Improving Petrophysical Interpretation With Wide-Band Electromagnetic Measurements

SPE Journal ◽  
2008 ◽  
Vol 13 (02) ◽  
pp. 205-215 ◽  
Author(s):  
Emmanuel Toumelin ◽  
Carlos Torres-Verdin ◽  
Nicola Bona

Summary Because of their sensitivity to ionic content and surface texture, wide-band electromagnetic (WBEM) measurements of saturated rocks exhibit frequency dispersions of electrical conductivity and dielectric constant that are influenced by a variety of petrophysical properties. Factors as diverse as fluid saturation, porosity, pore morphology, thin wetting films, and electrically charged clays affect the WBEM response of rocks. Traditional dielectric mixing laws fail to quantitatively and practically integrate these factors to quantify petrophysical information from WBEM measurements. This paper advances a numerical proof of concept for useful petrophysical WBEM measurements. A comprehensive pore-scale numerical framework is introduced that incorporates explicit geometrical distributions of grains, fluids and clays constructed from core pictures, and that reproduces the WBEM saturated-rock response on the entire kHz-GHz frequency range. WBEM measurements are verified to be primarily sensitive (a) in the kHz range to clay amounts and wettability; (b) in the MHz range to pore morphology (i.e., connectivity and eccentricity), fluid distribution, salinity, and clay presence; and (c) in the GHz range to porosity, pore morphology and fluid saturation. Our simulations emphasize the need to measure dielectric dispersion in the entire frequency spectrum to capture the complexity of the different polarization effects. In particular, it is crucial to accurately quantify the phenomena occurring in the MHz range where pore connectivity effects are confounded with clay polarization and pore/grain shape effects usually considered in dielectric phenomena. These different sensitivities suggest a strong complementarity between WBEM and NMR measurements for improved assessments of pore-size distribution, hydraulic permeability, wettability, and fluid saturation. Introduction A number of experimental and theoretical studies suggest the measurable sensitivity of WBEM to various petrophysical factors, including porosity, brine salinity, fluid saturation and wettability, clay content, surface roughness, and even pore surface-to-volume ratio. Given the complexity of the different phenomena under consideration, practical models are designed to fit measured dielectric dispersions to ad-hoc models whose parameters are marginally supported by quantitative petrophysical concepts. Therefore, to assess whether accurate and reliable petrophysical interpretations are possible with WBEM measurements requires an analysis that (a) incorporates pore structure, pore connectivity, multiphase saturation and electrochemical effects; and (b) quantifies the contributions of each factor in the measured WBEM dispersions. However, extracting explicit petrophysical information from WBEM responses is a difficult task. Myers (1991), for instance, illustrated the non-uniqueness of WBEM measurements when a decrease of water saturation, porosity, or brine salinity yielded similar responses. Recent advances in NMR logging and interpretation (Freedman et al. 1990) can eliminate some of these ambiguities with adequate experimental conditions, and if rock wettability is known. Conversely, WBEM measurements could provide independent wettability assessment in the cases where NMR measurements alone reach their limits of sensitivity [for instance, the impact of fluid saturation history on wettability determination was studied by Toumelin et al. (2006)]. Likewise, the interpretation of NMR measurements can be biased by unaccounted rock morphology (Ramakrishnan et al. 1999) or by internal magnetic fields in shaly or iron-rich sands (Zhang et al. 2003), whereas WBEM measurements provide independent information on overall rock morphology. It is therefore timely to consider integrating both technologies for improving petrophysical analysis. The objectives of this paper are twofold:Review existing results on the extraction of petrophysical information from rock WBEM measurements, andestablish a proof of concept for the necessity to integrate electromagnetic measurements on the wide-frequency band from the kHz range to the GHz range, and study how WBEM techniques may yield petrophysical information unavailable from other in-situ measurements. To reach the second objective, we introduce a generalized pore-scale simulation framework that allows incorporating arbitrary rock morphology and multiphase fluid distribution.

Geophysics ◽  
2007 ◽  
Vol 72 (3) ◽  
pp. F97-F110 ◽  
Author(s):  
Emmanuel Toumelin ◽  
Carlos Torres-Verdín

Effective medium theories (EMTs) are invoked routinely to interpret multifrequency dispersions of dielectric permittivity and electrical conductivity of saturated rocks. However, EMTs exhibit limitations that substantially restrict their validity for petrophysical interpretation. For instance, pore connectivity is of significant interest in the study of subsurface reservoirs, but no existing EMT includes it as an explicit property in the analysis of kilohertz- to gigahertz-range dielectric measurements. We introduce a new approach to quantify the effects of pore geometry and connectivity on the kilohertz-gigahertz frequency dispersion of dielectric permittivity and electrical conductivity of clay-free porous rocks. This approach is based on the numerical solution of the internal electric fields within submicron-resolution pore maps constructed with grain and rock pixels. The discrepancy between the internal fields and electrical currents calculated for ahomogeneous scatterer and those calculated for a given pore map is minimized to yield the effective electrical conductivity and dielectric constant for that pore map. This minimization is performed independently for each frequency and is verified to agree implicitly with Kramers-Kronig's causality relationships. We show that EMTs only predict an average dispersion for given microscopic geometrical parameters (e.g., porosity, pore eccentricity), whereas individual realizations honoring the same parameters are associated with dispersion about average values predicted by EMTs. Unlike any EMT prediction, we show that pore connectivity plays a major role in both the shape and amplitude of wide-band electromagnetic property dispersions. The simulation procedure introduced in this paper provides a systematic method to assess the sensitivity of a multitude of pore-scale properties on the macroscopic wide-band dielectric dispersion of saturated rocks.


Geofluids ◽  
2020 ◽  
Vol 2020 ◽  
pp. 1-13
Author(s):  
Boli Wang ◽  
Xisen Zhao ◽  
Wen Zhou ◽  
Bin Chang ◽  
Hao Xu

The pore connectivity and distribution of moveable fluids, which determines fluid movability and recoverable reserves, are critical for enhancing oil/gas recovery in tight sandstone reservoirs. In this paper, multiple techniques including high-pressure mercury intrusion porosimetry (MIP), nuclear magnetic resonance (NMR), scanning electron microscopy (SEM), and microcomputer tomography scanning (micro-CT) were used for the quantitative characterization of pore structure, pore connectivity, and movable fluid distribution. Firstly, sample porosity and permeability were obtained. Pore morphology and the 3D distribution of the pore structures were analyzed using SEM and micro-CT, respectively. The pore-size distribution (PSD) from NMR was generally broader than that from MIP because this technique simply characterized the connected pore volume, whereas NMR showed the total pore volume. Therefore, an attempt was made to calculate pore connectivity percentages of pores with different radii (<50 nm, 50 nm–0.1 μm, and 0.1 μm–1 μm) using the difference between the PSD obtained from MIP and NMR. It was found that small pores (r<0.05 μm) contributed 5.02%–18.00% to connectivity, which is less than large pores (r>0.05 μm) with contribution of 36.60%–92.00%, although small pores had greater pore volumes. In addition, a new parameter, effective movable fluid saturation, was proposed based on the initial movable fluid saturation from NMR and the pore connectivity percentage from MIP and NMR. The results demonstrated that the initial movable fluid saturation decreased by 14.16% on average when disconnected pores were excluded. It was concluded that the effective movable fluid saturation has a higher accuracy in evaluating the recovery of tight sandstone reservoirs.


1965 ◽  
Vol 5 (01) ◽  
pp. 15-24 ◽  
Author(s):  
Norman R. Morrow ◽  
Colin C. Harris

Abstract The experimental points which describe capillary pressure curves are determined at apparent equilibria which are observed after hydrodynamic flow has ceased. For most systems, the time required to obtain equalization of pressure throughout the discontinuous part of a phase is prohibitive. To permit experimental points to be described as equilibria, a model of capillary behavior is proposed where mass transfer is restricted to bulk fluid flow. Model capillary pressure curves follow if the path described by such points is independent of the rate at which the saturation was changed to attain a capillary pressure point. A modified suction potential technique is used to study cyclic relationships between capillary pressure and moisture content for a porous mass. The time taken to complete an experiment was greatly reduced by using small samples. Introduction Capillary retention of liquid by porous materials has been investigated in the fields of hydrology, soil science, oil reservoir engineering, chemical engineering, soil mechanics, textiles, paper making and building materials. In studies of the immiscible displacement of one fluid by another within a porous bed, drainage columns and suction potential techniques have been used to obtain relationships between pressure deficiency and saturation (Fig. 1). Except where there is no hysteresis of contact angle and the solid is of simple geometry, such as a tube of uniform cross section, there is hysteresis in the relationship between capillary pressure and saturation. The relationship which has received most attention is displacement of fluid from an initially saturated bed (Fig. 1, Curve Ro), the final condition being an irreducible minimum fluid saturation Swr. Imbibition (Fig. 1, Curve A), further desaturation (Fig. 1, Curve R), and intermediate scanning curves have been studied to a lesser but increasing extent. This paper first considers the nature of the experimental points tracing the capillary pressure curves with respect to the modes and rates of mass transfer which are operative during the course of measurement. There are clear indications that the experimental points which describe these curves are obtained at apparent equilibria which are observed when viscous fluid flow has ceased; and any further changes in the fluid distribution are the result of much slower mass transfer processes, such as diffusion. Unless stated otherwise, this discussion applies to a stable packing of equal, smooth, hydrophilic spheres supported by a suction plate with water as the wetting phase and air as the nonwetting phase. SPEJ P. 15ˆ


Author(s):  
Willem Vos ◽  
Petter Norli ◽  
Emilie Vallee

This paper describes a novel technique for the detection of cracks in pipelines. The proposed in-line inspection technique has the ability to detect crack features at random angles in the pipeline, such as axial, circumferential, and any angle in between. This ability is novel to the current ILI technology offering and will also add value by detecting cracks in deformed pipes (i.e. in dents), and cracks associated with the girth weld (mid weld cracks, rapid cooling cracks and cracks parallel to the weld). Furthermore, the technology is suitable for detection of cracks in spiral welded pipes, both parallel to the spiral weld as well as perpendicular to the weld. Integrity issues around most features described above are not addressed with ILI tools, often forcing operators to perform hydrostatic tests to ensure pipeline safety. The technology described here is based on the use of wideband ultrasound inline inspection tools that are already in operation. They are designed for the inspection of structures operating in challenging environments such as offshore pipelines. Adjustments to the front-end analog system and data collection from a grid of transducers allow the tools to detect cracks in any orientation in the line. Description of changes to the test set-up are presented as well as the theoretical background behind crack detection. Historical development of the technology will be presented, such as early laboratory testing and proof of concept. The proof of concept data will be compared to the theoretical predictions. A detailed set of results are presented. These are from tests that were performed on samples sourced from North America and Europe which contain SCC features. Results from ongoing testing will be presented, which involved large-scale testing on SCC features in gas-filled pipe spools.


2016 ◽  
Author(s):  
Katherine J. Dobson ◽  
Sophia B. Coban ◽  
Sam A. McDonald ◽  
Joanna Walsh ◽  
Robert Atwood ◽  
...  

Abstract. A variable volume flow cell has been integrated with state-of-the-art ultra-high speed synchrotron x-ray tomography imaging. The combination allows the first real time (sub-second) capture of dynamic pore (micron) scale fluid transport processes in 4D (3D + time). With 3D data volumes acquired at up to 20 Hz, we perform in situ experiments that capture high frequency pore-scale dynamics in 5–25 mm diameter samples with voxel (3D equivalent of a pixel) resolution of 2.5 to 3.8 µm. The data are free from motion artefacts, can be spatially registered or collected in the same orientation making them suitable for detailed quantitative analysis of the dynamic fluid distribution pathways and processes. The method presented here are capable of capturing a wide range of high frequency non equilibrium pore-scale processed including wetting, dilution, mixing and reaction phenomena, without sacrificing significant spatial resolution. As well as fast streaming (continuous acquisition) at 20 Hz, it also allows larger-scale and longer term experimental runs to be sampled intermittently at lower frequency (time-lapse imaging); benefiting from fast image acquisition rates to prevent motion blur in highly dynamic systems. This marks a major technical breakthrough for quantification of high frequency pore scale processes: processes that are critical for developing and validating more accurate multiscale flow models through spatially and temporally heterogeneous pore networks.


2010 ◽  
Vol 86 (2) ◽  
pp. 495-515 ◽  
Author(s):  
Dmitriy Silin ◽  
Liviu Tomutsa ◽  
Sally M. Benson ◽  
Tad W. Patzek

SPE Journal ◽  
2016 ◽  
Vol 21 (04) ◽  
pp. 1436-1449 ◽  
Author(s):  
Lu Chi ◽  
Zoya Heidari

Summary This paper proposes a new method for directional-permeability assessment with nuclear-magnetic-resonance (NMR) measurements. Conventional techniques for permeability assessment from NMR measurements include empirical correlations such as SDR (Schlumberger-Doll-Research) and Coates models. However, carbonate rocks are known for lack of good correlations between pore-body-size and pore-throat-size, which makes it challenging and often unreliable to estimate permeability from NMR T2 (spin-spin relaxation time) distribution in carbonate formations with complex pore structure. It also was proposed that conventional permeability models can be improved by incorporating an estimated pore-connectivity factor. However, none of the previously introduced techniques reflects the anisotropic characteristics of rock permeability. The new NMR-based directional-permeability model, introduced in this paper, incorporates a directional pore-connectivity factor into a conventional NMR-based permeability model. We introduce two approaches to quantify the directional pore-network connectivity of rock samples with pore-scale images. The first approach calculates directional pore connectivity in 3D pore-scale images with a topological technique. The second approach combines image analysis and electrical formation factor. The new NMR-based permeability model enables assessment of rock permeability in any desired direction. We successfully calibrated and tested the introduced NMR-based permeability model on carbonate, sandstone, and sandpack samples with complex pore geometry or anisotropic permeability. The anisotropic permeability used for calibration and test purposes was obtained by the lattice Boltzmann method (LBM) simulations on microcomputed tomography (CT) images of rock samples. The comparison between the permeability estimates with our new NMR model and conventional NMR models (e.g., SDR and Coates models) demonstrated that the NMR-based directional-permeability model significantly improves assessment of rock permeability, by reflecting rock's anisotropic characteristics and minimizing calibration efforts. The outcomes of this research can significantly improve permeability assessment in complex carbonate reservoirs and anisotropic sandstone reservoirs, and can be extended further to organic-rich mudrock formations.


Geophysics ◽  
1998 ◽  
Vol 63 (1) ◽  
pp. 154-160 ◽  
Author(s):  
Thierry Cadoret ◽  
Gary Mavko ◽  
Bernard Zinszner

Extensional and torsional wave‐attenuation measurements are obtained at a sonic frequency around 1 kHz on partially saturated limestones using large resonant bars, 1 m long. To study the influence of the fluid distribution, we use two different saturation methods: drying and depressurization. When water saturation (Sw) is higher than 70%, the extensional wave attenuation is found to depend on whether the resonant bar is jacketed. This can be interpreted as the Biot‐Gardner‐White effect. The experimental results obtained on jacketed samples show that, during a drying experiment, extensional wave attenuation is influenced strongly by the fluid content when Sw is between approximately 60% and 100%. This sensitivity to fluid saturation vanishes when saturation is obtained through depressurization. Using a computer‐assisted tomographic (CT) scan, we found that, during depressurization, the fluid distribution is homogeneous at the millimetric scale at all saturations. In contrast, during drying, heterogeneous saturation was observed at high water‐saturation levels. Thus, we interpret the dependence of the extensional wave attenuation upon the saturation method as principally caused by a fluid distribution effect. Torsional attenuation shows no sensitivity to fluid saturation for Sw between 5% and 100%.


SPE Journal ◽  
2017 ◽  
Vol 22 (05) ◽  
pp. 1362-1373 ◽  
Author(s):  
W.-B.. -B. Bartels ◽  
H.. Mahani ◽  
S.. Berg ◽  
R.. Menezes ◽  
J. A. van der Hoeven ◽  
...  

Summary Low-salinity waterflooding (LSF) is receiving increased interest as a promising method to improve oil-recovery efficiency. Most of the literature agrees that, on the Darcy scale, LSF can be regarded as a wettability-modification process, leading to a more-water-wet state, although no consensus on the microscopic mechanisms has been reached. To establish a link between the pore-scale and the Darcy-scale description, the flow dynamic at an intermediate scale—i.e., networks of multiple pores—should be investigated. One of the main challenges in addressing phenomena on this scale is to design a model system representative of natural rock. The model system should allow for a systematic investigation of influencing parameters with pore-scale resolution while simultaneously being large enough to capture larger-length-scale effects such as saturation changes and the mobilization and connection of oil ganglia. In this paper, we use micromodels functionalized with active clay minerals as a model system to study the low-salinity effect (LSE) on the pore scale. A new method was devised to deposit clays in the micromodel. Clay suspensions were made by mixing natural clays (montmorillonite) with isopropyl alcohol (IPA) and were injected into optically transparent 2D glass micromodels. After drying the models, the clay particles were deposited and stick naturally to the glass surfaces. The micromodel was then used to investigate the dependence of the LSE on the type of oil (crude oil vs. n-decane), the presence of clay particles, and aging. Our results show that the system is responsive to low-salinity brine as the effective contact angle of crude oil shifts toward a more-water-wetting state when brine salinity is reduced. When using n-decane as a reference case of inert oil, no change in contact angle occurred after a reduction in brine salinity. This responsiveness in terms of contact angle does not necessarily mean that more oil is recovered. Only in the cases where the contact-angle change (because of low-salinity exposure) led to release of oil and reconnection with oil of adjacent pore bodies did the oil become mobile and the oil saturation effectively reduce. This makes contact-angle changes a necessary but not sufficient requirement for incremental recovery by LSF. Interestingly, the wettability modification was observed in the absence of clay. Osmosis and interfacial tension (IFT) change were found not to be the primary driving mechanisms of the low-salinity response.


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