Under Bump Metallization Development for Eutectic Pb-Sn Solders

1998 ◽  
Vol 515 ◽  
Author(s):  
S. J. Hong ◽  
T. M. Korhonen ◽  
M. A. Korhonen ◽  
C.-Y. LI

ABSTRACTDue to its advantage in number of I/Os over other interconnection method, flip chip interconnection technology plays a key role in today's electronics packaging. Good understanding of interfacial reactions between the solder balls and under bump metallizations (UBM) is crucial in producing sound and reliable solder joints. In the present paper, several new under bump metallization (UBM) schemes using Ni or CuNi alloys as solderable layer are investigated. Cr or Ti is used as the adhesion layer. Test joint are made by reflowing eutectic Pb-Sn solder balls on UBMs and through the use of scanning electron microscopy (SEM) and micromechanical shear testing, the reliability of the UBM scheme is determined. Experimental result shows that some of the new schemes, featuring CuNi wettable layer with Cr or Ti adhesion layer produce reliable joints.

2012 ◽  
Vol 573-574 ◽  
pp. 1156-1160
Author(s):  
Hong Yu Shi ◽  
Hui Liu ◽  
Shu Lan Guo

This study is focusing on the protein sand binder on the performance of wet sand, and explores the protein binding mold sand reusability and reclamation. With thermal analysis and scanning electron microscopy testing, and by comparing with other traditional technologies, the experimental result shows that it is a more environmental friendly.


2005 ◽  
Vol 78 (5) ◽  
pp. 844-854 ◽  
Author(s):  
Jong Myoung Kim

Abstract Change in the morphological features of the adhesion layer formed on brass was observed with Field Emission-Scanning Electron Microscopy (FE-SEM). The effect of the key compounding ingredients on the morphology of the adhesion layer was studied. Morphology of the various metal sulfides of cobalt, zinc, copper, bronze and brass was also observed with FE-SEM. Fracture mode appeared during the pull-out test was categorized and was correlated with the adhesion strength. The damage on the adhesion layer after humidity aging test was examined by FE-SEM.


2005 ◽  
Vol 20 (11) ◽  
pp. 2914-2918 ◽  
Author(s):  
R. Kinyanjui ◽  
L.P. Lehman ◽  
L. Zavalij ◽  
E. Cotts

The degree of undercooling of Sn in near eutectic, SnAgCu solder balls upon cooling at a rate of 1 °C/s from the melt was examined and found to increase linearly with inverse nominal sample diameter (for balls of radius between 100 and 1000 μm). The mean undercooling for SnAgCu solder balls in a flip chip assembly was 62 °C. The microstructures of these different samples were examined by means of scanning electron microscopy. The Sn dendrite arm width was observed to monotonically increase with ball diameter, indicating a possible dependence of the mechanical response of such solder balls upon size.


1997 ◽  
Vol 505 ◽  
Author(s):  
T. M. Korhonen ◽  
S. J. Hong ◽  
P. Su ◽  
C. Zhou ◽  
M. A. Korhonen ◽  
...  

ABSTRACTSeveral under bump metallisation (UBM) schemes using Ni or CuNi alloys as the solderable layer were investigated. Cr or Ti was used as the adhesion layer. The UBM pads of different compositions were sputter deposited on silicon wafers and patterned using standard photolithographic processes. Eutectic Sn-Pb solder balls were reflowed on top of the pads. The resulting interfacial microstructures were examined by SEMIEDX analysis of cross-sectioned samples. The integrity of the UBMIsolder interface was characterized by micromechanical shear testing of flip chip test samples. Growth of intermetallic layers was found to be significantly slower in Ni and CuNi schemes compared to pure Cu. The joints on Ni and CuNi had also a better adhesion at the UBM/solder interface, and in the shear tests the fracture occurred through the solder


2017 ◽  
Vol 2017 (1) ◽  
pp. 000619-000623 ◽  
Author(s):  
Timothy Dittman ◽  
David Ebner ◽  
Alex Bailey

Abstract Reliability in microelectronic packaging has been, and will continue to be, a major concern that must be taken into account early in the design of a package. System-in-package (SiP) assemblies, as well as other high density packaging technologies, are being used in many system architectures in order to incorporate a high level of integration, reduce cost and fit on tighter next higher assembly (NHA) grid spacing. While these technologies are being adopted into system architectures, there is limited test data on the reliability of these packages in military applications. A better understanding of the impacts of design variables in a SiP assembly allows the design community to determine the most appropriate packaging solution for use in a given application. The term “system-in-package” covers a wide range of microelectronic packaging technologies. Microelectronic packaging technology is trending towards taking the SiP concept and incorporating a very high level of integration within as small of a footprint as possible. In many cases, a fan out design technique is used in order to utilize die with high density bump patterns and then use an interposer technology to increase the bump pitch to match pitches achievable on NHA board technologies. While increasing the packaging density appears beneficial in theory, its reliability becomes a risk as the complexity of the assembly increases and more interfaces are added. Mechanical and structural considerations must be taken into account when designing this type of assembly in order to limit the stresses observed in the assembly, especially when exposed to environmental conditions. This study will focus on traditional two dimensional (2D) integrated circuit (IC) designs. For the purposes of this study, a 2D IC package will be considered as multiple die attached to a SiP substrate via flip-chip bumps. These SiP assemblies will in turn be attached to a test circuit board via solder bumps, which are at a larger pitch relative to the flip-chip bump patterns. A daisy-chain circuit design was incorporated into the test board and die in order to evaluate the reliability of the assembly interconnects at various points throughout the assembly. Design variables such as underfill material, SiP substrate material and flip-chip bump density were incorporated into a design of experiments in order to evaluate their impact on the reliability of a SiP assembly. The materials selected for use in this testing allow for the evaluation of the impacts of coefficient of thermal expansion (CTE), modulus and other material properties on the reliability of a SiP assembly. Reliability of the assemblies was tested via temperature cycling and biased humidity testing. Successful reliability of each test was dictated by the continuity of the daisy chain circuits throughout testing, as well as a visual examination of the interconnects after test. Samples of each assembly design configuration were used in cross sectional analysis to further examine the effects of the reliability on the assembly. Material characterization techniques such as scanning electron microscopy (SEM) and focus ion beam scanning electron microscopy (FIB-SEM) were used, as necessary, to investigate failure modes. This paper will review a design of experiments study of SiP assemblies and present the results of reliability testing on various SiP assembly designs. Further study is suggested for the use of these results in developing and refining finite element models capable of accurately predicting failure modes in SiP assemblies.


Author(s):  
P.S. Porter ◽  
T. Aoyagi ◽  
R. Matta

Using standard techniques of scanning electron microscopy (SEM), over 1000 human hair defects have been studied. In several of the defects, the pathogenesis of the abnormality has been clarified using these techniques. It is the purpose of this paper to present several distinct morphologic abnormalities of hair and to discuss their pathogenesis as elucidated through techniques of scanning electron microscopy.


Author(s):  
P.J. Dailey

The structure of insect salivary glands has been extensively investigated during the past decade; however, none have attempted scanning electron microscopy (SEM) in ultrastructural examinations of these secretory organs. This study correlates fine structure by means of SEM cryofractography with that of thin-sectioned epoxy embedded material observed by means of transmission electron microscopy (TEM).Salivary glands of Gromphadorhina portentosa were excised and immediately submerged in cold (4°C) paraformaldehyde-glutaraldehyde fixative1 for 2 hr, washed and post-fixed in 1 per cent 0s04 in phosphosphate buffer (4°C for 2 hr). After ethanolic dehydration half of the samples were embedded in Epon 812 for TEM and half cryofractured and subsequently critical point dried for SEM. Dried specimens were mounted on aluminum stubs and coated with approximately 150 Å of gold in a cold sputtering apparatus.Figure 1 shows a cryofractured plane through a salivary acinus revealing topographical relief of secretory vesicles.


Author(s):  
Nakazo Watari ◽  
Yasuaki Hotta ◽  
Yoshio Mabuchi

It is very useful if we can observe the identical cell elements within the same sections by light microscopy (LM), transmission electron microscopy (TEM) and/or scanning electron microscopy (SEM) sequentially, because, the cell fine structure can not be indicated by LM, while the color is; on the other hand, the cell fine structure can be very easily observed by EM, although its color properties may not. However, there is one problem in that LM requires thick sections of over 1 μm, while EM needs very thin sections of under 100 nm. Recently, we have developed a new method to observe the same cell elements within the same plastic sections using both light and transmission (conventional or high-voltage) electron microscopes.In this paper, we have developed two new observation methods for the identical cell elements within the same sections, both plastic-embedded and paraffin-embedded, using light microscopy, transmission electron microscopy and/or scanning electron microscopy (Fig. 1).


Author(s):  
Ronald H. Bradley ◽  
R. S. Berk ◽  
L. D. Hazlett

The nude mouse is a hairless mutant (homozygous for the mutation nude, nu/nu), which is born lacking a thymus and possesses a severe defect in cellular immunity. Spontaneous unilateral cataractous lesions were noted (during ocular examination using a stereomicroscope at 40X) in 14 of a series of 60 animals (20%). This transmission and scanning microscopic study characterizes the morphology of this cataract and contrasts these data with normal nude mouse lens.All animals were sacrificed by an ether overdose. Eyes were enucleated and immersed in a mixed fixative (1% osmium tetroxide and 6% glutaraldehyde in Sorenson's phosphate buffer pH 7.4 at 0-4°C) for 3 hours, dehydrated in graded ethanols and embedded in Epon-Araldite for transmission microscopy. Specimens for scanning electron microscopy were fixed similarly, dehydrated in graded ethanols, then to graded changes of Freon 113 and ethanol to 100% Freon 113 and critically point dried in a Bomar critical point dryer using Freon 13 as the transition fluid.


Author(s):  
Jane A. Westfall ◽  
S. Yamataka ◽  
Paul D. Enos

Scanning electron microscopy (SEM) provides three dimensional details of external surface structures and supplements ultrastructural information provided by transmission electron microscopy (TEM). Animals composed of watery jellylike tissues such as hydras and other coelenterates have not been considered suitable for SEM studies because of the difficulty in preserving such organisms in a normal state. This study demonstrates 1) the successful use of SEM on such tissue, and 2) the unique arrangement of batteries of nematocysts within large epitheliomuscular cells on tentacles of Hydra littoralis.Whole specimens of Hydra were prepared for SEM (Figs. 1 and 2) by the fix, freeze-dry, coat technique of Small and Màrszalek. The specimens were fixed in osmium tetroxide and mercuric chloride, freeze-dried in vacuo on a prechilled 1 Kg brass block, and coated with gold-palladium. Tissues for TEM (Figs. 3 and 4) were fixed in glutaraldehyde followed by osmium tetroxide. Scanning micrographs were taken on a Cambridge Stereoscan Mark II A microscope at 10 KV and transmission micrographs were taken on an RCA EMU 3G microscope (Fig. 3) or on a Hitachi HU 11B microscope (Fig. 4).


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