scholarly journals Preparation and Evaluation of a Stable Solid State Ion Selective Electrode of Polypyrrole/Electrochemically Reduced Graphene/Glassy Carbon Substrate for Soil Nitrate Sensing

Author(s):  
Pu Pan ◽  
Water ◽  
2021 ◽  
Vol 13 (20) ◽  
pp. 2869
Author(s):  
Cecylia Wardak ◽  
Karolina Pietrzak ◽  
Małgorzata Grabarczyk

A new copper sensitive all solid-state ion-selective electrode was prepared using multiwalled carbon nanotubes-ionic liquid (1-butyl-3-methylimidazolium hexafluorophosphate) nanocomposite as an additional membrane component. The effect of nanocomposite content in the membrane on the electrode parameters was investigated. The study compares, among others, detection limits, sensitivity, and the linearity ranges of calibration curves. Content 6 wt.% was considered optimal for obtaining an electrode with a Nernstian response of 29.8 mV/decade. An electrode with an optimal nanocomposite content in the membrane showed a lower limit of detection, a wider linear range and pH range, as well as better selectivity and potential stability compared to the unmodified electrode. It was successfully applied for copper determination in real water samples.


2013 ◽  
Vol 39 (4) ◽  
pp. 3765-3769 ◽  
Author(s):  
I. Khalakhan ◽  
M. Dubau ◽  
S. Haviar ◽  
J. Lavková ◽  
I. Matolínová ◽  
...  

2019 ◽  
Vol 52 (1-2) ◽  
pp. 23-33 ◽  
Author(s):  
Kun'ichi Miyazawa ◽  
Takuro Nagai ◽  
Koji Kimoto ◽  
Masaru Yoshitake ◽  
Yumi Tanaka

2020 ◽  
Vol 7 (11) ◽  
pp. 2070059
Author(s):  
Gaurav Chauhan ◽  
Alejandro Lujambio Ángeles ◽  
Everardo Gonzalez‐González ◽  
Manish M. Kulkarni ◽  
Braulio Cardenas‐Benitez ◽  
...  

1971 ◽  
Vol 54 (4) ◽  
pp. 760-763
Author(s):  
William L Hoover ◽  
James R Melton ◽  
Peggy A Howard

Abstract A method for determining low levels of iodide in feeds and plants is proposed. The samples are mixed with a 10% phosphate solution to maintain relatively constant ionic strength and pH and analyzed with a solid-state iodide electrode. Ashing is not required and there are no significant interferences by ions commonly found in feeds. The method is accurate in determining iodide content ranging from 10.0 ppm to high concentrations. Necessary conditions for storing and cleaning the electrodes are described. The proposed method is rapid and results compare favorably with AOAC method 7.091.


10.5772/8741 ◽  
2010 ◽  
Author(s):  
Kevin J. ◽  
Gordon R. ◽  
Tessema Astatkie ◽  
John F. ◽  
Paul C.

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