scholarly journals Arc Plasma Deposition of TiO2 Nanoparticles from Colloidal Solution

10.30544/587 ◽  
2020 ◽  
Vol 26 (4) ◽  
pp. 341-348
Author(s):  
Vesna Maksimović ◽  
Milovan Stoiljković ◽  
Vladimir Pavkov ◽  
Jovan Ciganović ◽  
Ivana Cvijović‐Alagić

Surface modifications of metallic biomaterials can in great merit, improve the properties of the hard-tissue implants and in that way contribute to the success of the surgical implantation process. Coating deposition stands out as one of the many surface-modifying techniques that can be used to improve implant surface properties and, in turn, induce successful osseointegration. Deposition of the TiO2 layer on the surface of the metallic implants has a great potential to enhance not only their osseointegration ability but also their biocompatibility and corrosion resistance. In the present study, the possibility of successful deposition of the TiO2 layer on the surface of commercially pure titanium (CP-Ti), as the most commonly used metallic implant material, by spraying the colloidal nanoparticles aqueous solution in the electric discharge plasma at atmospheric pressure was investigated. To characterize the colloidal TiO2 nanoparticle solution, used for the coating deposition process, transmission electron microscopy (TEM) was utilized, while scanning electron microscopy (SEM) and optical profilometry were used to investigate the deposited surface layer morphology and quality. Estimation of the deposited film quality and texture was used to confirm that the arc plasma deposition technique can be successfully used as an advanced and easy-to-apply method for coating the metallic implant material surface with the bioactive TiO2 layer which favors the osseointegration process through the improvement of the implant surface properties. The TiO2 coating was successfully deposited using the arc plasma deposition technique and covered the entire surface of the CP-Ti substrate without any signs of coating cracking or detachment.

2011 ◽  
Vol 1307 ◽  
Author(s):  
M. Sajjad ◽  
H. X. Zhang ◽  
P. X. Feng

ABSTRACTThe synthesis of boron nitride nanowires on silicon (Si) and nanorods on molybdenum (Mo) substrates at the same experimental conditions was composed. Fine tip nanowires with diameters around 50 nm were produced on Si substrates, whereas, nanorods with diameter around 100 nm were formed on Mo substrates. The change in length from 5 μm to 100 μm for nanowires and 0.2 μm to 0.8μm for nanorods following variation of substrate temperature were studied systematically.Scanning Electron Microscopy was used to analyze the surface images of BN nanowires and nanorods. Energy Dispersive X-Ray spectroscopy (EDS) was used to analyze boron and nitrogen concentration in the samples. The crystal structures of BN samples were investigated using Raman spectroscopy and x-ray diffraction. The experimental results showed that the nanorods are hexagonal mixed with cubic, whereas the nanowires are hexagonal.


1995 ◽  
Vol 388 ◽  
Author(s):  
André Anders ◽  
Simone Anders ◽  
Ian G. Brown ◽  
Igor C. Ivanov

AbstractCathodic arc plasma deposition was used to coat Al2O3 powder (mesh size 60) with platinum. the power particles were moved during deposition using a mechanical system operating at a resonance frequency of 20 Hz. Scanning electron microscopy and auger electron microscopy show that all particles are completely coated with a platinum film having a thickness of about 100 nm. the actual deposition time was only 20 s, thus the deposition rate was very high (5 nm/s).


2011 ◽  
Vol 47 (4) ◽  
pp. 512-516
Author(s):  
Z. Iqbal ◽  
A. Ali ◽  
A. Rauf ◽  
A. ul Haq ◽  
S. Tajammul Hussain ◽  
...  

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
N. Saikumari ◽  
S. Monish Dev ◽  
S. Avinaash Dev

AbstractIn order to deal with the arising environmental issues across the globe at present nano particles with unique properties laid a benchmark in the name of nano catalysis. In this work the significance of calcination temperature on the thermal, electronic, structural and surface properties of a nano catalyst produced by sol–gel method using ultrasonic radiation against the disposal of toxic textile pollutants is studied in detail. The extract of tea leaves has been used as a bio-template during the synthesis to revise the crystallite size, surface area, optical absorption potential, and rate of agglomeration of nano sized grains by regulating their physico-chemical and surface properties. The influence of calcination in the transformation of single phased anatase titania to mixed phase anatase–rutile titania and the corresponding outcome in its photocatalytic activity employed in water treatment applications have been verified. The nano catalyst obtained is characterized by X-ray diffraction (XRD), Scanning electron microscopy (SEM), Transition electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR), Thermo gravimetric analysis (TGA), Brunaueur Emmett Teller (BET) analysis, UV–Vis diffused reflectance spectroscopy (DRS-UV–Vis) etc. The mesoporosity of the particle was examined using Barrett Joyner Halenda (BJH) model. The enhanced photo catalytic efficiency (about 97.7%) of templated nano titania due to calcination is verified against Congo red, a textile dye under optimized conditions. The nano catalyst produced can be easily separated, recycled to support its economic feasibility.


2016 ◽  
Vol 57 (2) ◽  
pp. 207-211 ◽  
Author(s):  
Daiki Horiyama ◽  
Masashi Matsuura ◽  
Tetsuro Yamamoto ◽  
Nobuki Tezuka ◽  
Satoshi Sugimoto

2017 ◽  
Vol 60 (12-14) ◽  
pp. 955-961 ◽  
Author(s):  
Satoshi Misumi ◽  
Hiroshi Yoshida ◽  
Akinori Matsumoto ◽  
Satoshi Hinokuma ◽  
Tetsuya Sato ◽  
...  

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