A New Technique to Determine the Equivalent Viscosity of Drilling Fluids Under High Temperatures and Pressures

1970 ◽  
Vol 10 (01) ◽  
pp. 33-40 ◽  
Author(s):  
B.K. Sinha

Abstract Knowledge concerning the behavior of drilling fluids under wellbore conditions is very desirable, and experimental results have shown that the extent to which the flow properties of drilling fluids are affected by high temperatures and pressures cannot be predicted by standard API pressures cannot be predicted by standard API tests. A Fann consistometer (Model 5S-TDL) is modified to obtain the experimental data reported in this study. Data obtained from the Fann viscometer Model 50 at elevated temperatures have been included to supplement the information derived from the modified Fann consistometer. Newtonian fluids of known viscosities are used in calibrating the modified consistometer. The technique followed here keeps the sample temperature constant and allows the pressure to vary at each desired temperature level. The equivalent viscosities of both laboratory-prepared and field muds of different densities have been obtained at temperatures up to 500 deg F and pressures up to 20,000 psi. The objective of this study is to show that the modified consistometer can give much more information concerning the flow behavior of muds under wellbore conditions than that derived in the past. It can show the pressure and temperature conditions under which the tendency to thicken begins, the gradual thickening, and also the conditions at which the mud completely gels and loses its fluidity. The study shows that both temperature and pressure affect the equivalent viscosity of invert pressure affect the equivalent viscosity of invert emulsion muds. The effect of pressure is very pronounced at low temperatures. Compared to the pronounced at low temperatures. Compared to the invert emulsion muds, the equivalent viscosity of water base muds is not affected to the same extent by temperature and pressure. Temperature is the dominating variable tin case of water base muds. However, the effect of pressure on the equivalent viscosity of water base muds seems to depend on composition and temperature of the system. Introduction Kennedy and Crawford designed and patented the consistometer to test the setting time of cement slurries. This consistometer as manufactured and later improved by Fann. Chisholm et al. adapted the first Fann consistometer for evaluating drilling fluids under wellbore conditions in 1961; their study was later continued by Cox and Pfleger. Weintritt and Hughes used a similar consistometer with a different recording device. They measured the relative viscosity of drilling fluids in seconds and pointed out the usefulness of this data when used with viscometric and fluid loss data. They applied the term "relative viscosity" to the time required for the bob to complete movement in one direction: it is not a ratio of two viscosities. In spite of its wide usage, no standard testing procedure has been established by the industry to procedure has been established by the industry to obtain correlative data. A consistometer similar to the ones mentioned above, has been further modified and used in this study along the Fann viscometer Model 50. EQUIPMENT AND CALIBRATION Fig.1 is a section diagram of the consistometer. The consistency or equivalent viscosity of a test fluid is measured by electrically timing the movement of a soft iron bob that is magnetically pulled up and down in the sample container. Sound pulled up and down in the sample container. Sound signals created by the impingement of the bob inside the container are picked up by a microphone and transmitted to a recorder. The time required to pull the bob through a test fluid is a function of its pull the bob through a test fluid is a function of its consistency. The test fluid can be subjected to pressures up to 20,000 psi and temperatures up pressures up to 20,000 psi and temperatures up to 500 deg F. SPEJ p. 33

1984 ◽  
Vol 24 (03) ◽  
pp. 249-255 ◽  
Author(s):  
Jaime A. Lescarboura ◽  
Thomas R. Sifferman ◽  
Harry A. Wahl

Abstract A flow loop was used to evaluate the stability of fracturing fluids at high temperatures. The design provides enough pressure to prevent vaporization of water-base systems up to 350F [177C]. Crosslinked polymer systems from four service companies were evaluated at 180 and 245F [82 and 118C]. The tests showed that crosslinked fracturing fluids degrade with temperature and shear, losing much of their viscosity and proppant-carrying capacity in a few hours. Thermal stability is a major factor in selecting gels for fracturing deep, high-temperature reservoirs. Introduction Job failures in deep, hot wells can be caused by "sand-outs." These sandouts, or "screenouts," can result from inadequate carrying capacity (reduced viscosity) or too high a fluid loss (dehydration) for the polymer loading of the fracturing fluid. This study investigates the reduction in viscosity of crosslinked fracturing fluids with time at temperatures and shear rates approximating downhole conditions. A flow loop was used to investigate the rheological properties of fracturing fluids as a function of time under shear at temperatures as high as 245F [118C]. The pipe loop configuration was chosen because our field experience indicated that rotational viscometers were too "kind" to fracturing systems. We experienced sandouts that should not have happened if the crosslinked fracturing systems used had the flow characteristics that rotational viscometry indicated they had. The flow loop configuration also avoids some of the problems inherent in rotational viscometers, such as fluid climbing the shaft and contamination of the sample. Flow loops have been used to condition and evaluate drilling fluids at high temperatures. However, some of these instruments were not designed to give quantitative results. Our instrument permits measurement of apparent viscosity at known shear rates, flow index, and consistency index, all at high temperatures. This paper describes the flow loop, test procedures used, and results obtained. The flow loop gives reproducible results at high temperatures and allows the evaluation of the rheological properties of fracturing fluids under flow conditions nearer those encountered in actual fracturing jobs than do rotational, high-temperature instruments. Previous Work Previous Work Very little information has been reported on temperature stability of crosslinked fracturing fluids, especially under shearing conditions. Elbel and Thomas discussed the use of viscosity stabilizers for high-temperature fracturing. Conway et al. subjected crosslinked fracturing fluids to shear and to high temperatures. Hsu and Conway described the development of more stable crosslinked gels for use in deep, hot formations. All these investigators used the Fann 50 viscometer for their work, although Conway et al. used a pump to shear the samples before testing. Flow Loop Description The flow loop was built to evaluate the flow properties of drilling fluids, fracturing fluids, heavy crudes, and waxy crudes. The current test system can operate up to 350F [177C] and 250 psi [1,724 kPa]. The flow loop schematic is shown in Fig. 1. The test fluid is poured into the mixing vessel (Pfaudler) and then flows through the pump. The capacity of the system--including the heat exchangers, the test section, and the mixing unit--is about 25 gal [0.095 m3]. A high-accuracy, oval gear flowmeter was used for flow rate measurement. The meter was used only intermittently because it is a high- shear device that was originally intended to handle oil-base systems. A low-shear magnetic flowmeter has been added to the loop. The magnetic flowmeter shears the test fluids much less than the gear meter and can thus be left on continuously when testing shear-sensitive fracturing fluids. A differential pressure transducer measures pressure drop over the 20-ft-long [6.1-m], 0.957-in.-ID [2.43-cm] test section. The system is heated with a hot oil heater. An in-line, variable-shear-rate cup and bob viscometer allows continuous measurement of apparent viscosity at test temperature and pressure. It also-permits the running of rheograms to measure the flow pressure. It also-permits the running of rheograms to measure the flow parameters of the test fluid at any time during a test. parameters of the test fluid at any time during a test. A remote indication panel provides displays of flow rate, pressure drop, temperatures, shear stress, and shear rate. These values also are recorded on paper and magnetic tapes. A detailed description of the equipment, including recent improvements, is given in the Appendix. The improvements include the magnetic flowmeter mentioned previously, an automated data collection and reduction system, and a smaller pump. SPEJ p. 249


Spurious kinks in estimated palaeogeotherms may result from small errors in the calibration of the geothermometers and geobarometers. New data indicate that the equilibrium solubility of alumina in enstatite is even less than shown by recent studies, and that the slopes (d T /d P ) of the isopleths of equal alumina content are steeper than hitherto believed. Consequently, pressures of equilibration estimated from current formulations of the orthopyroxene-garnet geobarometer will be too high at high temperatures (> 1200 °C) and too low at low temperatures.


2021 ◽  
Author(s):  
Haifeng Li ◽  
Xinyu ZHang ◽  
Yi Wu ◽  
Feng ZHang ◽  
CHunlin Li

Abstract Personality has been observed in a variety of animal taxa with important implications in ecology and evolution. Exploring the influence of environmental temperature during early life on personality could help to understand the ontogeny of this phenotypic trait in animals. In this study, we reared newborn mosquitofish Gambusia affinis at high (30°C) and low (25°C) water temperatures and measured their shyness and exploration upon sexual maturity. We tested the repeatability of each behavioral trait; the correlation between them; and the effects of rearing temperature, sex, and body length on the behaviors. When growing up at low temperatures, female fish exhibited repeatability in shyness and exploration, and males exhibited marginal repeatability in shyness. However, neither of the 2 behaviors were repeatable when the fish were reared at high temperatures. There was a negative correlation between shyness and exploration, indicating that the 2 behaviors comprise a behavioral syndrome in this species. Mosquitofish reared at high temperatures were more explorative than those reared at low temperatures, while there was no difference in shyness between the 2 treatments. Body length and sex had no significant effects on the average values of the 2 behaviors. The results indicate that environmental temperature during early life could shape the personality of mosquitofish and modify the average of the behavioral traits. These findings might provide insights to understand the ontogeny of animal personality and how changes in environmental temperature influence animal dispersal by shaping their personality.


2017 ◽  
Vol 136 ◽  
pp. 96-102 ◽  
Author(s):  
Zhihua Luo ◽  
Jingjing Pei ◽  
Longxiang Wang ◽  
Peizhi Yu ◽  
Zhangxin Chen

2004 ◽  
Vol 811 ◽  
Author(s):  
Nobuhiro Kin ◽  
Koichiro Honda

ABSTRACTTo develop higher density FRAM requires reducing cell size. Therefore, the size effects resulting from device processing and the material's physical properties must be measured. Therefore, analyzing the electric characteristics of a single bit cell capacitor has become important. Two known characteristics of ferroelectric material are that the Vc increases at low temperatures, and the Pr falls at high temperatures. To further evaluate the impact of temperature on ferroelectrics, we constructed a new evaluation system based on a scanning probe microscope, that can measure the electric characteristics of a single bit cell capacitor. This system can be used in the temperature range from −120 degrees to 300 degrees C. We accomplished this by circulating liquid nitrogen around a SPM stage and by using an electrical heater. We measured the electrical properties of ferroelectric microcapacitors by using a sample with IrOx/PZT/Pt structure. Our measurements revealed that 2Pr really increases at low temperatures, and Pr decreases at high temperatures. That is, we have shown that Vc increases 30% at low temperatures and Pr decreases 10% also in an actual FRAM single bit cell capacitor.


2000 ◽  
Vol 646 ◽  
Author(s):  
Haruyuki Inui ◽  
Koji Ishikawa ◽  
Masaharu Yamaguchi

ABSTRACTEffects of ternary additions on the deformation behavior of single crystals of MoSi2 with the hard [001] and soft [0 15 1] orientations have been investigated in compression and compression creep. The alloying elements studied include V, Cr, Nb and Al that form a C40 disilicide with Si and W and Re that form a C11b disilicide with Si. The addition of Al is found to decrease the yield strength of MoSi2 at all temperatures while the additions of V, Cr and Nb are found to decrease the yield strength at low temperatures and to increase the yield strength at high temperatures. In contrast, the additions of W and Re are found to increase the yield strength at all temperatures. The creep strain rate for the [001] orientation is significantly lower than that for the [0 15 1] orientation. The creep strain rate for both orientations is significantly improved by alloying with ternary elements such as Re and Nb.


2021 ◽  
Author(s):  
Vikrant Wagle ◽  
Abdullah Yami ◽  
Michael Onoriode ◽  
Jacques Butcher ◽  
Nivika Gupta

Abstract The present paper describes the results of the formulation of an acid-soluble low ECD organoclay-free invert emulsion drilling fluid formulated with acid soluble manganese tetroxide and a specially designed bridging package. The paper also presents a short summary of field applications to date. The novel, non-damaging fluid has superior rheology resulting in lower ECD, excellent suspension properties for effective hole cleaning and barite-sag resistance while also reducing the risk of stuck pipe in high over balance applications. 95pcf high performance invert emulsion fluid (HPIEF) was formulated using an engineered bridging package comprising of acid-soluble bridging agents and an acid-soluble weighting agent viz. manganese tetroxide. The paper describes the filtration and rheological properties of the HPIEF after hot rolling at 300oF. Different tests such as contamination testing, sag-factor analysis, high temperature-high pressure rheology measurements and filter-cake breaking studies at 300oF were performed on the HPIEF. The 95pcf fluid was also subjected to particle plugging experiments to determine the invasion characteristics and the non-damaging nature of the fluids. The 95pcf HPIEF exhibited optimal filtration properties at high overbalance conditions. The low PV values and rheological profile support low ECDs while drilling. The static aging tests performed on the 95pcf HPIEF resulted in a sag factor of less than 0.53, qualifying the inherent stability for expected downhole conditions. The HPIEF demonstrated resilience to contamination testing with negligible change in properties. Filter-cake breaking experiments performed using a specially designed breaker fluid system gave high filter-cake breaking efficiency. Return permeability studies were performed with the HPIEF against synthetic core material, results of which confirmed the non-damaging design of the fluid. The paper thus demonstrates the superior performance of the HPIEF in achieving the desired lab and field performance.


2021 ◽  
Vol 13 (1) ◽  
pp. 140-151
Author(s):  
Minrui Guo ◽  
Xinglin Zhou

The effects of the cross-anisotropy of different materials of the asphalt surface layer and the depth-temperature relationship on pavement responses and damage are investigated. A three-dimensional Finite-Element Model (FEM) of the pavement, which considers the depth-temperature relationship of the surface layer under moving tire load, is developed. Pavement damage models are established to evaluate the damage ratio for primary rutting and fatigue cracking. The results show that the compressive strain at the bottom of the surface layer increases as the temperature increases, and the cross-anisotropy (n-value) decreases, indicating that a decrease in the horizontal modulus of different materials of the surface layer increases the damage ratio for primary rutting at high temperatures. The tensile strain at the bottom of the surface layer declines as the n-value increases to 1. For the same change in the n-value, the rate of change of the damage ratio for fatigue cracking is greater at low temperatures than at high temperatures, demonstrating that the number of allowable load repetitions is more sensitive at low temperatures. In addition, the effect of cross-anisotropy and temperature on the vertical stress are larger on the top of the base than in the subbase and subgrade.


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