scholarly journals 4D imaging of sub-second dynamics in pore-scale processes using real time synchrotron x-ray tomography

Author(s):  
Katherine J. Dobson ◽  
Sophia B. Coban ◽  
Sam A. McDonald ◽  
Joanna Walsh ◽  
Robert Atwood ◽  
...  

Abstract. A variable volume flow cell has been integrated with state-of-the-art ultra-high speed synchrotron x-ray tomography imaging. The combination allows the first real time (sub-second) capture of dynamic pore (micron) scale fluid transport processes in 4D (3D + time). With 3D data volumes acquired at up to 20 Hz, we perform in situ experiments that capture high frequency pore-scale dynamics in 5–25 mm diameter samples with voxel (3D equivalent of a pixel) resolution of 2.5 to 3.8 µm. The data are free from motion artefacts, can be spatially registered or collected in the same orientation making them suitable for detailed quantitative analysis of the dynamic fluid distribution pathways and processes. The method presented here are capable of capturing a wide range of high frequency non equilibrium pore-scale processed including wetting, dilution, mixing and reaction phenomena, without sacrificing significant spatial resolution. As well as fast streaming (continuous acquisition) at 20 Hz, it also allows larger-scale and longer term experimental runs to be sampled intermittently at lower frequency (time-lapse imaging); benefiting from fast image acquisition rates to prevent motion blur in highly dynamic systems. This marks a major technical breakthrough for quantification of high frequency pore scale processes: processes that are critical for developing and validating more accurate multiscale flow models through spatially and temporally heterogeneous pore networks.

Solid Earth ◽  
2016 ◽  
Vol 7 (4) ◽  
pp. 1059-1073 ◽  
Author(s):  
Katherine J. Dobson ◽  
Sophia B. Coban ◽  
Samuel A. McDonald ◽  
Joanna N. Walsh ◽  
Robert C. Atwood ◽  
...  

Abstract. A variable volume flow cell has been integrated with state-of-the-art ultra-high-speed synchrotron X-ray tomography imaging. The combination allows the first real-time (sub-second) capture of dynamic pore (micron)-scale fluid transport processes in 4-D (3-D + time). With 3-D data volumes acquired at up to 20 Hz, we perform in situ experiments that capture high-frequency pore-scale dynamics in 5–25 mm diameter samples with voxel (3-D equivalent of a pixel) resolutions of 2.5 to 3.8 µm. The data are free from motion artefacts and can be spatially registered or collected in the same orientation, making them suitable for detailed quantitative analysis of the dynamic fluid distribution pathways and processes. The methods presented here are capable of capturing a wide range of high-frequency nonequilibrium pore-scale processes including wetting, dilution, mixing, and reaction phenomena, without sacrificing significant spatial resolution. As well as fast streaming (continuous acquisition) at 20 Hz, they also allow larger-scale and longer-term experimental runs to be sampled intermittently at lower frequency (time-lapse imaging), benefiting from fast image acquisition rates to prevent motion blur in highly dynamic systems. This marks a major technical breakthrough for quantification of high-frequency pore-scale processes: processes that are critical for developing and validating more accurate multiscale flow models through spatially and temporally heterogeneous pore networks.


2018 ◽  
Vol 25 (4) ◽  
pp. 1135-1143 ◽  
Author(s):  
Faisal Khan ◽  
Suresh Narayanan ◽  
Roger Sersted ◽  
Nicholas Schwarz ◽  
Alec Sandy

Multi-speckle X-ray photon correlation spectroscopy (XPCS) is a powerful technique for characterizing the dynamic nature of complex materials over a range of time scales. XPCS has been successfully applied to study a wide range of systems. Recent developments in higher-frame-rate detectors, while aiding in the study of faster dynamical processes, creates large amounts of data that require parallel computational techniques to process in near real-time. Here, an implementation of the multi-tau and two-time autocorrelation algorithms using the Hadoop MapReduce framework for distributed computing is presented. The system scales well with regard to the increase in the data size, and has been serving the users of beamline 8-ID-I at the Advanced Photon Source for near real-time autocorrelations for the past five years.


2019 ◽  
Vol 81 (1) ◽  
pp. 118-128
Author(s):  
V. V. Balandin ◽  
V. V. Balandin ◽  
V. V. Parkhachev

Investigating impact interaction of solid and deformed bodies with obstacles of various physical natures requires developing experimental methodologies of registering the parameters of the interaction process. In experimental investigations of impact interaction of solids, it is common practice to measure displacement of strikers as a function of time, as well as their velocity and deceleration. To determine the displacement and velocity of a striker, a radio-interferometric methodology of registering the displacement of its rear end is proposed. In contrast with the registration methods based on high-speed filming and pulsed X-ray photography, the method using a millimeter-range radio-interferometer provides continuous high-accuracy registering of the displacement of the rear end of a striker in a wide range of displacement values. To test the effectiveness of the methodology, a series of experiments have been conducted on registering the motion of a cylindrical striker of an aluminum alloy, fired from a 20mm-dia gas gun. The displacement of the striker was also monitored using high-speed filming. The results of measuring using the two methodologies differ within the limits of the error of measurement. Based on the results of the above experiments, it has been concluded that the methodology of determining the displacement and velocity of strikers in a ballistic experiment using a mm-range radio-interferometer makes it possible to measure practically continuously large displacements (100 mm and larger) to a safe accuracy. The present methodology can be used for measuring the displacement and velocity of the rear end of a striker interacting with obstacles of various physical natures (metals, ceramics, soils, concretes, etc.).


2021 ◽  
Author(s):  
Mingming Ge ◽  
Guangjian Zhang ◽  
Navid Nematikourabbasloo ◽  
Kamel Fezzaa ◽  
Olivier Coutier-Delgosha

Hydrodynamic cavitation is a complex two-phase flow phenomenon involving mass and heat transfer between liquid and vapor. It occurs in many widely-used hydraulic machines, such as pumps and marine propellers, and often leads to undesired effects like material erosion, noise, and vibration. To control these detrimental effects, the visualization of two-phase flow morphology inside the opaque cavity is a crucial point to improve the physical and numerical models of cavitation. The major challenge in experimental measurements of cavitating flow fields is the fact that multiple scattering and a direct reflection of visible light from phase boundaries make the flow optically opaque. In recent years, unlike traditional local measurements using various probes, the development of the third-generation synchrotron radiation sources promotes the application of Xray phase-contrast imaging, which enables clear visualization of boundaries between phases with different refractive indices. In this study, the partial cavity is formed in a convergent-divergent (Venturi) channel with a small contraction ratio where the relatively stable cavitation regime can be sustained in a wide range of cavitation numbers. The experiment performed at Advanced Photon Source (APS) of Argonne uses the short high-flux X-ray pulses emitted from synchrotron sources to capture fast dynamic events and minimize motion blur. The internal two-phase structures and bubble development dynamics inside the quasi-stable sheet cavitation can be identified. Aside from the detailed illustration of two-phase morphology, X-ray phase-contrast images were also used to perform velocimetry by tracking either seeded particles or phase interfaces inside the opaque regions. Through appropriate postprocessing to the recorded X-ray images of cavitation, the time resolved velocity and void fraction fields are obtained simultaneously. These unprecedented experimental data will be further explored in understanding fluid mechanics underneath the cavity, estimating slip velocity between fluid-vapor interactions, and reconstructing pressure fields for compressible flows.


Soil Research ◽  
2019 ◽  
Vol 57 (6) ◽  
pp. 575
Author(s):  
Erika Shiota ◽  
Toshifumi Mukunoki ◽  
Laurent Oxarango ◽  
Anne-Julie Tinet ◽  
Fabrice Golfier

Water retention in granular soils is a key mechanism for understanding transport processes in the vadose zone for various applications from agronomy to hydrological and environmental sciences. The macroscopic pattern of water entrapment is mainly driven by the pore-scale morphology and capillary and gravity forces. In the present study, the drainage water retention curve (WRC) was measured for three different granular materials using a miniaturised hanging column apparatus. The samples were scanned using X-ray micro-computed tomography during the experiment. A segmentation procedure was applied to identify air, water and solid phases in 3D at the pore-scale. A representative elementary volume analysis based on volume and surface properties validated the experimental setup size. A morphological approach, the voxel percolation method (VPM) was used to model the drainage experiment under the assumption of capillary-dominated quasi-static flow. At the macro-scale, the VPM showed a good capability to predict the WRC when compared with direct experimental measurements. An in-depth comparison with image data also revealed a satisfactory agreement concerning both the average volumetric distributions and the pore-scale local topology. Image voxelisation and the quasi-static assumption of VPM are likely to explain minor discrepancies observed at low suctions and for coarser materials.


Author(s):  
Chen Yuan ◽  
Jun Wu

Abstract A real-time hard X-ray (HXR) tomographic system is designed for HL-2A tokamak, which is dedicated to the real-time tomography of fast electron bremsstrahlung radiation during the lower hybrid (LH) driven mode within the energy range of 20keV to 200keV. This system has realized the investigation of HXR energy from 12 different chords on the equatorial plane of the reaction region. The spatial and temporal resolutions of the system are 2cm and 10ms, separately. HXR detection is accomplished by a self-designed detector array, with a structure of 12 arc arranged cadmium telluride (CdTe) semiconductors and their corresponding collimators. The real-time HXR acquisition and processing is achieved by the main electronic system, which is comprised of a high speed analog-to-digital module and a high performance signal processing unit. Due to high HXR flux and the real-time demand in measurement, the HXR tomography is accomplished by several customized digital processing algorithms based on FPGA logic resources, such as the digital real-time spectrum measurement, the trapezoidal shaper, the pile up filter, and the baseline restorer, etc. This system has been proved to be qualified as a dependable platform of fast electron bremsstrahlung radiation research during LH mode on HL-2A, which provides indispensable parameters for plasma state during fusion reaction.


2020 ◽  
Vol 117 (38) ◽  
pp. 23443-23449 ◽  
Author(s):  
Sharul Hasan ◽  
Vahid Niasar ◽  
Nikolaos K. Karadimitriou ◽  
Jose R. A. Godinho ◽  
Nghia T. Vo ◽  
...  

Solute transport in unsaturated porous materials is a complex process, which exhibits some distinct features differentiating it from transport under saturated conditions. These features emerge mostly due to the different transport time scales at different regions of the flow network, which can be classified into flowing and stagnant regions, predominantly controlled by advection and diffusion, respectively. Under unsaturated conditions, the solute breakthrough curves show early arrivals and very long tails, and this type of transport is usually referred to as non-Fickian. This study directly characterizes transport through an unsaturated porous medium in three spatial dimensions at the resolution of 3.25 μm and the time resolution of 6 s. Using advanced high-speed, high-spatial resolution, synchrotron-based X-ray computed microtomography (sCT) we obtained detailed information on solute transport through a glass bead packing at different saturations. A large experimental dataset (>50 TB) was produced, while imaging the evolution of the solute concentration with time at any given point within the field of view. We show that the fluids’ topology has a critical signature on the non-Fickian transport, which yet needs to be included in the Darcy-scale solute transport models. The three-dimensional (3D) results show that the fully mixing assumption at the pore scale is not valid, and even after injection of several pore volumes the concentration field at the pore scale is not uniform. Additionally, results demonstrate that dispersivity is changing with saturation, being twofold larger at the saturation of 0.52 compared to that at the fully saturated domain.


2000 ◽  
Author(s):  
Toshikazu Sakano ◽  
Takahiro Yamaguchi ◽  
Tatsuya Fujii ◽  
Akira Okumura ◽  
Isao Furukawa ◽  
...  

2016 ◽  
Author(s):  
Katherine J. Dobson ◽  
Sophia B. Coban ◽  
Sam A. McDonald ◽  
Joanna Walsh ◽  
Robert Atwood ◽  
...  

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