Microstructural and Chemical Components of Ceramic-Metal Interfacial Fracture Energies

1986 ◽  
Vol 72 ◽  
Author(s):  
R. M. Cannon ◽  
V. Jayaram ◽  
B. J. Dalgleish ◽  
R. M. Fisher
Keyword(s):  
Electron Microscopy ◽  
Fracture Toughness ◽  
Flow Stress ◽  
Plastic Strain ◽  
Chemical Bonding ◽  
Chemical Components ◽  
Internal Stresses ◽  
Relative Importance ◽  
Metal Interfaces ◽  
Local Internal Stresses

AbstractFailure of ceramic-metal interfaces induced by residual or applied stress is often brittle in nature although plastic strain in one or more bonding layers may add to the fracture energy for decohesion. Thus, the fracture toughness depends on chemical bonding across the interface, the plasticity and flow stress of the metal as well as other factors, arising from local internal stresses and the microstructure of the ceramic-metal couple, that cause crack tip branching, deflection, bridging, blunting or shielding. Electron microscopy and DCB testing of metal-glass systems provide insights into the relative importance of factors that determine the decohesion resistance.

scholarly journals Microstructure and dislocation hardening mechanism of VT8 alloy

2021 ◽  
Vol 99 (3) ◽  
pp. 22-31
Author(s):  
Z.A. Duriagina ◽  
◽  
I.A. Lemishka ◽  
O.S. Filimonov ◽  
A.M. Trostianchyn ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Titanium Alloy ◽  
Dislocation Density ◽  
Internal Stresses ◽  
Structural Components ◽  
Transmission Electron ◽  
Dislocation Densities ◽  
Local Internal Stresses ◽  
Scalar Dislocation Density

Specimens of titanium alloy VT8, which is used for the manufacture of gas turbine engine elements, were investigated in the initial state and after fracture toughness testing by methods of transmission electron microscopy and diffraction analysis. The features of the microstructure, structure morphology, the nature of phase distribution and structural components were established. Defects in the crystal structure, the formations of dislocation inhomogeneities and local concentrators of internal stresses were identified using JEM-200CX transmission electron microscope. The scalar dislocation density is determined by the secant method. The study of VT8 titanium alloy samples before and after destruction, which is used for the manufacture of GTE elements, using the methods of transmission electron microscopy and diffraction analysis was made. Microstructural investigations for a detailed analysis of the structure features, morphology and phase formations distribution, as well as their components establishment, the nature of crystal lattice defects, the formation of dislocation inhomogeneities and local concentrators of internal stresses were performed on a JEM-200CX transmission electron microscope. The scalar dislocation density was measured by the secant method. It is shown that the studied samples of VT8 titanium alloy are characterized by a two-phase (α + β) microstructure in the form of large -phase plates, 0.15 ... 0.76 μm in size, interspersed with an insignificant amount of thin-plate β-phase, with a size of 0.04 ... 0.21 μm. Based on scalar dislocation densities, the level of local internal stresses in the places of dislocation accumulations, which are sources of crack formation, was analytically estimated. Dispersed particles of secondary phases characterized by different sizes and different structure morphologies were identified. The calculated dislocation densities and an estimate of the average distance over which they move in the process of deformation are used as the basis for creating a statistical map of localized deformation level indicators in the alloy structural components and on the fracture surface. It is shown that as a result of fracture after testing for low-cycle fatigue, the dislocation density increases, the level of local internal stresses increases, and the formation of a cellular structure in the α- and β-phases and deformation grain-boundary defects occurs. Keywords: VT8 alloy, dislocation structure, microstructure, transmission electron microscopy, local internal stresses.

Fostering crack deviation via local internal stresses in Al/NiTi composites and its correlation with fracture toughness

2019 ◽  
Vol 126 ◽  
pp. 105617 ◽  
Author(s):  
Lv Zhao ◽  
Lipeng Ding ◽  
Jeroen Soete ◽  
Hosni Idrissi ◽  
Greet Kerckhofs ◽  
...  
Keyword(s):  
Fracture Toughness ◽  
Internal Stresses ◽  
Local Internal Stresses

A Modified Peric Model for Al-Mg Alloy Sheet with Rate-Independent Initial Yield Stress at Warm Temperatures

2019 ◽  
Vol 287 ◽  
pp. 3-7
Author(s):  
Yong Zhang ◽  
Qing Zhang ◽  
Yuan Tao Sun ◽  
Xian Rong Qin
Keyword(s):  
Flow Stress ◽  
Plastic Strain ◽  
Strain Rate ◽  
Yield Stress ◽  
Constitutive Models ◽  
Mg Alloy ◽  
Initial Yield Stress ◽  
Initial Yield ◽  
Rate Dependent ◽  
Dependent Flow

The constitutive modeling of aluminum alloy under warm forming conditions generally considers the influence of temperature and strain rate. It has been shown by published flow stress curves of Al-Mg alloy that there is nearly no effect of strain rate on initial yield stress at various temperatures. However, most constitutive models ignored this phenomenon and may lead to inaccurate description. In order to capture the rate-independent initial yield stress, Peric model is modified via introducing plastic strain to multiply the strain rate, for eliminating the effect of strain rate when the plastic strain is zero. Other constitutive models including the Wagoner, modified Hockett–Sherby and Peric are also considered and compared. The results show that the modified Peric model could not only describe the temperature-and rate-dependent flow stress, but also capture the rate-independent initial yield stress, while the Wagoner, modified Hockett–Sherby and Peric model can only describe the temperature-and rate-dependent flow stress. Moreover, the modified Peric model could obtain proper static yield stress more naturally, and this property may have potential applications in rate-dependent simulations.

Organoclay-reinforced polyethersulfone-modified epoxy-based hybrid nanocomposites

2011 ◽  
Vol 23 (7) ◽  
pp. 526-534 ◽  
Author(s):  
Yang Wang ◽  
Boming Zhang ◽  
Jinrui Ye
Keyword(s):  
Electron Microscopy ◽  
Fracture Toughness ◽  
Electron Microscope ◽  
Optical Microscope ◽  
Mechanical Analysis ◽  
Hybrid Nanocomposites ◽  
X Ray Diffraction ◽  
Transmission Electron ◽  
Modified Epoxy ◽  
Scanning Electron

Hybrid nanocomposites were successfully prepared by the incorporation of polyethersulfone (PES) and organoclay into epoxy resin. They had higher fracture toughness than the prepared PES/epoxy blend and organoclay/epoxy nanocomposites. The microstructures of the hybrid nanocomposites were studied. They were comprised of homogeneous PES/epoxy semi-interpenetrating network (semi-IPN) matrices and organoclay micro-agglomerates made up of tactoid-like regions composed of ordered exfoliated organoclay with various orientations. The former was confirmed with dynamic mechanical analysis, scanning electron microscopy and transmission electron microscopy, while the latter was successfully observed with X-ray diffraction measurements, optical microscope, scanning electron microscope and transmission electron microscope. The improvement of their fracture toughness was due to the synergistic toughening effect of the PES and the organoclay and related to their microstructures.

Effect of Sintering Temperature on Microstructure and Mechanical Properties of Al2O3-TiC-ZrO2 Ceramic Composites

2012 ◽  
Vol 476-478 ◽  
pp. 1031-1035
Author(s):  
Wei Min Liu ◽  
Xing Ai ◽  
Jun Zhao ◽  
Yong Hui Zhou
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Relative Density ◽  
Sintering Temperature ◽  
Ceramic Composites ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

Al2O3-TiC-ZrO2ceramic composites (ATZ) were fabricated by hot-pressed sintering. The phases and microstructure of the composites were studied by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The relative density and mechanical properties (flexural strength, fracture toughness and Vicker’s hardness) of the composites were tested. The results show that the microstructure of the composites was the gray core-white rim. With the increase of sintering temperature, the relative density and mechanical properties of the composites increased first and then decreased. The composite sintered at 1705°C has the highest synthetical properties, and its relative density, flexural strength, fracture toughness and Vickers hardness are 98.3%,970MPa,6.0 MPa•m1/2and 20.5GPa, respectively.

Titanium Effect on Microstructure and Fracture toughness of Al2O3-BASED Composites

2011 ◽  
Vol 691 ◽  
pp. 32-36
Author(s):  
José G. Miranda-Hernández ◽  
Elizabeth Refugio-García ◽  
Eduardo Térres-Rojas ◽  
Enrique Rocha-Rangel
Keyword(s):  
Electron Microscopy ◽  
Fracture Toughness ◽  
Scanning Electron Microscopy ◽  
Fine Particles ◽  
Ceramic Matrix ◽  
High Energy ◽  
Titanium Content ◽  
Indentation Method ◽  
Sintered Temperature ◽  
Scanning Electron

The effect of different titanium additions (0.5, 1, 2, 3 and 10 vol. %), milling intensity (4 and 8 h) and sintered temperature (1500 and 1600 °C) on microstructure and fracture toughness of Al2O3-based composites was analyzed in this study. After high energy milling of a titanium and Al2O3mixtures, powder mixture presents fine distribution and good homogenization between ceramic and metal. After milling powders during 8 h they were obtained very fine particles with 200 nm average sizes. Microstructures of the sintered bodies were analyzed with a scanning electron microscopy, where it was observed that the microstructure presents the formation of a small and fine metallic net inside the ceramic matrix. From fracture toughness measurements realized by the fracture indentation method, it had that when titanium content in the composite increases, fracture toughness is enhanced until 83% with respect to the fracture toughness of pure Al2O3. This behavior is due to the formation of metallic bridges by titanium in the Al2O3matrix.

Modified Equation to Predict Leak/Rupture Criteria for Axially Through-Wall Notched X80 and X100 Linepipes Having Higher Charpy Energy

2004 ◽  
Author(s):  
Shinobu Kawaguchi ◽  
Naoto Hagiwara ◽  
Mitsuru Ohata ◽  
Masao Toyoda
Keyword(s):  
Fracture Toughness ◽  
Flow Stress ◽  
Pipe Material ◽  
Test Results ◽  
Absorbed Energy ◽  
Bending Tests ◽  
Full Scale Tests ◽  
Hoop Stresses ◽  
The Relationship ◽  
Modified Equation

A method of predicting the leak/rupture criteria for API 5L X80 and X100 linepipes was evaluated, based on the results of hydrostatic full-scale tests for X60, X65, X80 and X100 linepipes with an axially through-wall (TW) notch. The TW notch test results clarified the leak/rupture criteria, that is, the relationship between the initial notch lengths and the maximum hoop stresses during the TW notch tests. The obtained leak/rupture criteria were then compared to the prediction of the Charpy V-notch (CVN) absorbed energy-based equation, which has been proposed by Kiefner et al. The comparison revealed that the CVN-based equation was not applicable to the pipes having a CVN energy (Cv) greater than 130 J and flow stress greater than X65. In order to predict the leak/rupture criteria for these linepipes, the static absorbed energy for ductile cracking, (Cvs)i, was introduced as representing the fracture toughness of a pipe material. The (Cvs)i value was determined from the microscopic observation of the cut and buffed Charpy V-notch specimens after static 3-point bending tests. The CVN energy in the original CVN-based equation was replaced by an equivalent CVN energy, (Cv)eq’ which was defined as follows: (Cv)eq = 4.5 (Cvs)i. The leak/rupture criteria for the X80 and X100 linepipes with higher CVN energies were reasonably predicted by the modified equation using the (Cvs)i value.

A Weibull Stress Approach Incorporating the Coupling Effect of Constraint and Plastic Strain in Cleavage Fracture Toughness Predictions

2014 ◽  
Author(s):  
Claudio Ruggieri ◽  
Robert H. Dodds
Keyword(s):  
Fracture Toughness ◽  
Plastic Strain ◽  
Cleavage Fracture ◽  
Coupling Effect ◽  
Crack Size ◽  
Parameter Analysis ◽  
Pressure Vessel Steel ◽  
Fracture Parameter ◽  
Vessel Steel ◽  
Weibull Stress

This work describes a micromechanics methodology based upon a local failure criterion incorporating the strong effects of plastic strain on cleavage fracture coupled with statistics of microcracks. A central objective is to gain some understanding on the role of plastic strain on cleavage fracture by means of a probabilistic fracture parameter and how it contributes to the cleavage failure probability. A parameter analysis is conducted to assess the general effects of plastic strain on fracture toughness correlations for conventional SE(B) specimens with varying crack size over specimen width ratios. Another objetive is to evaluate the effectiveness of the modified Weibull stress (σ̃w) model to correct effects of constraint loss in PCVN specimens which serve to determine the indexing temperature, T0, based on the Master Curve methodology. Fracture toughness testing conducted on an A285 Grade C pressure vessel steel provides the cleavage fracture resistance (Jc) data needed to estimate T0. Very detailed non-linear finite element analyses for 3-D models of plane-sided SE(B) and PCVN specimens provide the evolution of near-tip stress field with increased macroscopic load (in terms of the J-integral) to define the relationship between σ̃w and J. For the tested material, the Weibull stress methodology yields estimates for the reference temperature, T0, from small fracture specimens which are in good agreement with the corresponding estimates derived from testing of much larger crack configurations.

Effect of BN Short Fiber Content on Mechanical Properties of ZrB2-SiC UHTCs

2012 ◽  
Vol 512-515 ◽  
pp. 706-709 ◽  
Author(s):  
Chang Ling Zhou ◽  
Yan Yan Wang ◽  
Zhi Qiang Cheng ◽  
Chong Hai Wang ◽  
Rui Xiang Liu
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fracture Toughness ◽  
Scanning Electron Microscopy ◽  
Flexural Strength ◽  
Hot Pressing ◽  
Ceramic Composites ◽  
Short Fiber ◽  
Hot Pressing Sintering ◽  
Scanning Electron

ZrB2-20%volSiC ceramic composites with different volume of BN short fiber were fabricated by the hot-pressing sintering under 2000°C. The content of BN short fiber changed from 0 to 15vol%. The density, flexural strength, fracture toughness and thermal expansions coefficient were studied. The microstructures of the samples were observed by scanning electron microscopy. The results show that the introducing of BN short fiber into the ZrB2-20%volSiC lead to a serious of change to the mechanical properties of the ceramic. When the content of the BN short fiber is 10vol%, the flexural strength and fracture toughness reach 422.1MPa and 6.15 MPa•m 1/2 respectively. And the mechanism of the increasing toughness was studied.

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