scholarly journals Mass transfer from the wall of a column to the fluid in a fluidized bed of inert spherical particles

2004 ◽  
Vol 58 (2) ◽  
pp. 69-72
Author(s):  
Danica Brzic ◽  
Nevenka Boskovic-Vragolovic ◽  
Zeljko Grbavcic

Mass transfer in fluidized beds is an important operation for separation processes. Two effects can be achieved by using fluidized beds in mass transfer processes increasing interface area and relative movement between the phases. These effects are both desirable because they lead to greater process rates. This paper presents an experimental investigation regarding mass transfer from the wall of a column to the fluid in a fluidized bed of inert spherical particles. The experiments were conducted in column 40 mm in diameter with spherical particles 0,8-3 mm in diameter and water as one fluidizing fluid. The method of dissolution of benzoic acid was used to provide very low mass flux. The average wall-to-fluid mass transfer coefficients were determined for two systems: single-phase fluid flow and a fluidized bed of inert particles The measurements encompassed a Reynolds number range from 100-4000 for single-phase flow and 600-4000 in fluidized beds. The mass transfer coefficients for both systems were calculated from weight loss of benzoic acid. The effects of superficial liquid velocity and particle diameter on the mass transfer coefficient were investigated. It was found that mass transfer was more intensive in the fluidized bed in comparison with single phase flow. The best conditions for mass transfer were reached at a minimum fluidization velocity, when the mass transfer coefficient had the greatest value. The experimental data were correlated in the form: jd = f(Re), where jd is the dimensionless mass transfer factor and Re the Reynolds number.

2014 ◽  
Vol 68 (1) ◽  
pp. 15-25
Author(s):  
Darko Jacimovski ◽  
Radmila Garic-Grulovic ◽  
Zeljko Grbavcic ◽  
Mihal Djuris ◽  
Nevenka Boskovic-Vragolovic

Wall-to-bed momentum, heat and mass transfer in vertical liquid-solids flow, as well as in single phase flow, were studied. The aim of this investigation was to establish the analogy among those phenomena. Also, effect of particles concentration on momentum, heat and mass transfer was studied. The experiments in hydraulic transport were performed in a 25.4 mm I.D. cooper tube equipped with a steam jacket, using spherical glass particles of 1.94 mm in diameter and water as a transport fluid. The segment of the transport tube used for mass transfer measurements was inside coated with benzoic acid. In the hydraulic transport two characteristic flow regimes were observed: turbulent and parallel particle flow regime. The transition between two characteristic regimes (?*=0), occurs at a critical voidage ??0.85. The vertical two-phase flow was considered as the pseudofluid, and modified mixture-wall friction coefficient (fw) and modified mixture Reynolds number (Rem) were introduced for explanation of this system. Experimental data show that the wall-to-bed momentum, heat and mass transfer coefficients, in vertical flow of pseudofluid, for the turbulent regime are significantly higher than in parallel regime. Wall-to-bed, mass and heat transfer coefficients in hydraulic transport of particles were much higher then in single-phase flow for lower Reynolds numbers (Re<15000), while for high Reynolds numbers (Re>15000), there was not significant difference. The experimental data for wall-to-bed momentum, heat and mass transfer in vertical flow of pseudofluid in parallel particle flow regime, show existing analogy among these three phenomena.


2007 ◽  
Vol 72 (11) ◽  
pp. 1103-1113 ◽  
Author(s):  
Nevenka Boskovic-Vragolovic ◽  
Radmila Garic-Grulovic ◽  
Zeljko Grbavcic

Mass transfer coefficients in single phase flow, liquid fluidized beds and vertical hydraulic transport of spherical inert particles were studied experimentally using 40 mm and 25.4 mm diameter columns. The mass transfer data were obtained by studying the transfer of benzoic acid from a tube segment to water using the dissolution method. In all runs, the mass transfer rates were determined in the presence of spherical glass particles 1.2, 1.94 and 2.98 mm in diameter. The influence of different parameters, such as liquid velocity, particles size and voids on mass transfer in fluidized beds and hydraulic transport are presented. The data for mass transfer in all the investigated systems are shown using the Sherwood number (Sh) and mass transfer factor - Colburn factor (jD) - as a function of Reynolds number (Re) for the particles and for the column. The data for mass transfer in particulate fluidized beds and for vertical hydraulic transport of spherical particles were correlated by treating the flowing fluid-particle mixture as a pseudo fluid by introducing a modified mixture Reynolds number (Rem). A new correlation for the mass transfer factor in fluidized beds and in vertical hydraulic transport is proposed.


Author(s):  
Suizheng Qiu ◽  
Minoru Takahashi ◽  
Guanghui Su ◽  
Dounan Jia

Water single-phase and nucleate boiling heat transfer were experimentally investigated in vertical annuli with narrow gaps. The experimental data about water single-phase flow and boiling two-phase flow heat transfer in narrow annular channel were accumulated by two test sections with the narrow gaps of 1.0mm and 1.5mm. Empirical correlations to predict the heat transfer of the single-phase flow and boiling two-phase flow in the narrow annular channel were obtained, which were arranged in the forms of the Dittus-Boelter for heat transfer coefficients in a single-phase flow and the Jens-Lottes formula for a boiling two-phase flow in normal tubes, respectively. The mechanism of the difference between the normal channel and narrow annular channel were also explored. From experimental results, it was found that the turbulent heat transfer coefficients in narrow gaps are nearly the same to the normal channel in the experimental range, and the transition Reynolds number from a laminar flow to a turbulent flow in narrow annuli was much lower than that in normal channel, whereas the boiling heat transfer in narrow annular gap was greatly enhanced compared with the normal channel.


2015 ◽  
Vol 138 (2) ◽  
Author(s):  
Zan Wu ◽  
Bengt Sundén

Experimental single-phase, condensation, and evaporation (flow boiling) pressure drop data from the literature and our previous studies were collected to evaluate previous frictional pressure drop correlations for horizontal microfin tubes of different geometries. The modified Ravigururajan and Bergles correlation, by adopting the Churchill model to calculate the smooth-tube friction factor and by using the hydraulic diameter in the Reynolds number, can predict single-phase turbulent frictional pressure drop data relatively well. Eleven pressure drop correlations were evaluated by the collected database for condensation and evaporation. Correlations originally developed for condensation and evaporation in smooth tubes can be suitable for microfin tubes if the friction factors in the correlations were calculated by the Churchill model to include microfin effects. The three most accurate correlations were recommended for condensation and evaporation in microfin tubes. The Cavallini et al. correlation and the modified Friedel correlation can give good predictions for both condensation and evaporation. However, some inconsistencies were found, even for the recommended correlations.


2019 ◽  
Vol 8 (3) ◽  
pp. 5763-5766

Nanomaterial has unique physical property which made it important for many applications and that is why the use of nanomaterials rapidly increasing in the field of science and engineering.1 . This work focuses on mass transfer of solids into liquid in three phase fluidized beds in presence of nanomaterial. This include the study of effect of gas velocity, time and different concentration of nanomaterials on mass transfer coefficient in stagnant liquid column in three phase fluidized bed system. To measure coefficient of the mass transfer, known quantity of solid pellets ie benzoic acid and known amount of nanomaterial fraction ie Arachitol nano were charged in the test column of three phase fluidized bed system. At the beginning of each run, test section was partially filled with water which prevent breakage of particles. The experiments were conducted by sequentially varying gas velocity for different volumes of nanomaterial and measuring the rate of mass transfer by collecting samples directly from the outlet ports at the top subsequently analysed by volumetric titration method. The results show enhancement in mass transfer coefficient by addition of nanomaterials. Arachitol nano has been taken in different volumes ie 3ml, 7ml, 10ml and 20ml in (GLS) gas ,liquid and solid fluidized bed with air, water and benzoic acid pellets as three phases respectively in the system. The presence of nanomaterial increases the solid liquid mass transfer coefficient value with increasing fraction of nanomaterial, increasing gas velocity and increasing time although experimental run has been taken only for one hour.


Author(s):  
Nan Zhang ◽  
Zhongning Sun ◽  
Ming Ding

A computational fluid dynamic (CFD) model for single phase flow in the three dimensional randomly packed bed with spherical particles has been developed and validated with experimental results. The flow characteristics within this complex geometry are very complicated. In order to obtain insight into the interior and local flow characteristics, Three-dimensional simulation is required. First, we constructed the randomly packed bed with spherical particle, using Discrete Element Method (DEM) based on the integration of Newton’s laws of motion. To validate the DEM simulations the global bed porosity and the radial porosity distribution were compared with empirical correlation from literature. Second, the complex geometrical properties of random packed bed make it difficult to produce a fine mesh. Herein, the bridge method for meshing the particle-particle and particle-wall contact points in the packed bed was applied. The contact zones are modified and then partitioned into several regular parts, so the structure gird was meshed. Finally, the simulation of water flow in the randomly packed bed with a tube-to-particle diameter ratio of 6.325 has been carried out by the commercial CFD code. A comparison with previously published correlations and experimental data shows that the relationship proposed by KTA agree well with the measured pressure drop. Furthermore the results of simulation for distribution of velocity in the bed were analyzed and discussed.


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