scholarly journals Low-Pressure Limit due to the Soft X-Ray Effect for Use of the Sub-Standard Ionization Gauge of Type VS-1

Shinku ◽  
1961 ◽  
Vol 4 (2) ◽  
pp. 68-73
Author(s):  
Katsuya NAKAYAMA
Author(s):  
Ogün Baris Tapar ◽  
Jérémy Epp ◽  
Matthias Steinbacher ◽  
Jens Gibmeier

AbstractAn experimental heat treatment chamber and control system were developed to perform in-situ X-ray diffraction experiments during low-pressure carburizing (LPC) processes. Results from the experimental chamber and industrial furnace were compared, and it was proven that the built system is reliable for LPC experiments. In-situ X-ray diffraction investigations during LPC treatment were conducted at the German Electron Synchrotron Facility in Hamburg Germany. During the boost steps, carbon accumulation and carbide formation was observed at the surface. These accumulation and carbide formation decelerated the further carbon diffusion from atmosphere to the sample. In the early minutes of the diffusion steps, it is observed that cementite content continue to increase although there is no presence of gas. This effect is attributed to the high carbon accumulation at the surface during boost steps which acts as a carbon supply. During quenching, martensite at higher temperature had a lower c/a ratio than later formed ones. This difference is credited to the early transformation of austenite regions having lower carbon content. Also, it was noticed that the final carbon content dissolved in martensite reduced compared to carbon in austenite before quenching. This reduction was attributed to the auto-tempering effect.


1969 ◽  
Vol 40 (12) ◽  
pp. 1552-1554
Author(s):  
D. L. Swingler

1995 ◽  
Vol 10 (11) ◽  
pp. 2685-2688 ◽  
Author(s):  
Qijin Chen ◽  
Zhangda Lin

Diamond film was synthesized on thin Ti wafers (as thin as 40 μm) via hot filament chemical vapor deposition (HFCVD). The hydrogen embrittlement of the titanium substrate and the formation of a thick TiC interlayer were suppressed. A very low pressure (133 Pa) was employed to achieve high-density rapid nucleation and thus to suppress the formation of TiC. Oxygen was added to source gases to lower the growth temperature and therefore to slow down the hydrogenation of the thin Ti substrate. The role of the very low pressure during nucleation is discussed, providing insight into the nucleation mechanism of diamond on a titanium substrate. The as-grown diamond films were characterized by scanning electron microscopy (SEM), Raman spectroscopy, and x-ray analysis.


2006 ◽  
Vol 39 (2) ◽  
pp. 342-346 ◽  
Author(s):  
Yongpeng Zhao ◽  
Yuanli Cheng ◽  
Bohan Luan ◽  
Yinchu Wu ◽  
Qi Wang

1950 ◽  
Vol 21 (6) ◽  
pp. 571-572 ◽  
Author(s):  
Robert T. Bayard ◽  
Daniel Alpert

2019 ◽  
Vol 965 ◽  
pp. 125-132
Author(s):  
Gabriela H.G. Santos ◽  
Maíra A. Rodrigues ◽  
Helen Conceição Ferraz ◽  
Luiza Cristina Moura ◽  
Jussara Lopes de Miranda

Membrane separation technology has been recently attracted more attention as an option for gas separations due to its compact system, ease of operation and low power consumption. In this study, polymer membranes with different percentages of polyurethane were synthesized and submitted to permeability and selectivity tests for the following gases, CO2, N2, O2 and CH4, at two pressures of 4 and 8 bar and at room temperature. The membranes were characterized by FTIR-ATR, Scanning electron microscope (SEM), Thermogravimetric analysis (TGA) and X-ray diffractometer (XRD). At low pressure of 4 bar and room temperature, the membrane with low percentage of PU, 10 %, presented the higher selectivity to CO2 in relation to both N2 and CH4. The same behavior was observed at a high pressure of 8 bar, with higher selectivity to CO2 in relation to all studied gases, N2, O2 and CH4, compared to the already analogous reported membranes submitted at greater pressures.


Nanoscale ◽  
2019 ◽  
Vol 11 (2) ◽  
pp. 752-761 ◽  
Author(s):  
Axel Wilson ◽  
Aude Bailly ◽  
Romain Bernard ◽  
Yves Borensztein ◽  
Alessandro Coati ◽  
...  

Au–Cu bimetallic nanoparticles (NPs) grown on TiO2(110) have been followed in situ using grazing incidence X-ray diffraction and X-ray photoemission spectroscopy from their synthesis to their exposure to a CO/O2 mixture at low pressure (P < 10−5 mbar) and at different temperatures (300 K–470 K).


1990 ◽  
Vol 193-194 ◽  
pp. 1079-1086 ◽  
Author(s):  
A.R Chourasia ◽  
D.R Chopra ◽  
S.C Sharma ◽  
M Green ◽  
C.A Dark ◽  
...  

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