Using Optical Fluid Analysis To Evaluate Downhole Fluid Sample Contamination

1998 ◽  
Author(s):  
C.W. Morris ◽  
M.M. Felling ◽  
R.J. Butsch ◽  
W. Sass
2001 ◽  
Author(s):  
J. Bouton ◽  
M.G. Prammer ◽  
P. Masak ◽  
S. Menger

2008 ◽  
Vol 11 (06) ◽  
pp. 1107-1116 ◽  
Author(s):  
Chengli Dong ◽  
Michael D. O'Keefe ◽  
Hani Elshahawi ◽  
Mohamed Hashem ◽  
Stephen M. Williams ◽  
...  

Summary Downhole fluid analysis (DFA) has emerged as a key technique for characterizing the distribution of reservoir-fluid properties and determining zonal connectivity across the reservoir. Information from profiling the reservoir fluids enables sealing barriers to be proved and compositional grading to be quantified; this information cannot be obtained from conventional wireline logs. The DFA technique has been based largely on optical spectroscopy, which can provide estimates of filtrate contamination, gas/oil ratio (GOR), pH of formation water, and a hydrocarbon composition in four groups: methane (C1), ethane to pentane (C2-5), hexane and heavier hydrocarbons (C6+), and carbon dioxide (CO2). For single-phase assurance, it is possible to detect gas liberation (bubblepoint) or liquid dropout (dewpoint) while pumping reservoir fluid to the wellbore, before filling a sample bottle. In this paper, a new DFA tool is introduced that substantially increases the accuracy of these measurements. The tool uses a grating spectrometer in combination with a filter-array spectrometer. The range of compositional information is extended from four groups to five groups: C1, ethane (C2), propane to pentane (C3-5), C6+, and CO2. These spectrometers, together with improved compositional algorithms, now make possible a quantitative analysis of reservoir fluid with greater accuracy and repeatability. This accuracy enables comparison of fluid properties between wells for the first time, thus extending the application of fluid profiling from a single-well to a multiwall basis. Field-based fluid characterization is now possible. In addition, a new measurement is introduced--in-situ density of reservoir fluid. Measuring this property downhole at reservoir conditions of pressure and temperature provides important advantages over surface measurements. The density sensor is combined in a package that includes the optical spectrometers and measurements of fluid resistivity, pressure, temperature, and fluorescence that all play a vital role in determining the exact nature of the reservoir fluid. Extensive tests at a pressure/volume/temperature (PVT) laboratory are presented to illustrate sensor response in a large number of live-fluid samples. These tests of known fluid compositions were conducted under pressurized and heated conditions to simulate reservoir conditions. In addition, several field examples are presented to illustrate applicability in different environments. Introduction Reservoir-fluid samples collected at the early stage of exploration and development provide vital information for reservoir evaluation and management. Reservoir-fluid properties, such as hydrocarbon composition, GOR, CO2 content, pH, density, viscosity, and PVT behavior are key inputs for surface-facility design and optimization of production strategies. Formation-tester tools have proved to be an effective way to obtain reservoir-fluid samples for PVT analysis. Conventional reservoir-fluid analysis is conducted in a PVT laboratory, and it usually takes a long time (months) before the results become available. Also, miscible contamination of a fluid sample by drilling-mud filtrate reduces the utility of the sample for subsequent fluid analyses. However, the amount of filtrate contamination can be reduced substantially by use of focused-sampling cleanup introduced recently in the next-generation wireline formation testers (O'Keefe et al. 2008). DFA tools provide results in real time and at reservoir conditions. Current DFA techniques use absorption spectroscopy of reservoir fluids in the visible-to-near-infrared (NIR) range. The formation-fluid spectra are obtained in real time, and fluid composition is derived from the spectra on the basis of C1, C2-5, C6+, and CO2; then, GOR of the fluid is estimated from the derived composition (Betancourt et al. 2004; Fujisawa et al. 2002; Dong et al. 2006; Elshahawi et al. 2004; Fujisawa et al. 2008; Mullins et al. 2001; Smits et al. 1995). Additionally, from the differences in absorption spectrum between reservoir fluid and filtrate of oil-based mud (OBM) or water-based mud (WBM), fluid-sample contamination from the drilling fluid is estimated (Mullins et al. 2000; Fadnes et al. 2001). With the DFA technique, reservoir-fluid samples are analyzed before they are taken, and the quality of fluid samples is improved substantially. The sampling process is optimized in terms of where and when to sample and how many samples to take. Reservoir-fluid characterization from fluid-profiling methods often reveals fluid compositional grading in different zones, and it also helps to identify reservoir compartmentalization (Venkataramanan et al. 2008). A next-generation tool has been developed to improve the DFA technique. This DFA tool includes new hardware that provides more-accurate and -detailed spectra, compared to the current DFA tools, and includes new methods of deriving fluid composition and GOR from optical spectroscopy. Furthermore, the new DFA tool includes a vibrating sensor for direct measurement of fluid density and, in certain environments, viscosity. The new DFA tool provides reservoir-fluid characterization that is significantly more accurate and comprehensive compared to the current DFA technology.


2019 ◽  
Vol 7 (SI-TeMIC18) ◽  
Author(s):  
Norhanifah Abdul Rahman ◽  
Matzaini Katon Katon ◽  
Nurina Alya Zulkifli Zulkifli

Automatic Transmission (AT) system is efficient in the aspects of vehicle safety, comfort, reliability and driving performance. The objectives of this paper are to collect the oil samples from AT systems of engine bus according to manufacturer's recommendations and analyse collected oil samples using oil analysis technique. The sample transmission fluid which was taken from the AT gearbox has been experimentally analyzed. The oil samples were taken with an interval of 5,000km, 30,000km, 50,000km, 80,000km, 180,000km and 300,000km for AT bus operation. These samples then have been analyzed by comparing between new and used transmission fluid using Fourier Transform Infrared (FTIR) spectroscopy. Oil analysis by FTIR is a form of Predictive Maintenance (PdM) to avoid major failure in machine elements. Most machine elements are not easily accessible in the transmission system. Having a reliable technique would avoid the needs to open the components unnecessarily, hence, help to prevent catastrophic failure which are very costly, and ease of regular monitoring. In order to identify the major failures of automatic gearbox, forecasts can be made regarding the lube transmission fluid analysis test. By using this test, the minor problems can be determined before they become major failures. At the end of this research, the wear particles profile for interval mileage of AT system was obtained. Keywords: Wear, Automatic Transmission (AT), Transmission fluid, Fourier Transform Infrared (FTIR), Oil analysis.


2018 ◽  
Vol 09 (01) ◽  
pp. 026-031 ◽  
Author(s):  
Manoj Munirathinam ◽  
Pugazhendhi Thangavelu ◽  
Ratnakar Kini

ABSTRACTPancreatico‑pleural fistula is a rare but serious complication of acute and chronic pancreatitis. The pleural effusion caused by pancreatico‑pleural fistula is usually massive and recurrent. It is predominately left‑sided but right‑sided and bilateral effusion does occur. We report four cases of pancreatico‑pleural fistula admitted to our hospital. Their clinical presentation and management aspects are discussed. Two patients were managed by pancreatic endotherapy and two patients were managed conservatively. All four patients improved symptomatically and were discharged and are on regular follow‑up. Most of these patients would be evaluated for their breathlessness and pleural effusion delaying the diagnosis of pancreatic pathology and management. Hence, earlier recognition and prompt treatment would help the patients to recover from their illnesses. Pancreatic pleural fistula diagnosis requires a high index of suspicion in patients presenting with chest symptoms or pleural effusion. Extremely high pleural fluid amylase levels are usual but not universally present. A chest X‑ray, pleural fluid analysis, and abdominal imaging (magnetic resonance cholangiopancreatography/magnetic resonance imaging abdomen more useful than contrast‑enhanced computed tomography abdomen) would clinch the diagnosis. Endoscopic retrograde cholangiopancreatography with stent or sphincterotomy should be considered when pancreatic duct (PD) reveals a stricture or when medical management fails in patients with dilated or irregular PD. Surgical intervention may be indicated in patients with complete disruption of PD or multiple strictures.


Pancreatology ◽  
2008 ◽  
Vol 8 (3) ◽  
pp. 277-284 ◽  
Author(s):  
Martha Bishop Pitman ◽  
Paul J. Michaels ◽  
Vikram Deshpande ◽  
William R. Brugge ◽  
Brenna C. Bounds

2020 ◽  
Vol 79 (Suppl 1) ◽  
pp. 440.1-441
Author(s):  
M. L. Peral ◽  
I. Calabuig ◽  
A. Martín-Carratalá ◽  
M. Andrés ◽  
E. Pascual

Background:Synovial fluid analysis using polarized microscopy is the gold standard for the diagnosis of crystal-related arthritis. In our experience, we have noted that, when calcium pyrophosphate (CPP) crystals are observed, they sometimes appear within intracellular vacuoles. However, this phenomenon is not seen in those samples containing monosodium urate (MSU) crystals. This finding has been scantly reported in the literature, but may be useful in clinical practice to ensure accurate crystal identification.Objectives:Our study aims to assess whether the presence of vacuoles contributes to identifying the type of crystal, and also to gauge the frequency of their presentation.Methods:We conducted an observational study in a rheumatology unit between February and June of 2019. Synovial fluids containing CPP or MSU crystals, obtained in daily clinical practice, were consecutively included for analysis. Two observers simultaneously analyzed the presence of vacuoles by ordinary light and phase contrast microscopy in less than 24 hours after their extraction, using a microscope equipped with two viewing stations. The primary study variable was to determine whether CPP and MSU crystals are seen inside intracellular vacuoles, and to calculate the frequency of this finding for each type of crystal, estimating their 95% confidence interval (95% CI) and comparing rates using Fisher’s exact test.Results:Twenty-one samples were obtained. Data is given in the Table. MSU crystals were present in 7 (33.3%) and CPP crystals in 14 (66.6%). Interestingly, none of the MSU samples showed crystal-containing vacuoles (95% CI 0-35.4%). On the contrary, cytoplasmic vacuoles containing crystals were present in all of the CPP samples (95% CI 78.5-100%). The findings were confirmed by phase-contrast microscopy. Differences were statistically significant (p<0.001).Table.SAMPLES ACCORDING TO TYPE OF MICROCRYSTAL(n=21)SAMPLES WITH VACUOLS(UNDER ORDINARY LIGHT)SAMPLES WITH VACUOLS(UNDER PHASE CONTRAST)CPP (14; 66.6%)14 (100%)(95%CI 78.5-100%)14 (100%)(95%CI 78.5-100%)MSU (7; 33.3%)0 (0%)(95%CI 0-35.4%)0 (0%)(95%CI 0-35.4%)Conclusion:The presence of vacuoles may be a useful and easy way to differentiate MSU and CPP crystals when performing synovial fluid microscopy in clinical practice, since it appears to be a distinctive feature in CPP crystal fluids.References:[1]Kohn NN, Hughes RE, McCarty DJ Jr, Faires JS. The significance of calcium phosphate crystals in the synovial fluid of arthritic patients: the «pseudogout syndrome». II. Identification of crystals. Ann InternMed. 1962 May;56:738-45.[2]Pascual E, Sivera F, Andrés M. Synovial Fluid Analysis for Crystals. CurrOpRheumatol 2011;23:161-169.[3]McCarty DJ, Koopman WJ. Arthritis and allied conditions: A textbook of rheumatology, volumen 1. Lea &amp;Febiger. 1993.[4]Pascual E, Sivera F. Synovial fluid crystal Analysis. En Gout and other crystal arthropathies. Terkeltaub R ed. Elsevier; 2012: p.20-34.[5]Hwang HS, Yang CM, Park SJ, Kim HA. Monosodium Urate Crystal-Induced Chondrocyte Death via Autophagic Process. Int J Mol Sci. 2015 Dec 8;16(12):29265-77.Image 1. Microscopy with ordinary light. Cells with cytoplasmic vacuoles are observed, as well as abundant intra and extracellular CPP crystals.Image 2. Microscopy with phase contrast technique. Cells with intracellular vacuoles are observed inside which have microcrystals with parallelepiped morphology, compatible with CPP.Disclosure of Interests: :None declared


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