scholarly journals Influence of the Curing Mode on Fluoride Ion Release of Self-adhesive Resin Luting Cements in Water or During pH-Cycling Regimen

2012 ◽  
Vol 37 (1) ◽  
pp. 63-70 ◽  
Author(s):  
TR Aguiar ◽  
CF Pinto ◽  
V Cavalli ◽  
M Nobre-dos-Santos ◽  
GMB Ambrosano ◽  
...  
Keyword(s):  
The Self ◽  
Fluoride Ion ◽  
Fluoride Release ◽  
Ion Release ◽  
Resin Cements ◽  
Experimental Conditions ◽  
Adhesive Resin ◽  
Luting Cements ◽  
Release Capacity ◽  
Ph Cycling

Clinical Relevance Within the limited experimental conditions, the self-adhesive cements provided fluoride ion release capacity. The fluoride release for all resin cements was not uniform during pH cycling, decreasing throughout the duration of the study.

Microleakage of All-ceramic Crowns Using Self-etching Resin Luting Agents

2008 ◽  
Vol 33 (4) ◽  
pp. 392-399 ◽  
Author(s):  
C. P. Trajtenberg ◽  
S. J. Caram ◽  
S. Kiat-amnuay
Keyword(s):  
Clinical Relevance ◽  
The Self ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Luting Agents ◽  
Relyx Unicem ◽  
All Ceramic ◽  
Ceramic Crowns ◽  
Die Spacer

Clinical Relevance Among the self-adhesive resin cements, Panavia F 2.0 demonstrated less microleakage than RelyX Unicem or Multilink, whether or not a die spacer technique was used.

scholarly journals Effects of Polymerization Mode and Interaction with Hydroxyapatite on the Rate of pH Neutralization, Mechanical Properties, and Depth of Cure in Self-Adhesive Cements

2019 ◽  
Vol 13 (02) ◽  
pp. 178-186
Author(s):  
Fabiana S. A. S. Camargo ◽  
Alejandra H. M. González ◽  
Roberta C. B. Alonso ◽  
Vinicius Di Hipólito ◽  
Paulo H. P. D'Alpino
Keyword(s):  
Mechanical Properties ◽  
Infrared Spectroscopy ◽  
Elastic Modulus ◽  
Flexural Strength ◽  
The Self ◽  
Chemical Bonds ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Depth Of Cure ◽  
Ph Neutralization

Abstract Objective The aim of the study was to evaluate the physicochemical properties of self-adhesive resin cements associated with hydroxyapatite (HAp) according to the polymerization activation. Materials and Methods Specimens of cements (PermaCem 2.0 [DMG]; MaxCem Elite [Kerr], and RelyX U200 [3M ESPE]) were distributed into three groups: activation mode; self-cured and dual-cured modes; and association or not with HAp powder mode. The pH neutralization was evaluated as a function of time. Flexural strength and elastic modulus were also tested (0.5 mm/min.). The depth of cure was also analyzed using the scraping test (ISO 4049). Infrared spectroscopy was also used to collect the spectra of specimens to evaluate the chemical bonds. Statistical comparisons were conducted at 5% of significance. Results The aggressiveness of the self-adhesive resin cements evaluated varied among the materials with a tendency for neutralization. Self-cure groups exhibited lower pH throughout the entire evaluation when compared with that of the dual-cure ones, irrespective of the addition of HAp. MaxCem Elite when photoactivated was the only cement influenced by the addition of the HAp in terms of mechanical properties. The self-adhesive cements tested presented equivalent depth of cure based on the ISO 4049 requirements, regardless of the evaluated factors. Conclusions Based on the parameters evaluated, the results demonstrated that most of the self-adhesive cements remained unaltered or improved when mixed with HAp, regardless of the activation mode.

scholarly journals Influence of Relining Post on the Bond Strength of Resin Cements

2015 ◽  
Vol 16 (7) ◽  
pp. 559-564 ◽  
Author(s):  
Matheus Coelho Bandéca ◽  
Adriano Augusto Melo de Mendonça ◽  
Etevaldo Matos Maia Filho ◽  
Fausto da Silva Bramante ◽  
Darlon Martins Lima ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Cement ◽  
The Self ◽  
Fiber Post ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Fiber Posts ◽  
Significant Difference ◽  
Adhesive Cement ◽  
Push Out

ABSTRACT This study evaluated the influence of relining fiber posts on the bond strength (BS) of resin cements in the root canal. Forty bovine teeth were divided in four groups (n = 10)G1 (ARC)—fiber post cemented with resin cement RelyX ARC; G2 (ARC+Z350)—relined fiber post cemented with RelyX ARC; G3 (U200)—fiber post cemented with self-adhesive cement RelyX U200; G4 (U200+Z350)—relined fiber post cemented with RelyX U200. The roots were sectioned in six 1.2-mm slices and the push-out test was performed. Data were analyzed by three-way analysis of variance (ANOVA), and Tukey's test (α = 0.05). For the conventional resin cement, there was no significant difference between groups G1-ARC (15.5 ± 3.8) and G2-ARC+Z350 (16.1 ± 4.5). For the self-adhesive cement, the results revealed higher BS values for relined posts G4-U200 + Z350 (19.9 ± 7.9) as compared to non-relined posts G3-U200 (14.4 ± 4.5). For both cements, in groups of relined posts, the apical and the cervical thirds presented similar BS. Relining enhances the performance of the self-adhesive resin cement, and the interaction between relining and root third influences the BS to the conventional resin cement. How to cite this article Conde DM, Rodrigues VP, de Fátima Carvalho Souza S, Bauer JRO, da Silva Bramante F, Lima SNL, Filho EMM, Bandeca MC, de Mendonça AAM, Lima DM. Influence of Relining Post on the Bond Strength of Resin Cements. J Contemp Dent Pract 2015;16(7):559-564.

scholarly journals Mechanical Properties and Sliding-impact Wear Resistance of Self-adhesive Resin Cements

2016 ◽  
Vol 41 (3) ◽  
pp. E83-E92 ◽  
Author(s):  
T Furuichi ◽  
T Takamizawa ◽  
A Tsujimoto ◽  
M Miyazaki ◽  
WW Barkmeier ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Wear Resistance ◽  
Elastic Modulus ◽  
Flexural Strength ◽  
Sliding Wear ◽  
Resin Cement ◽  
The Self ◽  
Volume Loss ◽  
Resin Cements ◽  
Adhesive Resin

SUMMARY The present study determined the mechanical properties and impact-sliding wear characteristics of self-adhesive resin cements. Five self-adhesive resin cements were used: G-CEM LinkAce, BeautiCem SA, Maxcem Elite, Clearfil SA Automix, and RelyX Unicem 2. Clearfil Esthetic Cement was employed as a control material. Six specimens for each resin cement were used to determine flexural strength, elastic modulus, and resilience according to ISO specification #4049. Ten specimens for each resin cement were used to determine the wear characteristics using an impact-sliding wear testing apparatus. Wear was generated using a stainless-steel ball bearing mounted inside a collet assembly. The maximum facet depth and volume loss were determined using a noncontact profilometer in combination with confocal laser scanning microscopy. Data were evaluated using analysis of variance followed by the Tukey honestly significantly different test (α=0.05). The flexural strength of the resin cements ranged from 68.4 to 144.2 MPa; the elastic modulus ranged from 4.4 to 10.6 GPa; and the resilience ranged from 4.5 to 12.0 MJ/m3. The results for the maximum facet depth ranged from 25.2 to 235.9 μm, and volume loss ranged from 0.0107 to 0.5258 mm3. The flexural properties and wear resistance were found to vary depending upon the self-adhesive resin cement tested. The self-adhesive cements tended to have lower mechanical properties than the conventional resin cement. All self-adhesive resin cements, apart from G-CEM LinkAce, demonstrated significantly poorer wear resistance than did the conventional resin cement.

Effect of CaF2 Content on Rate of Fluoride Release from Filled Resins

2005 ◽  
Vol 84 (5) ◽  
pp. 440-444 ◽  
Author(s):  
K.J. Anusavice ◽  
N.-Z. Zhang ◽  
C. Shen
Keyword(s):  
Filler Content ◽  
Particle Surface ◽  
Triethylene Glycol ◽  
Resin Matrix ◽  
Fluoride Ion ◽  
Fluoride Release ◽  
Ion Release ◽  
Buffer Solution ◽  
Solution Ph ◽  
Particle Surface Area

Information on the time-dependent release of fluoride from filled resins containing fluoride particles as a function of particle content and solution pH is limited. This study characterized the fluoride ion release from filled resins containing CaF2 particles as a function of filler content and pH. Urethane dimethacrylate and triethylene glycol dimethacrylate resins were used to make filled-resin disks containing 9.09, 23.08, or 33.33 mass% CaF2 filler. Fluoride ion release for the 9.09 mass% concentration was independent of pH. Increasing the filler content from 9.09 to 33.33 mass% increased the fluoride release rate in pH 4.0 buffer solution, because of greater surface degradation. Fluoride ion release from disks stored in pH 6.0 buffer solutions occurred mainly by diffusion from disk surfaces, while fluoride release from disks in pH 4.0 buffers was controlled by diffusion from disk surfaces and degeneration of the resin matrix, which exposed more CaF2 particle surface area.

Influence of Post-cure Time on the Microhardness of Self-Adhesive Resin Cements Inside the Root Canal

2012 ◽  
Vol 37 (5) ◽  
pp. 548-556 ◽  
Author(s):  
E Baena ◽  
MV Fuentes ◽  
MA Garrido ◽  
J Rodríguez ◽  
L Ceballos
Keyword(s):  
Root Canal ◽  
Acrylic Resin ◽  
Resin Cement ◽  
The Self ◽  
Polymerization Reaction ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Fiber Posts ◽  
Relyx Unicem ◽  
Cure Time

SUMMARY Purpose To compare the microhardness of several dual-cure, self-adhesive resin cements used to lute fiber posts at 24 hours and seven days after cementation. Methods Bovine incisors were selected to lute 15 fiber posts that were 12 mm long (FRC Postec Plus size 3, Ivoclar-Vivadent). Five resin cements were tested: Multilink Automix (Ivoclar-Vivadent), without light-curing, and the self-adhesive resin cements Maxcem Elite (Kerr), RelyX Unicem (3M ESPE), G-Cem (GC), and Smartcem 2 (Dentsply), which were light-cured for 40 seconds (LED Bluephase, Ivoclar-Vivadent). Each root was embedded in chemically cured acrylic resin and stored at 37°C for 24 hours. The roots were transversally sectioned into nine specimens that were each 1 mm thick, with three specimens corresponding to each root third. Indentations (100g, 30 seconds) were performed on each section in the resin cement, at 24 hours and seven days after cementation, using a Vickers digital microdurometer (Buehler). Data were analyzed by two-way analysis of variance, Student-Newman-Keuls test, and paired t-test (p<0.05). Results A significant influence was found (p<0.05) for the resin cement evaluated, the root third, and their interactions on microhardness values at 24 hours and seven days after post cementation. RelyX Unicem and G-Cem exhibited the highest microhardness values, whereas Multilink Automix presented the lowest. All resin cements suffered a decrease in microhardness according to root canal depth, with the exception of G-Cem and Multilink Automix at 24 hours and Smartcem 2 after seven days. After seven days, the evaluated resin cements showed a significant increase in microhardness values, with the exception of Maxcem Elite and Smartcem 2 at the coronal third. Conclusions Microhardness of the self-adhesive resin cements when used to lute fiber posts was material-dependent and higher values were obtained in the coronal third, revealing their sensitivity to light irradiation. More information regarding the polymerization reaction of these cements is warranted. According to the current results, microhardness values were significantly higher one week after post luting.

scholarly journals Fluoride Release/Uptake from Different Orthodontic Adhesives: A 30-Month Longitudinal Study

2013 ◽  
Vol 24 (4) ◽  
pp. 410-414 ◽  
Author(s):  
Rogerio Lacerda dos Santos ◽  
Matheus Melo Pithon ◽  
Aline Birra Nolasco Fernandes ◽  
Fabiola Galbiatti Carvalho ◽  
Alessandro Leite Cavalcanti ◽  
...  
Keyword(s):  
Null Hypothesis ◽  
Fluoride Ion ◽  
Fluoride Release ◽  
Glass Ionomer ◽  
Bonferroni Correction ◽  
Time Intervals ◽  
Orthodontic Adhesives ◽  
Release Capacity ◽  
Resin Modified Glass Ionomer

The aim of this study was to test the null hypothesis that there is no difference in fluoride release between resin-modified glass ionomer cements (RMGICs) and composites in the long term. The materials were divided into 5 groups: a nonfluoride-releasing composite - Group TXT (Transbond XT), a fluoride-releasing composite - Group QC (Quick-Cure), and three RMGICs - Groups FOLC, FOB and MC (Fuji Ortho LC, Fuji Ortho Band, and Multi-Cure). Fluoride release was measured at time intervals of 1 h, 1, 7, 14, 21 and 29 days, followed by further evaluations performed at 6, 12, 18, 24 and 30 months using selective ion electrodes connected to an ionic analyzer. Fluoride releasing and re-releasing experiments were analyzed using the Kruskal-Wallis test and Mann-Whitney test with the Bonferroni correction. The amount of fluoride released by FOB was larger in comparison with the other adhesives (p=0.01). In the long-term, FOLC and MC had a similar performance (p>0.05). The composites presented a low fluoride release, but fluoride ion uptake and re-release capacity of QC was statistically significant (p<0.05) during the experiment. In conclusion, the null hypothesis was rejected, the RMGIC Fuji Ortho Band and the composite Quick-Cure presented greater fluoride release and re-release capacity when recharged.

scholarly journals Fluoride Ion Release Characteristics of Fluoride-Containing Varnishes—An In Vitro Study

2021 ◽  
Vol 11 (4) ◽  
pp. 1452
Author(s):  
Sachin Chhatwani ◽  
Jennifer Hoppe ◽  
Ella A. Naumova ◽  
Wolfgang H. Arnold ◽  
Stephan C. Möhlhenrich ◽  
...  
Keyword(s):  
Single Dose ◽  
In Vitro Study ◽  
White Spot ◽  
Control Group ◽  
Fluoride Ion ◽  
Fluoride Release ◽  
White Spot Lesions ◽  
Ion Release ◽  
One Step

Despite the latest advances in orthodontic treatment, white spot lesions remain a common side effect of fixed appliance therapy. An effective treatment for the prevention of white spot lesions is the use of fluoride-containing products. The aim of the present in vitro study was to check the durability of the tested products for their fluoride release into the surrounding solution. Three varnishes (Protecto CaF2 Nano one-step seal, Bifluorid 12 single dose, and Fluor Protector S) were applied to hydroxyapatite discs and kept in diluted Total Ionic Strength Adjustment Buffer III (TISAB III) solution for fluoride ion release measurement. A group of clear hydroxyapatite discs served as the control group. The carrier discs (N = 40) underwent three thermal cycling runs for 20 days. Before the first run and after each run, the fluoride ion concentration in the solution was measured at appointed times (T) T0, T1, T2, and T3. Fluoride ion release was highest at T1 for all products (median values for Protecto CaF2 Nano one-step seal: 0.09 ppm, Bifluorid 12 single dose: 37.67 ppm, and Fluor Protector S: 3.36 ppm) except for the control group, showing its peak at T0 (0.04 ppm). There was a significant difference between the tested fluoride varnishes at all measurement times. Bifluorid 12 achieved significantly higher fluoride release values than the other products (p < 0.05 at all measurement times). A solitary product application of only once or twice per year, as stated by the manufacturers, cannot be supported.

scholarly journals Biophysical and Fluoride Release Properties of a Resin Modified Glass Ionomer Cement Enriched with Bioactive Glasses

Symmetry ◽  
2021 ◽  
Vol 13 (3) ◽  
pp. 494
Author(s):  
Ascensión Vicente ◽  
Francisco Javier Rodríguez-Lozano ◽  
Yolanda Martínez-Beneyto ◽  
María Jaimez ◽  
Julia Guerrero-Gironés ◽  
...  
Keyword(s):  
Cell Migration ◽  
Bond Strength ◽  
Glass Ionomer Cement ◽  
Fluoride Ion ◽  
Fluoride Release ◽  
Glass Ionomer ◽  
Ion Release ◽  
Bioactive Glasses ◽  
Resin Modified Glass Ionomer ◽  
Ionomer Cement

The aim of this study was to evaluate the bond strength, microleakage, cytotoxicity, cell migration and fluoride ion release over time from a resin-modified glass-ionomer cement (RMGIC) enriched with bioactive glasses (BAGs) and a nanohybrid restorative polymer resin agent used as adhesion material in the cemented brackets. One hundred and twenty bovine lower incisors were divided into three groups: (Transbond Plus Self Etching Primer (TSEP)/Transbond XT (TXT), TSEP/ACTIVA, orthophosphoric acid gel/ACTIVA) and brackets were bonded. A bond strength test and microleakage test were applied. A fluoride release test was applied after 60 days for the TXT and ACTIVA group. To evaluate cytotoxicity and cell migration, a cell viability and scratch migration assay were done for each group. p values < 0.05 were considered significant. Regarding bond strength and microleakage test, no significant differences were found between TSEP/TXT and TSEP/ACTIVA. At 6.4 pH, ACTIVA showed a higher degree of fluoride ion release, which increased with acid pH (3.5), with a maximum fluoride secretion at 30 days. MTT assay revealed that TXT reduces the viability of gingival cells with significant differences (p < 0.001) compared to the untreated cells (control group). ACTIVA provides optimal adhesive and microfiltration properties, releases substantial amounts of fluoride ions in both acid and neutral media, and its biocompatibility is greater than that of traditional composite resin adhesive systems.

scholarly journals Evaluation of Cements Curing Modes Regarding Microleakage During Cementation of E-max Laminate Veneers

2021 ◽  
Vol 9 (D) ◽  
pp. 155-159
Author(s):  
Waleed Alqahtani ◽  
Rami Mohammed Galal ◽  
Ghada Hamza
Keyword(s):  
Resin Cement ◽  
The Self ◽  
Qualitative Assessment ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Significant Difference ◽  
Blue Stain ◽  
To Receive ◽  
Laminate Veneers ◽  
Descriptive Statistical Analysis

Purpose: The aim of this study is to investigate the effect of the curing modes of two adhesive resin cements (Light cure mode of the Variolink Veneer, the self-cure mode and dual cure mode of the Multilink Automix) on the marginal leakage of lithium disilicate ceramic laminate veneers. Methods: A total number of forty eight extracted natural central incisors were prepared to receive ceramic laminate veneers, constructed using E-max ceramic divided into three groups cemented using three curing modes of two adhesive resin cements {light-cure mode of Variolink Veneer, self-cure mode of Multilink Automix and dual-cure mode of Multilink Automix adhesive resin cements} . Die penetration test was done using the methylene blue stain {qualitative assessment} for testing the die penetration along the tooth/ceramic interface. Results: Descriptive statistical analysis revealed that the self-curing mode recorded the significantly least degree of leakage compared to the light and dual cure modes.  The self-cure mode recorded (0.1±0.3) which was significantly lower than light cure (1.2 ±0.9) and dual cure mode (1.2 ±0.4), there was no statistical significant difference between the later two curing modes. The self-cure mode of the resin cement is considered a more effective method for having the least marginal leakage at the tooth/ceramic interface. There was no difference between the light cure mode and the dual cure mode.

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