scholarly journals PRE-TREATMENT OF INDUSTRIAL MINERAL OIL WASTEWATER USING RESPONSE SURFACE METHODOLOGY

2017 ◽  
Author(s):  
EMMANUEL KWEINOR TETTEH ◽  
SUDESH RATHILAL ◽  
MARTHA NORO CHOLLOM
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Mineral Oil ◽  
Industrial Mineral ◽  
Pre Treatment ◽  
Oil Wastewater

scholarly journals Effects of a polymeric organic coagulant for industrial mineral oil wastewater treatment using response surface methodology (RSM)

Water SA ◽  
2018 ◽  
Vol 44 (2 April) ◽  
Author(s):  
E Kweinor Tetteh ◽  
S Rathilal
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Mineral Oil ◽  
Chemical Oxidation ◽  
Water Soluble ◽  
Oil Droplets ◽  
Flotation Process ◽  
Coagulant Dosage ◽  
Oil Wastewater ◽  
Response Variables

In this study, treatment of a local South African oil refinery effluent using a coagulation flotation process is designed using response surface methodology (RSM). A Box-Behnken design (BBD) implementing the RSM is applied to evaluate the effects and interactions of three operating parameters, viz., pH, coagulant dosage and flotation time, on the treatment of mineral oil wastewater (MOW). Polyacrylamide (Zetag-FS/A50), which is a water-soluble compound, is applied to enhance the adsorption mechanism and intermolecular bridging to minimise the amount of oil droplets. In addition, due to the monomeric nature and the charge density of the Zetag-FS/A50, its efficiency was evaluated to serve as an alternative coagulant for the pretreatment of the MOW. The removal of chemical oxidation demand (COD), soap oil and grease (SOG), total suspended solids (TSS) and turbidity from the MOW were used as the response variables for the coagulation flotation process. This was done with a standard dissolved air flotation jar test. The results show that the actual COD, SOG, TSS and turbidity percentage removal at optimised conditions with a coagulant dosage of 50 mg/L were 82%, 83%,70% and 83% respectively, while the predicted response was 92%, 96%, 73% and 87% for COD, SOG, TSS and turbidity, respectively. The analysis of variance (ANOVA) showed that the proposed models are significant at a 95% confidence level. A quadratic model was generated for response variables COD and SOG, while TSS and turbidity produced a linear model. The models fitted well with the experimental data with correlation coefficients (actual R2) of 0.94 for COD, 0.91 for SOG, 0.81 for TSS, and 0.75 for turbidity. The outcome of the study shows that the RSM has merit to optimise and identify the most important factor to control and the Zetag-FS/A50 coagulant has the potential to adsorb the oil droplets in order to enhance the treatment efficiency of the process.

Enzyme-assisted Extraction for Optimized Recovery of Phenolic Bioactives from Peganum hermala Leaves Using Response Surface Methodology

2018 ◽  
Vol 17 (4) ◽  
pp. 349-354
Author(s):  
Qadir Rahman ◽  
Anwar Farooq ◽  
Amjad Gilani Mazhar ◽  
Nadeem Yaqoob Muhammad ◽  
Ahmad Mukhtar
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Enzyme Concentration ◽  
Coumaric Acid ◽  
Assisted Extraction ◽  
Pre Treatment ◽  
Optimized Conditions ◽  
Enzyme Complexes ◽  
Hydrolysis Of ◽  
Central Composite

This study investigates the effect of enzyme formulations (Zympex-014, Kemzyme dry-plus and Natuzyme) on recovery of phenolics from Peganum hermala (harmal) leaves, under optimized conditions using response surface methodology. As compared to the other enzyme complexes, the yield (34 g/100g) obtained through Zympex-014-assisted extraction was higher under optimized conditions such as time (75 min), temperature (70°C), pH (6.5) and enzyme concentration (5 g/100 g) using central composite design (CCD). Effectiveness of Zympex-014 towards hydrolysis of P. hermala leaves cell wall was examined by analyzing the control and enzyme-treated leave residues using scanning electron microscope (SEM). GC/MS characterization authenticated the presence of quercetin (1.44), gallic acid (0.23), caffeic acid (0.04), cinnamic acid (0.05), m-coumaric acid (0.23) and p-coumaric acid (0.37 μg/g) as the potent phenolics in Zympex-014 based extract. It can be concluded from the findings of the current work that pre-treatment of P. hermala leaves with Zympex-014 significantly enhanced the recovery of phenolics that supports its potential uses in the nutra-pharamaceutical industry.

scholarly journals Treatment of industrial mineral oil wastewater – effects of coagulant type and dosage

2017 ◽  
Vol 12 (1) ◽  
pp. 139-145 ◽  
Author(s):  
E. Kweinor Tetteh ◽  
S. Rathilal ◽  
K. Robinson
Keyword(s):  
Oxygen Demand ◽  
Mineral Oil ◽  
Quality Parameters ◽  
Oil Refinery ◽  
Oil And Grease ◽  
Water And Wastewater Treatment ◽  
Dissolved Air Flotation ◽  
Jar Test ◽  
Industrial Mineral ◽  
Oil Wastewater

The use of coagulants is essential in the diverse disciplines of conventional water and wastewater treatment. This work aimed to select an economic and effective coagulant, to minimize the cost of treatment and the oil droplet content of the water, thus enhancing the efficiency of a local South African oil refinery effluent plant recovering water and oil for reuse by treating the industrial mineral oil wastewater. A standard dissolved air flotation jar test preceded evaluation of four coagulants, viz. aluminum sulfate (Alum), aluminum chloride, ferric sulfate and ferric chloride. Chemical oxygen demand, soap oil and grease, total suspended solids and turbidity were determined as water quality parameters to check coagulant efficiency. Removal of over 70% was achieved for each parameter. The results obtained at pH 5 and coagulant dose of 50 mg/L showed that alum was the best pretreatment coagulant for destabilizing and minimizing oil droplets in water, due to its trivalent cationic nature. It was also economically viable.

ASSESSING THE TRIBOLOGICAL PROPERTIES OF VEGETABLE OIL EMULSIONS AND MACHINING PARAMETER OPTIMIZATION USING RESPONSE SURFACE METHODOLOGY

2021 ◽  
Author(s):  
D. K. KARUPANNASAMY ◽  
M. SAMBATHKUMAR ◽  
R. GUKENDRAN ◽  
K. S. K. SASIKUMAR ◽  
N. BAASKARAN ◽  
...  
Keyword(s):  
Response Surface Methodology ◽  
Tool Wear ◽  
Response Surface ◽  
Surface Finish ◽  
Castor Oil ◽  
Mineral Oil ◽  
Machining Process ◽  
Neem Oil ◽  
Machining Performance ◽  
Oil Emulsions

Bio-degradable lubricants are the need for industries to promote eco-friendly manufacturing process and protect the workers from health hazards. In this paper, the use of oil–water emulsions from the bio-substitute oils have been formulated and its process parameter on a machining process are optimized using response surface methodology. The emulsions are prepared from the vegetable oils such as castor, mahua, palm and neem oil with polysorbate as emulsifying agent. The friction and wear characteristics are studied with a standard pin on disc tribometer for all the emulsions prepared with the base oils namely castor, mahua and palm oil. From the tribological characterization tests, the castor oil emulsions have shown better performance and stability in comparison to other oils. Hence, castor oil emulsions have been tested for its machining performance studies against a conventional mineral oil emulsion in a turning process. Further, an emulsion based on castor oil and neem oil have been tested for tool wear to utilize the antimicrobial properties of neem oil for reducing the bio fouling effects. The machining performance is indicated based on the surface finish and tool wear. Response surface methodology have been used for optimization of the machining parameters, such as cutting velocity, feed rate and depth of cut to achieve an optimal surface finish for a maximum material removal rate. The results show that the castor oil based emulsion can be used as an excellent alternative for mineral oil emulsions.

scholarly journals Response surface methodology for the optimization of sludge solubilization by ultrasonic pre-treatment

2018 ◽  
Vol 113 ◽  
pp. 012177
Author(s):  
Mingyue Zheng ◽  
Xiaohui Zhang ◽  
Peng Lu ◽  
Qiguang Cao ◽  
Yuan Yuan ◽  
...  
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Pre Treatment

scholarly journals Collagen Extraction Optimization from the Skin of the Small-Spotted Catshark (S. canicula) by Response Surface Methodology

Marine Drugs ◽  
2019 ◽  
Vol 17 (1) ◽  
pp. 40 ◽  
Author(s):  
María Blanco ◽  
José Antonio Vázquez ◽  
Ricardo I. Pérez-Martín ◽  
Carmen G. Sotelo
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Extraction Procedure ◽  
Amino Acid Content ◽  
Combined Effect ◽  
Human Consumption ◽  
Concentration Time ◽  
Sds Page ◽  
Skin Collagen ◽  
Pre Treatment

The small-spotted catshark is one of the most abundant elasmobranchs in the Northeastern Atlantic Ocean. Although its landings are devoted for human consumption, in general this species has low commercial value with high discard rates, reaching 100% in some European fisheries. The reduction of post-harvest losses (discards and by-products) by promotion of a full use of fishing captures is one of the main goals of EU fishing policies. As marine collagens are increasingly used as alternatives to mammalian collagens for cosmetics, tissue engineering, etc., fish skins represent an excellent and abundant source for obtaining this biomolecule. The aim of this study was to analyze the influence of chemical treatment concentration, temperature and time on the extractability of skin collagen from this species. Two experimental designs, one for each of the main stages of the process, were performed by means of Response Surface Methodology (RSM). The combined effect of NaOH concentration, time and temperature on the amount of collagen recovered in the first stage of the collagen extraction procedure was studied. Then, skins treated under optimal NaOH conditions were subjected to a second experimental design, to study the combined effect of AcOH concentration, time and temperature on the collagen recovery by means of yield, amino acid content and SDS-PAGE characterization. Values of independent variables maximizing collagen recovery were 4 °C, 2 hours and 0.1 M NaOH (pre-treatment) and 25 °C, 34 hours and 1 M AcOH (collagen extraction).

A Thermomechanical Preprocessing for Pectin Isolation from Orange Peel with Optimisation by Response Surface Methodology

2008 ◽  
Vol 4 (1) ◽  
Author(s):  
Sid-Ahmed Rezzoug ◽  
Zoulikha Maache-Rezzoug ◽  
Frédéric Sannier ◽  
Karim Allaf
Keyword(s):  
Response Surface Methodology ◽  
Moisture Content ◽  
Response Surface ◽  
Processing Time ◽  
Initial Moisture Content ◽  
Control Sample ◽  
Orange Peel ◽  
Response Surfaces ◽  
Acid Extraction ◽  
Pre Treatment

The instantaneous controlled pressure drop process (or D.I.C process: ``Détente Instantanée Contrôlée") was used as a pre-treatment prior to pectin acid extraction from orange peel. This process involves subjecting the orange peel for a short time to steam pressure varying from 100 to 700 kPa, followed by an instantaneous decompression to vacuum at 5 kPa. Effects of processing pressure, moisture content of peels before the thermomechanical treatment and processing time were examined with response surface methodology. The optimal conditions were determined and the response surfaces were plotted from the mathematical models. The Fisher test and p-value indicated that both processing pressure and moisture content of peels before the pre-treatment had a highly significant effect on the pectin yield. The quadratic effect of processing pressure as well as the interaction effects of the initial moisture content and processing time also had a significant effect on the response. Moreover, the kinetics of pectin extraction showed that after few minutes of hydrolysis, the yields of pectin were systematically higher than that of the control sample and this is important from industrial point of view because the hydrolysis of pectin is generally performed in 10-15 minutes.

scholarly journals Optimization of Oil Removal by Sugarcane Bagasse using Response Surface Methodology

2021 ◽  
Vol 4 (2) ◽  
pp. 82-87
Author(s):  
Asilah Ahmad Samsuir ◽  
Norhisyam Ismail ◽  
Rozidaini Mohd Ghazi
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Sugarcane Bagasse ◽  
Contact Time ◽  
Oil Pollution ◽  
Oil Removal ◽  
Industrial Growth ◽  
Synthetic Oil ◽  
Exploration And Production ◽  
Oil Wastewater

Oily wastewater is one of the environmental concerns nowadays. The seriousness of oil pollution problem comes in sync with the expansion of oil exploration and production activities, as well as industrial growth around the world. In this study, the ability of sugarcane bagasse in removing oil in synthetic oil wastewater was investigated. Parameters affecting oil removal such as concentrations of synthetic oil wastewater, biosorbent dosage and contact time were optimized using Response Surface Methodology (RSM) via Box Behnken Design. Sugarcane bagasse showed excellent efficiency in removing oil with percentage removal up to 98.73% at 1.3 h contact time with 3.06 g of biosorbent dosage and 16.9% of synthetic oil wastewater concentration. The use of sugarcane bagasse in removing oil in water was successfully prove in this study.

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