Unveil the Unknown: Combining the Laboratory Study of Fracturing Fluids at High Pressure with a State-of-the-Art Hydraulic Fracturing Simulator

2018 ◽  
Author(s):  
Denis Vernigora ◽  
Olesya Olennikova ◽  
Sergey Parkhonyuk ◽  
Andrey Fedorov ◽  
Ludmila Belyakova ◽  
...  
Keyword(s):  
High Pressure ◽  
Hydraulic Fracturing ◽  
Laboratory Study ◽  
State Of The Art ◽  
Fracturing Fluids

Revisiting the High-Pressure Properties of the Metal-Organic Frameworks ZIF-8 and ZIF-67

2020 ◽  
Author(s):  
Pia Vervoorts ◽  
Stefan Burger ◽  
Karina Hemmer ◽  
Gregor Kieslich
Keyword(s):  
High Pressure ◽  
State Of The Art ◽  
Energy Landscape ◽  
Structural Flexibility ◽  
Zeolitic Imidazolate Frameworks ◽  
Stimuli Responsive ◽  
X Ray Diffraction ◽  
X Ray ◽  
Open Questions ◽  
Metal Organic

The zeolitic imidazolate frameworks ZIF-8 and ZIF-67 harbour a series of fascinating stimuli responsive properties. Looking at their responsitivity to hydrostatic pressure as stimulus, open questions exist regarding the isotropic compression with non-penetrating pressure transmitting media. By applying a state-of-the-art high-pressure powder X-ray diffraction setup, we revisit the high-pressure behaviour of ZIF-8 and ZIF-67 up to <i>p</i> = 0.4 GPa in small pressure increments. We observe a drastic, reversible change of high-pressure powder X-ray diffraction data at <i>p</i> = 0.3 GPa, discovering large volume structural flexibility in ZIF-8 and ZIF-67. Our results imply a shallow underlying energy landscape in ZIF-8 and ZIF-67, an observation that might point at rich polymorphism of ZIF-8 and ZIF-67, similar to ZIF-4(Zn).<br>

Revisiting the High-Pressure Properties of the Metal-Organic Frameworks ZIF-8 and ZIF-67

2020 ◽  
Author(s):  
Pia Vervoorts ◽  
Stefan Burger ◽  
Karina Hemmer ◽  
Gregor Kieslich
Keyword(s):  
High Pressure ◽  
State Of The Art ◽  
Energy Landscape ◽  
Structural Flexibility ◽  
Zeolitic Imidazolate Frameworks ◽  
Stimuli Responsive ◽  
X Ray Diffraction ◽  
X Ray ◽  
Open Questions ◽  
Metal Organic

The zeolitic imidazolate frameworks ZIF-8 and ZIF-67 harbour a series of fascinating stimuli responsive properties. Looking at their responsitivity to hydrostatic pressure as stimulus, open questions exist regarding the isotropic compression with non-penetrating pressure transmitting media. By applying a state-of-the-art high-pressure powder X-ray diffraction setup, we revisit the high-pressure behaviour of ZIF-8 and ZIF-67 up to <i>p</i> = 0.4 GPa in small pressure increments. We observe a drastic, reversible change of high-pressure powder X-ray diffraction data at <i>p</i> = 0.3 GPa, discovering large volume structural flexibility in ZIF-8 and ZIF-67. Our results imply a shallow underlying energy landscape in ZIF-8 and ZIF-67, an observation that might point at rich polymorphism of ZIF-8 and ZIF-67, similar to ZIF-4(Zn).<br>

scholarly journals Laboratory Testing of Fracture Conductivity Damage by Foam-Based Fracturing Fluids in Low Permeability Tight Gas Formations

Energies ◽  
2021 ◽  
Vol 14 (6) ◽  
pp. 1783
Author(s):  
Klaudia Wilk-Zajdel ◽  
Piotr Kasza ◽  
Mateusz Masłowski
Keyword(s):  
Hydraulic Fracturing ◽  
Guar Gum ◽  
Polymer Concentration ◽  
Laboratory Research ◽  
Damage Effect ◽  
Tight Gas ◽  
Fracturing Fluid ◽  
Fracture Conductivity ◽  
Fracturing Fluids ◽  
Sandstone Rock

In the case of fracturing of the reservoirs using fracturing fluids, the size of damage to the proppant conductivity caused by treatment fluids is significant, which greatly influence the effective execution of hydraulic fracturing operations. The fracturing fluid should be characterized by the minimum damage to the conductivity of a fracture filled with proppant. A laboratory research procedure has been developed to study the damage effect caused by foamed and non-foamed fracturing fluids in the fractures filled with proppant material. The paper discusses the results for high quality foamed guar-based linear gels, which is an innovative aspect of the work compared to the non-foamed frac described in most of the studies and simulations. The tests were performed for the fracturing fluid based on a linear polymer (HPG—hydroxypropyl guar, in liquid and powder form). The rheology of nitrogen foamed-based fracturing fluids (FF) with a quality of 70% was investigated. The quartz sand and ceramic light proppant LCP proppant was placed between two Ohio sandstone rock slabs and subjected to a given compressive stress of 4000–6000 psi, at a temperature of 60 °C for 5 h. A significant reduction in damage to the quartz proppant was observed for the foamed fluid compared to that damaged by the 7.5 L/m3 natural polymer-based non-foamed linear fluid. The damage was 72.3% for the non-foamed fluid and 31.5% for the 70% foamed fluid, which are superior to the guar gum non-foamed fracturing fluid system. For tests based on a polymer concentration of 4.88 g/L, the damage to the fracture conductivity by the non-foamed fluid was 64.8%, and 26.3% for the foamed fluid. These results lead to the conclusion that foamed fluids could damage the fracture filled with proppant much less during hydraulic fracturing treatment. At the same time, when using foamed fluids, the viscosity coefficient increases a few times compared to the use of non-foamed fluids, which is necessary for proppant carrying capacities and properly conducted stimulation treatment. The research results can be beneficial for optimizing the type and performance of fracturing fluid for hydraulic fracturing in tight gas formations.

scholarly journals Cavitation patterns in high-pressure homogenization nozzles with cylindrical orifices: Influence of mixing stream in Simultaneous Homogenization and Mixing

2021 ◽  
Author(s):  
V. Gall ◽  
E. Rütten ◽  
H. P. Karbstein
Keyword(s):  
High Pressure ◽  
Process Design ◽  
High Speed ◽  
State Of The Art ◽  
Back Pressure ◽  
High Pressure Homogenization ◽  
Unit Operation ◽  
Mixing Chamber ◽  
Cavitation Intensity ◽  
Droplet Sizes

AbstractHigh-pressure homogenization is the state of the art to produce high-quality emulsions with droplet sizes in the submicron range. In simultaneous homogenization and mixing (SHM), an additional mixing stream is inserted into a modified homogenization nozzle in order to create synergies between the unit operation homogenization and mixing. In this work, the influence of the mixing stream on cavitation patterns after a cylindrical orifice is investigated. Shadow-graphic images of the cavitation patterns were taken using a high-speed camera and an optically accessible mixing chamber. Results show that adding the mixing stream can contribute to coalescence of cavitation bubbles. Choked cavitation was observed at higher cavitation numbers σ with increasing mixing stream. The influence of the mixing stream became more significant at a higher orifice to outlet ratio, where a hydraulic flip was also observed at higher σ. The decrease of cavitation intensity with increasing back-pressure was found to be identical with conventional high-pressure homogenization. In the future, the results can be taken into account in the SHM process design to improve the efficiency of droplet break-up by preventing cavitation or at least hydraulic flip.

scholarly journals pH-responsive viscoelastic supramolecular viscosifiers based on dynamic complexation of zwitterionic octadecylamidopropyl betaine and triamine for hydraulic fracturing applications

RSC Advances ◽  
2021 ◽  
Vol 11 (37) ◽  
pp. 22517-22529
Author(s):  
Shuhao Liu ◽  
Yu-Ting Lin ◽  
Bhargavi Bhat ◽  
Kai-Yuan Kuan ◽  
Joseph Sang-II Kwon ◽  
...  
Keyword(s):  
Hydraulic Fracturing ◽  
Ph Responsive ◽  
Fracturing Fluids ◽  
Efficient Transport ◽  
Critical Components

Viscosity modifying agents are one of the most critical components of hydraulic fracturing fluids, ensuring the efficient transport and deposition of proppant into fissures.

Chemistry, Physical Nature, and Rheology of Aqueous Stimulation Foams

1981 ◽  
Vol 21 (04) ◽  
pp. 410-414 ◽  
Author(s):  
David L. Holcomb ◽  
Ed Callaway ◽  
Lynn L. Curry
Keyword(s):  
High Pressure ◽  
Surfactant Concentration ◽  
High Pressures ◽  
Foam Stability ◽  
Streaming Potential ◽  
Physical Nature ◽  
Chemical Additives ◽  
Laboratory Equipment ◽  
Foaming Agent ◽  
Fracturing Fluids

Abstract Laboratory equipment has been designed specificallyto study effectively the microscopic structure offlowing foams at high pressures. In addition, application of foaming-agent optimization techniquesto design stable foams at varying foam qualities isdemonstrated at high pressures - i.e., 500 to 2,000psig (3448 to 13 792 kPa). Capillary viscosity datafor these foams is established and correlated with avideo-photomicroscopic study of the flowing foamand their designated bubble qualities. Foaming-agent screening information from the tests is providedindicating the foaming-agent generic chemistry thatallows optimal foam stability under high-pressure conditions. Introduction The study of contemporary foam rheology has arather interrupted history beginning with Fried'swork in 1961 on a foam drive process, which was followed by Raza and Marsden's 1965 paper onrheology and streaming potential. During 1969Blauer et al. studied foam flow properties andmade successful comparisons of data obtained incapillary viscometer tests and actual oilfield tubulardata. These investigations lead to the development ofdata and calculated procedures for using high-qualityfoams as fracturing fluids to transport proppanteffectively with extremely low formation damage as aresult of smaller amounts of water or liquid incontact with the formation. With all the theoretical depiction of flowing foamstructure, it was felt that a study was needed to showvisually the actual flowing foam under pressure. Thiswas undertaken in a study' where oil-foamingsurfactant concentrations were optimized using anapparatus similar to ours. (The majority of foamstimulation treatments use aqueous bases, and thisstudy was conducted exclusively with them.) The goal of this project was to design equipmentthat could be adapted to a TV camera/microscopesystem to allow videotaping of flowing foam in aview cell under pressure. To study effectively thechemical nature of four different surfactant foams, the temperature was kept at 80 deg. F (26.7 deg. C)throughout the study. Also, one foam quality of88%, or 88% nitrogen and 12% water was chosenusing 2% KCl water as the liquid phase. Selected pictures from the videotape are presented to show thesuccession of bubble-structure change with pressure.In addition, the effect of surfactant concentration (which had been thought to play a small role, if any, in the rheology of foams) is shown. This allows aneven greater ability to optimize surfactant concentration in the production of stable foams forstimulation. The subjective bubble-quality scale of Holcomb etal. is refined by showing the average bubblediameters at various study pressures and is demonstrated photographically in Figs. 1 through 3.For the viscosity tests through the capillaryviscometer system, a constant 1,000-psi input pressure was maintained for the generation of foam. Testing Apparatus, Procedure, and Chemical Additives The high-pressure test apparatus was designed tomeet the rate requirements for a laboratory testsample of 700 cm (liquid) or more. The system iscapable of pressures to 3,000 psi (20 683 kPa). The pump is a Williams Oscillamatic TM single-strokemodel with a pressure rating to 10,000 psi (68 946kPa). All main lines are 6.35 mm in diameter. Trunklines to the gauges are 3.175-mm-diameter tubing.All tubing in the apparatus is 316 stainless steel. (SeeFig. 4.) SPEJ P. 410^

scholarly journals Environmentally friendly, rheoreversible, hydraulic-fracturing fluids for enhanced geothermal systems

Geothermics ◽  
2015 ◽  
Vol 58 ◽  
pp. 22-31 ◽  
Author(s):  
Hongbo Shao ◽  
Senthil Kabilan ◽  
Sean Stephens ◽  
Niraj Suresh ◽  
Anthon N. Beck ◽  
...  
Keyword(s):  
Hydraulic Fracturing ◽  
Environmentally Friendly ◽  
Enhanced Geothermal Systems ◽  
Geothermal Systems ◽  
Fracturing Fluids
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