimental Studies ◽  
Extraction Process ◽  
Polyphenol Content ◽  
Total Polyphenols ◽  
Total Polyphenol ◽  
Batch Extraction ◽  
Total Polyphenol Content ◽  
Curry Leaves ◽  
Solid Liquid ◽  
Kinetics Of

Solid-liquid batch extraction of total polyphenol content from curry leaves (Murraya koenigii L.) was studied in this paper. The effect of different solvent concentrations and temperatures on total polyphenol content was investigated by performing batch experiments. The experimental studies showed that the kinetics of solid-liquid batch extraction was influenced by different solvent concentrations and temperatures. In solid-liquid batch extraction, more recovery of total polyphenols was obtained for 50% (v/v) aqueous methanol and at 333 K temperature. The total polyphenol obtained at optimum conditions was 79.34 mgGAE/L. Mathematical modelling is an important engineering tool used to study the kinetics of extraction as well as in the design of the extraction process to reduce time, energy, and chemical reagents. Peleg and Power law, the two mathematical models, were used to study the kinetics of the batch extraction process. The Peleg model showed the best fit to explain the kinetics of process with R2 > 0.99. Further conventional extraction methods are compared with the novel extraction method.

scholarly journals Modelling of solid-liquid extraction process of total polyphenols from soybeans

2010 ◽  
Vol 28 (No. 3) ◽  
pp. 206-212 ◽  
Author(s):  
S. Jokić ◽  
D. Velić ◽  
M. Bilić ◽  
A. Bucić-Kojić ◽  
M. Planinić ◽  
...  
Keyword(s):  
Mathematical Models ◽  
Aqueous Ethanol ◽  
Extraction Process ◽  
Extraction Yield ◽  
Liquid Extraction ◽  
Ethanol Solution ◽  
Aqueous Ethanol Solution ◽  
Total Polyphenols ◽  
Solid Liquid Extraction ◽  
Solid Liquid

The influence of the solvent, temperature, and extraction time on the extractability of total polyphenols from milled soybeans variety Ika was investigated. The study was performed in order to select the most suitable solvent (water; 50, 60, 70, and 80% aqueous ethanol) for achieving the highest yield of total polyphenols. The most effective solvent (50% aqueous ethanol solution) was used for monitoring the kinetics and modelling of solid-liquid extraction of total polyphenols from soybeans, average particle size 0.459 mm, at solid-liquid ratio of 20 ml/g (ratio of the solvent volume per g of raw material). The total polyphenols content in the soybean extract was determined spectrophotometrically using Folin-Ciocalteu micro-methods at 765 nm. The applicability of different mathematical models (Peleg, Page, and Logarithmic models) to describe the kinetics of the solid-liquid extraction process of total polyphenols from soybeans was studied as well. The results exhibited a significant influence of the solvent and temperature on the kinetics and extraction yield of total polyphenols from soybeans. The best extraction yield of total polyphenols was obtained using 50% aqueous ethanol solution at 80&deg;C after 120 min (4.322 mg GAE/g<sub>db</sub>). The extraction yield of total polyphenols in soybean extracts increased by increasing the extraction temperature and extending the duration of the extraction process. The mathematical models applied showed a good agreement with the experimental results, which allows their application in modelling and optimisation of solid-liquid extraction process for the extraction of total polyphenols from soybeans.

scholarly journals FRESHWATER SAPROPEL: BIOLOGICALLY ACTIVE COMPONENTS AND METHODS OF EXTRACTION

2020 ◽  
Vol 1 ◽  
pp. 37-46
Author(s):  
Aneka Klavina ◽  
Agris Auce ◽  
Ilona Pavlovska ◽  
Ivars Vanadzins
Keyword(s):  
Quality Criteria ◽  
Analytical Techniques ◽  
Fulvic Acids ◽  
Extraction Process ◽  
Extraction Methods ◽  
Storage Conditions ◽  
Biologically Active ◽  
Bioactive Components ◽  
Active Components ◽  
Solid Liquid

Previously, sapropel has been commonly used in agriculture, cosmetology and medicine in its raw form and there has been no generally accepted method or standard for realizing sapropel extract. However, for sapropel usage in medicine, balneology and pharmacy, it is essential to develop quality criteria for raw sapropel and its extracts. This review aims at discussing and summing up different techniques for extracting bioactive compounds from sapropel as well as the possibilities of creating quality criteria. This paper covers existing analytical techniques and methodologies; currently, there are few extraction methods using several extractants for obtaining bioactive components from raw sapropel. Different freshwater sapropel types have been described and characterized. Bioactive components in sapropel have been identified and explained. Humic acids and fulvic acids have been identified as the main substances and their extraction methods have been listed. Solid-liquid, ultrasound assisted and supercritical fluid extraction methods have been pointed out as the most suitable. Additionally, analysis and storage conditions of the extracts have been discussed. There have been found to be no commonly accepted standard methods for sapropel extraction, or for the analysis and characterization of the sapropel extracts. For pharmacological applications, a common approach for the extraction process of active substances from sapropel and the analysis procedures of the extracts need to be established. This review will help equip other researchers with the latest information on this topic.

scholarly journals Kinetics and thermodynamics of the solid-liquid extraction process of total polyphenols from barley

2014 ◽  
Vol 3 (2) ◽  
pp. 58-63 ◽  
Author(s):  
Dusan Paunovic ◽  
Snezana Mitic ◽  
Danijela Kostic ◽  
Milan Mitic ◽  
Branka Stojanovic ◽  
...  
Keyword(s):  
Extraction Process ◽  
Liquid Extraction ◽  
Total Polyphenols ◽  
Kinetics And Thermodynamics ◽  
Solid Liquid Extraction ◽  
Solid Liquid

scholarly journals Solid-State Fermentation of Aspergillus niger to Optimize Extraction Process of Isoliquiritigenin from Glycyrrhiza uralensis

2020 ◽  
Vol 2020 ◽  
pp. 1-8
Author(s):  
Jingwei Hao ◽  
Dianwei Li ◽  
Yunrong Jing ◽  
Lei Zhang ◽  
Jiahui Liu ◽  
...  
Keyword(s):  
Aspergillus Niger ◽  
Extraction Procedure ◽  
Extraction Process ◽  
Glycyrrhiza Uralensis ◽  
Liquid Ratio ◽  
Fermentation Time ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Solid Liquid ◽  
Optimized Conditions

We successfully extracted isoliquiritigenin from Glycyrrhiza uralensis via fermentation with Aspergillus niger and ultrasonic-assisted extraction. In brief, we used A. niger fermentation to culture G. uralensis powder, and we optimized some key parameters such as reaction conditions of pH, inoculation concentration of A. niger, fermentation time, and solid-liquid ratio. Based on a single-factor experiment, we utilized the response surface methodology (RSM) approach to optimize this extraction procedure. Using the RSM approach, optimized conditions of pH = 3.694, the solid-liquid ratio = 1 : 2.155, and the inoculation concentration of A. niger = 1466745 were selected. Optimized conditions resulted in an extraction efficiency of 1.525 mg/g. These results showed that the extraction of isoliquiritigenin was most affected by pH and then the time of fermentation and the solid-liquid ratio. Overall, the developed extraction technique yielded 5 times the amount of isoliquiritigenin when compared to traditional methods.

scholarly journals Microwave-assisted extraction in dry fruit of andean species Vaccinium meridionale: Experimental conditions on the recovery of total polyphenols

2017 ◽  
Vol 41 (6) ◽  
pp. 701-712 ◽  
Author(s):  
Wilfred Edilberto Espinosa ◽  
Luis Carlos Arturo Garzón ◽  
Oscar Julio Medina
Keyword(s):  
Ethanol Concentration ◽  
Aqueous Media ◽  
Extraction Process ◽  
Microwave Assisted Extraction ◽  
Total Polyphenols ◽  
Experimental Conditions ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Extraction Processes ◽  
Solid Liquid

ABSTRACT Due to their nutraceutical properties, the fruits of the species Vaccinium meridionale, which inhabit the Andean region, are of scientific interest. Microwave-assisted extraction has been applied to different vegetal matrices for to extract efficiently polyphenolic compounds. In this work we study in microwave assisted extraction processes, the effect on the extraction of total polyphenols in dried fruits of Vaccinium meridionale, using response surface methodology. The main objective of this research was to analyze the relationships between power, temperature, solid-liquid ratio, time and ethanol concentration in aqueous media on the effectiveness of total polyphenols recovery in dry fruits of Vaccinium meridionale. A central composite design face-centered with three levels for each variable was used: P = 300 - 900 W; T = 70 -110 °C; L:Srat. = 30:1 - 70:1 w/w; t = 5 - 15 min; [EtOH] = 0 - 80%. In this sense, the effect of the input variables on the recovery of total polyphenols, the optimization process for maximum extraction, and the comparison to other solid-liquid extractions in terms of quantity of total polyphenols, are reported. It was found that the significant variables in the extraction process were ethanol concentration, temperature and time; the best yields were obtained in the range [EtOH] = 44 - 49%, T = 110 °C, and t = 10 - 15 min. In terms of quantity, time and consumption of energy, microwave-assisted extraction technique is more efficient than other solid-liquid extraction processes for the extraction of total polyphenols.

scholarly journals Potential of Pre-Harvest Wastes of Tobacco (Nicotiana tabacum L.) Crops, Grown for Smoke Products, as Source of Bioactive Compounds (Phenols and Flavonoids)

2021 ◽  
Vol 13 (4) ◽  
pp. 2087
Author(s):  
Maria Isabella Sifola ◽  
Linda Carrino ◽  
Eugenio Cozzolino ◽  
Luisa del Piano ◽  
Giulia Graziani ◽  
...  
Keyword(s):  
Bioactive Compounds ◽  
Dry Weight ◽  
Waste Biomass ◽  
Total Polyphenols ◽  
Nicotiana Tabacum L ◽  
Diammonium Salt ◽  
Q Exactive ◽  
Tobacco Cultivation ◽  
Folin Assay ◽  
Final Harvest

Tobacco cultivation is characterized by high amounts of waste biomasses whose disposal frequently represents a complex and expensive problem. A study was conducted to evaluate thepotential of pre-harvest light air-cured (Burley) and dark fire-cured (Kentucky) tobacco waste biomasses as a source of bioactive compounds (nutraceutical ingredients) such as polyphenols. Pre-harvest waste materials (topping fresh materials and residual stalks at final harvest) were collected to determine dry matter, total polyphenols content (TPC; Folin assay), and DPPH (2,2-diphenyl-1-picrylhydrazyl) and ABTS (2,20-azino-bis(3-ethylbenzothiazoline-60-sulfonic acid) diammonium salt) antioxidant capacity. Polyphenols quali-quantitative profiles obtained by Orbitrap Q Exactive of both tobacco types were also determined. Total pre-harvest waste biomass amounted to 3956.9 and 1304.4 kg d.w. ha−1 in light air-cured (Burley) and dark fire-cured (Kentucky) tobacco types, respectively. Polyphenols content, expressed as g kg−1 dry weight (d.w.), ranged between 4.6 and 15.7 g kg−1 d.w. and was generally greater in leaves than in stalks. Considering both leaves and stalks, the light air-cured (Burley) tobacco crop yielded 22.1 kg ha−1 of polyphenols, while the dark fire-cured (Kentucky) tobacco yielded 12.0 kg ha−1. DPPH and ABTS were significantly greater in leaves than in stalks waste biomass in both types of tobacco. The most abundant components were quinic and chlorogenic acids, rutin, and luteolin rutinoside.

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